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Search results for: SPECTROSCOPIC
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Spectroscopic and wireless sensor of hematocrit level
PublicationAn optical method for hematocrit measurement has been presented. the sensor, designed and developed by authors, consists of spectroscopic set-up controlled by a microcontroller. measurement results are sent via wireless module. experiment has confirmed the ability of the sensor to determine the hematocrit with appropriate measurementaccuracy.
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Spectroscopic wireless sensor of hematocrit level
PublicationAn optical method for hematocrit measurement is presented. The sensor, designed and developed by authors, consists of a spectroscopic set-up and a microcontroller. The work of the sensor is based on measurement of intensity of two selected spectral bands. Tests confirmed the ability of the sensor to determine the hematocrit level with appropriate measurement accuracy. Measurement results can be transmitted via wireless module to...
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Spectroscopic evaluation on pseudopolymorphs of sodium naproxen
PublicationThis paper demonstrates the assessment of vibrational spectroscopy methods such as middle infrared, near infrared and Raman spectroscopy (FTIR, FT-NIR, Raman) for the identification of pseudopolymorphic forms of a model active pharmaceutical ingredient (API) - sodium naproxen (NpxNa). NpxNa, in the form of three different pseudopolymorphs, was investigated by methods dedicated for solid state characterization: DSC (differential...
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Spectroscopic and Wireless Sensor of Hematocrit Level
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Spectroscopic evaluation on pseudopolymorphs of sodium naproxen
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Aggregation of imidazoacridinones - spectroscopic and microcalorimetric approach
PublicationImidazoacridinones (IA) belong to a group of polycyclic heteroaromatic antitumor compounds. IA create the aggregated form in water solution. Self-association of substances is a very important phenomenon in many fields of applied chemistry. It is also fundamental model reaction of many kinds of molecular interactions such as the micelle formation of amphiphilic substances and the binding of small organic molecules to macromolecules....
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Synthesis, spectroscopic and photophysical properties of novel styryldiazepinoporphyrazine
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Heteropolyanions doped polyimine—Preparation and spectroscopic properties
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Spectroscopic properties of the Ce-doped borate glasses
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Spectroscopic verification of ionic matrices for MALDI analysis
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Synthesis and Spectroscopic Properties of New Bis-tetrazoles
PublicationSyntheses of N,N'-phenyltetrazole podands link with aliphatic chains containing oxygen, nitrogen and sulphur atoms, are described. The complexing properties of these compounds towards metal cations (Fe2+, Cu2+, Zn2+, Co2+, Ni2+) were investigated by absorption and infrared spectroscopy. The UV-Vis titrations were performed to estimate the stability constant values of the respective complexes with Cu2+ ion. Changes in UV-Vis absorption...
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Raman spectroscopic investigation of blood and related materials
PublicationThis paper reports preliminary studies on use of Raman spectroscopy for investigation of blood. High quality blood spectra were recorded in-vitro with excitation wavelengths of 830 nm. Because of complex composition of the blood as well as by light attenuation and scattering in the tissues, spectra set up from wide, low-intensive Raman bands and intensive optical background. To get information about origin of bands in Raman spectra...
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Latent fingerprint imaging by spectroscopic optical coherence tomography
PublicationOptical coherence tomography (OCT) is a non-contact and non-invasive optical method for evaluating semitransparent and scattering objects. Its unique features, such as non-destructive 3D measurements of tested objects with a fast scanning rate, make this technique interesting for latent fingerprint reading, which is the subject of this paper. So far, OCT has not found widespread use for reading fingerprints directly from surfaces...
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Efficient signal processing in spectroscopic optical coherence tomography
PublicationSpectroscopic optical coherence tomography (SOCT) is an extension of a standard OCT technique, which allows to obtain depth-resolved, spectroscopic information on the examined sample. It can be used as a source of additional contrast in OCT images e.g. by encoding certain features of the light spectrum into the hue of the image pixels. However, SOCT require computation of time-frequency distributions of each OCT A-scan, what is...
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Polarization sensitive optical coherence tomography with spectroscopic analysis
PublicationOptyczna tomografia koherentna (OCT) jest nieinwazyjną, nieniszczącą i bezkontaktową metodą obrazowania wewnętrznej struktury obiektów i materiałów rozpraszających. Dodatkowo w połączeniu z analizą stanu polaryzacji metoda ta umożliwia badanie lokalnych zmian optycznej anizotropii występującej w badanym obiekcie. W artykule przedstawiono zalety oraz ograniczenia metody oraz przedstawiono propozycję rozszerzenia analizy o badanie...
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Spectroscopic analysis for polarization sensitive optical coherent tomography
PublicationW artykule przedstawiono właściwości oraz ograniczenia optycznej tomografii koherentnej z analizą stanu polaryzacji promieniowania optycznego. Zaproponowano nową spektroskopową metodę analizy sygnału pomiarowego w PS-OCT oraz przedstawiono i omówiono zalety nowego rozwiązania na bazie uzyskanych wyników pomiarowych.
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Spectroscopic Properties of Yb3+/Tb3+Doped Germanate Glasses
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Spectroscopic properties of rare earth doped germanate glasses
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Temperature-Dependent Spectroscopic Ellipsometry of Thin Polymer Films
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Heteropolyanions doped polyacetylene—Preparation, spectroscopic and catalytic properties
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FTIR- SPECTROSCOPIC CHARACTERISTICS OF THE DZHAKSY-KLYCH DEPOSIT SALTS
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Structural and spectroscopic analysis of a new family of monomeric diphosphinoboranes
PublicationWe present a series of amino- and aryl(diphosphino)boranes R2PB(R’’)PR’2, where R2P, R’2P = tBu2P, tBuPhP, Ph2P, Cy2P, and R’’ = iPr2N, Ph, which were obtained via the metathesis reaction of iPr2NBBr2 or PhBBr2 with selected lithium phosphides. The structures of isolated diphosphinoboranes were characterized in the solid state and in solution by means of X-ray diffraction and NMR spectroscopy, respectively. The utility of these...
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Determination of Selected Metals in Fruit Wines by Spectroscopic Techniques
PublicationThe determination of metals in different types of food and beverages samples has drawn significant attention due to several reasons with the most important one being the nutritional and toxic effects of these elements or their compounds. The knowledge of certain elements content in wines/fruit wines is of special interest due to their toxicity in case of excessive intake and also the effect they seem to have on the organoleptic...
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Feasibility study of a Raman spectroscopic route to drug detection
PublicationWe present an surface-enhanced Raman spectroscopy (SERS) approach for detection of drugs of abuse in whole human blood. We utilize a near infrared laser with 830 nm excitation wavelength in order to reduce the influence of fluorescence on the spectra of blood. However, regular plasmon resonance peak of plasmonic nanoparticles, such as silver or gold fall in a much lower wavelength regime about 400 nm. Therefore, we have shifted...
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Effect of ectoine on hydration spheres of peptides–spectroscopic studies
PublicationIn this paper, we use FTIR spectroscopy to characterize the hydration water of ectoine, its interactions with two peptides–diglycine and NAGMA, and the properties of water molecules in the hydration spheres of both peptides changed by the presence of the osmolyte. We found that the interaction of ectoine with the peptide hydration shells had no effect on its own hydration sphere. However, the enhanced hydration layer of the osmolyte...
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Microcrystalline diamond film evaluation by spectroscopic optical coherence tomography
PublicationThis study has focused on the microcrystalline diamond film (MCD) thickness evaluation. For this purpose, optical coherence tomography (OCT) enhanced by spectroscopic analysis has been used as a method of choice. The average thickness of the tested layer was about 1.5 µm, which is below the standard 2-point OCT resolution. In this case, the usefulness of the spectroscopic analysis was confirmed for the evaluation of the thickness...
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Parallel multithread computing for spectroscopic analysis in optical coherence tomography
PublicationSpectroscopic Optical Coherence Tomography (SOCT) is an extension of Optical Coherence Tomography (OCT). It allows gathering spectroscopic information from individual scattering points inside the sample. It is based on time-frequency analysis of interferometric signals. Such analysis requires calculating hundreds of Fourier transforms while performing a single A-scan. Additionally, further processing of acquired spectroscopic information...
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Low-temperature spectroscopic and scintillation characterisation of Ti-doped Al2O3
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Spectroscopic investigation of hydrothermally synthesized zeolites from expanded perlite
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Spectroscopic properties of Yb3+/Er3+-doped antimony-phosphate glasses
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Spectroscopic and quantum chemical study of phthalocyanines with 1,4,7-trioxanonyl moieties
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Spectroscopic investigations into degradation of polymer membranes for fuel cells applications
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Doping-Induced Immobile Charge Carriers in Polyazomethine: A Spectroscopic Study
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Spectroscopic and Physicochemical Investigations of Azomethines with Triphenylamine Core towards Optoelectronics
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Spectroscopic properties and energy level location of Eu2+ in Sr2Si5N8 phosphor
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Cobalt(II) silanethiolato complexes with dimethylpyridines:crystal structures and spectroscopic studies
PublicationTri-tert-butoksysilanotiolany kobaltu(II) z 2,5-dimetylopirydną, 3,4-dimetylopirydną i 3,5-dimetylopirydną jako dodatkowymi ligandami zostały zsyntetyzowane w reakcji z bimetalicznym [Co{SSi(OtBu)3}(NH3)]2 z odpowiednią pochodną pirydyny. Kompleksy zostały zcharakteryzowane za pomocą rentgenografii strukturalnej, analizy elementarnej, spektroskopii FT-IR oraz UV-vis. Prezentowane kompleksy są cztero- i pięciokoordynacyjne o rdzeniu...
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Spectroscopic and photophysical properties of ZNTPP in a room temperature ionic liquid
PublicationThe steady-state absorption and emission spectra and the time-resolved Soret- and Q-band excited fluorescence profiles of the model metalloporphyrin, ZnTPP, have been measured in a highly purified sample of the common room temperature ionic liquid, [bmim][PF(6)]. S(2)-S(0) emission resulting from Soret-band excitation behaves in a manner completely consistent with that of molecular solvents of the same polarizability. The ionic...
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Raman spectroscopic study of Ni2+-DNA interactions in aqueous systems
PublicationMetodą ramanowskich widm różnicowych określono sposób oddziaływania jonu Ni2+ z DNA(CT) w układach wodnych. Kation Ni(II) koordynuje w pozycjach N7 guaniny (G) i adeniny (A) w powtarzających się sekwencjach GG, AA i GA cząsteczki DNA. Jednocześnie Ni2+ oddziałuje zewnątrz sferowo poprzez cząsteczki wody z grupami fosforanowymi DNA.
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Spectroscopic Optical Coherence Tomography for Thin Layer and Foil Measurements
PublicationThe main goal of this research was to assess if it is possible to evaluate the thickness of thin layers (both thin films on the surface and thin layers below the surface of the tested object) and foils using optical coherence tomography (OCT) for thickness assessment under the resolution of the standard commercially available OCT measurement system. In the proposed solution, light backscattered from the evaluated thin layer has...
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Comparability of Raman Spectroscopic Configurations: A Large Scale Cross-Laboratory Study
PublicationThe variable configuration of Raman spectroscopic platforms is one of the major obstacles in establishing Raman spectroscopy as a valuable physicochemical method within real-world scenarios such as clinical diagnostics. For such real world applications like diagnostic classification, the models should ideally be usable to predict data from different setups. Whether it is done by training a rugged model with data from many setups...
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Comment on "Quantitative comparison of analysis methods for spectroscopic optical coherence tomography"
PublicationIn a recent paper by Bosschaart et al. [Biomed. Opt. Express 4, 2570 (2013)] various algorithms of time-frequency signal analysis have been tested for their performance in blood analysis with spectroscopic optical coherence tomography sOCT). The measurement of hemoglobin concentration and oxygen saturation based on blood absorption spectra have been considered. Short time Fourier transform (STFT) was found as the best method for...
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Magnetoelectric, spectroscopic, optical and elastic properties of Co-doped BaTiO3 ceramics
Publicationhe BaTiO3 perovskite is widely used in the electronic technology due to its dielectric, piezoelectric and ferroelectric properties and is a well-known base for obtaining a promising multifunctional material. In this paper we report the extensive studies on the Co-doped BaTiO3 ceramics for the wide range cobalt content. Full structural characterization of studied samples in a 20–450 K range was provided. The results of research...
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Interactions in aqueous solutions of K-peptide and DMSO – spectroscopic and calorimetric studies
PublicationIntroduction K-peptide (GILQINSRW) – short 9 amino acid fragment of the hen egg white lysozyme has the ability to form amyloid structures. Dimethyl sulfoxide (DMSO) is an osmolyte which can alter this ability. Our goal was to get an insight into the mechanism of Kpeptide-DMSO interactions in aqueous solutions. Such a knowledge can be helpful to understand processes leading to various neurodegenerative diseases. Methods ATR-FTIR...
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Optical Spectroscopic Studies of Tetrahydrofuran Fragmentation Induced by Collisions with Dihydrogen Cations
PublicationCollisions of dihydrogen cations with tetrahydrofuran molecules have been studied. Luminescence spectra and the emission functions of the excited products at projectile energies ranging from 8 to 1000 eV have been measured using collision-induced emission spectroscopy. The recorded spectra are dominated by the atomic lines of the hydrogen Balmer series, whose intensities decrease more quickly than derived by the quantum-theoretical...
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Spectroscopic Studies of Amino Acid Ionic Liquid-Supported Schiff Bases
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Hybrid carbon-TiO2 spheres: Investigation of structure, morphology and spectroscopic studies
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Spectroscopic properties of Eu-doped antimony-germanate glass and glass-ceramics
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Spectroscopic studies of UV-irradiated poly(vinyl alcohol)/elastin blends
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Spectroscopic and microscopic study of Prussian blue film for electrochromic device application
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Spectroscopic insight into supramolecular assemblies of boric acid derivatives and β-cyclodextrin
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