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Wyniki wyszukiwania dla: ambient mass spectrometry
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Influence of pH and low-molecular weight organic compounds in solution on selected spectroscopic and analytical parameters of flowing liquid anode atmospheric pressure glow discharge (FLA-APGD) for the optical emission spectrometric (OES) determination of Ag, Cd, and Pb
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Comparison of the performance of direct current atmospheric pressure glow microdischarges operated between a small sized flowing liquid cathode and miniature argon or helium flow microjets
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Effect of the addition of non-ionic surfactants on the emission characteristic of direct current atmospheric pressure glow discharge generated in contact with a flowing liquid cathode
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Wprowadzenie do analiz egzergetycznych, PG_00059783
Kursy OnlineThe aim of the course is to present the basic issues to carry out the balance of exergy and entropy in addition to the balance of mass and energy. To show the definition of the maximum work that a certain matter can do in a thermodynamic process when transitioning to equilibrium with its surroundings. To refer to chemical exergy and show the application of the exergy balance to define losses in a thermodynamic cycle.
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Od pragmatyzmu do masowej indywidualizacji w kształtowaniu form oświetlania miasta
Publikacja„Od pragmatyzmu do masowej indywidualizacji w kształtowaniu form oświetlenia miasta” podejmuje dwa istotne wątki. Z jednej strony mówi o ewolucji architektonicznych użytkowych form oświetleniowych na przestrzeni wieków, z drugiej zaś zwraca uwagę na oznaki rewolucji cyfrowej i jej wpływ na kształtowanie oświetlenia miasta. Te dwa wątki łączą się w dokonanej obserwacji pojawienia się nowego paradygmatu masowej indywidualizacji...
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Influence of Operation Conditions on Temperature Hazard of Lithium-Iron-Phosphate (LiFePO4) Cells
PublikacjaThe article presents and discusses the results of research on hazard, especially temperature, for selected lithium-ion-phosphate cells operated in accordance with the manufacturer’s recommendations but used under onerous mining conditions. This applies to the performance of cells in battery sets without the application of any management system (BMS). On the basis of the obtained test results, first of all, the influence of the...
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Techniques of acquiring additional features of the responses of individual gas sensors
PublikacjaGas sensors usually exhibit lack of selectivity, require fre quent calibration, exhibit drift of the response and a lot of factors, such as humidity or ambient temperature, influen ce their performance. Different approaches can be used to overcome this shortcomings. Building arrays of different sensors and usage of pattern recognition methods to analyze responses of elements...
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Structure and Stability Characterization of Natural Lake Pigments Made from Plant Extracts and Their Potential Application in Polymer Composites for Packaging Materials
PublikacjaNatural dyes were extracted from various plant sources and converted into lake pigments based on aluminum and tin. Three different plants (weld, Persian berries, and Brazilwood) were chosen as representative sources of natural dyes. High-performance liquid chromatography (HPLC) and triple-quadrupole mass spectrometry (QqQ MS) were used to identify dyestuffs in the raw extracts. The natural dyes and lake pigments were further characterized...
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Insight into Potassium Vanadates as Visible-Light-Driven Photocatalysts: Synthesis of V(IV)-Rich Nano/Microstructures for the Photodegradation of Methylene Blue
PublikacjaPhotocatalysis is regarded as a promising tool for wastewater remediation. In recent years, many studies have focused on investigating novel photocatalysts driven by visible light. In this study, K2V6O16·nH2O nanobelts and KV3O8 microplatelets were synthesized and investigated as photocatalysts. Samples were obtained via the facile method based on liquid-phase exfoliation with ion exchange. By changing the synthesis temperature...
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Green capsule phase microextraction employing hydrophobic monolithic sol-gel octadecyl siloxane platforms for the monitoring of organophosphorus pesticides in environmental water samples
PublikacjaIn this study, a novel, facile and green capsule phase microextraction (CPME) method is presented for the extraction and preconcentration of organophosphorus pesticides (i.e., chlorpyrifos, disulfoton, ethoprophos, fenchlorphos, prothiofos, and parathion-methyl) from environmental water samples. Monolithic sol-gel octadecyl siloxane (sol-gel C18) sorbent encapsulated within porous polypropylene capsules was synthesized, characterized,...
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The dispersive micro-solid phase extraction method for MS-based lipidomics of human breast milk*
PublikacjaA simple and rapid microextraction method ensuring high lipidome coverage was developed for liquid chromatography mass spectrometry (LC-MS)-based lipidomics of human breast milk. The dispersive microsolid phase extraction (D-µ-SPE) technique, coupled with the design of experiment (DoE) method, enabled the study of the influence of several conditions (desorption solvent, stationary phase ratio, and sorption and desorption time)...
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Qualitative analysis of phospholipids and their oxidised derivatives – used techniques and examples of their applications related to lipidomic research and food analysis
PublikacjaPhospholipids (PLs) are important biomolecules that not only constitute structural building blocks and scaffolds of cell and organelle membranes, but also play a vital role in cell biochemistry and physiology. Moreover, dietary exogenous PLs are characterized by high nutritional value and other beneficial health effects, which are confirmed by numerous epidemiological studies. For this reason, PLs are of high interest in lipidomics...
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Emission profile of butan-2-one oxime from commercially available neutral silicone sealant
PublikacjaThe paper presents results of research on emission profile of butan-2-one oxime (methyl ethyl ketoxime, MEKO) released from two types of commercially available neutral silicone sealants: silicone type ‘S’ and silicone type ‘T’. To determine the emissions from silicone samples, the system consists of a stationary emission chamber, and the thermal desorption-gas chromatography-mass spectrometry system was applied. First, the research...
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Two bacterial small heat shock proteins, IbpA and IbpB, form a functional heterodimer
PublikacjaSmall heat shock proteins (sHsps) are a conserved class of ATP-independent chaperones which in stress conditions bind to unfolded protein substrates and prevent their irreversible aggregation. Substrates trapped in sHsps-containing aggregates are efficiently refolded into native structures by ATP-dependent Hsp70 and Hsp100 chaperones. Most γ-proteobacteria possess a single sHsp (IbpA), while in a subset of Enterobacterales, as...
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Real-time monitoring of volatiles and particles emitted from thermoplastic filaments during 3D printing
PublikacjaThe proliferation of consumer-grade three-dimensional (3D) printers using fused deposition, also known as fused filament fabrication, has given rise to concerns over the exposure of users to potentially harmful substances. Thermoplastic filaments made of different polymers are extruded through a heated printer nozzle and deposited layer by layer on a build platform to form the printed object. This process leads to the emission...
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Development and Validation of SPE-HPLC-MS/MS Method for Determining Cyclophosphamide in Surface Waters
PublikacjaA rapid and selective method for trace amounts determination of cyclophosphamide in surface water samples has been developed. A solid phase extraction SPE method for extraction and clean-up procedure has been optimized for determination by reversed-phase high-performance liquid chromatography with tandem mass spectrometry. The analyses proceed in the positive ion mode by means of the electrospray ionization method (ESI). Clean...
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Phototransformation of Amlodipine: Degradation Kinetics and Identification of Its Photoproducts
PublikacjaNowadays, monitoring focuses on the primary compounds and does not include degradation products formed during various biological and chemical processes. Transformation products may have the same effects to human health and the environment or sometimes they can be more toxic than the parent compound. Unfortunately, knowledge about the formation of degradation products is still limited, however, can be very important for the environmental...
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Multi-Analytical Techniques for the Study of Burial Clothes of Polish King Sigismund III Vasa (1566–1633) and His Wife Constance Habsburg (1588–1631)
PublikacjaThe subjects of this research are the burial clothes of Polish King Sigismund III Vasa and his wife Constance, which were woven and embroidered with silk and metal threads. Fragments of the textiles underwent spectroscopic, spectrometric, and thermogravimetric analyses. The hydrofluoric acid extraction method was improved to isolate various classes of dyes from the textile samples that had direct contact with human remains. High-performance...
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Blood concentrations of a new psychoactive substance 4-chloromethcathinone (4-CMC) determined in 15 forensic cases
PublikacjaPurpose: The 4-chloromethcathinone (4-CMC) is a synthetic derivative of cathinone and belongs to new psychoactive substances. Neither data on the effects of 4-CMC on the human body, nor on nontoxic, toxic and lethal concentrations in biological materials have been published in the literature. This paper describes the results of an analysis of the blood concentrations of 4-CMC determined in 15 forensic cases related to nonfatal...
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Complementary use of GCxGC–TOF–MS and statistics for differentiation of variety in biosolid samples
PublikacjaFormation of biosolid cakes, which are one of the main wastes generated in wastewater treatment plants, is connected with emission of many hazardous chemical compounds, including odoriferous ones. To optimize particular processes of biosolid cake processing, it is necessary to assess chemical composition of the gas mixtures containing the compounds released from the cakes. The paper proposes application of two-dimensional gas chromatography...
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Determination of flow properties of a serial connection of a pressure relief valve (C=6.4, b=0.45) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...
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Determination of flow properties of a serial connection of a directional control valve (C=2.4, b=0.26) and a silencer (C=1.4) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a pressure relief valve (C=5.3, b=0.38) and a silencer (C=3.4) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...
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Determination of flow properties of a serial connection of a directional control valve (C=2.4, b=0.26) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a pressure relief valve (C=3.3, b=0.40) and a silencer (C=1.4) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...
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Determination of flow properties of a serial connection of a pressure relief valve (C=6.4, b=0.45) and a silencer (C=6.8) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...
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Determination of flow properties of a serial connection of a directional control valve (C=2.4, b=0.26) and a silencer (C=3.4) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a pressure relief valve (C=6.2, b=0.38) and a silencer (C=3.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...
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Determination of flow properties of a serial connection of a directional control valve (C=2.4, b=0.26) and a silencer (C=3.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.8, b=0.25) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=5.7, b=0.32) and a silencer (C=1.4) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.1, b=0.14) and a silencer (C=1.4) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=5.7, b=0.32) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a pressure relief valve (C=6.2, b=0.38) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...
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Determination of flow properties of a serial connection of a pressure relief valve (C=5.3, b=0.38) and a silencer (C=3.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...
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Determination of flow properties of a serial connection of a directional control valve (C=5.5, b=0.37) and a silencer (C=1.4) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.0, b=0.11) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.0, b=0.11) and a silencer (C=3.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.8, b=0.25) and a silencer (C=3.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.1, b=0.14) and a silencer (C=6.8) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=5.7, b=0.32) and a silencer (C=3.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a pressure relief valve (C=3.3, b=0.40) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...
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Determination of flow properties of a serial connection of a directional control valve (C=2.0, b=0.11) and a silencer (C=1.4) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.1, b=0.14) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a pressure relief valve (C=4.4, b=0.42) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...
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Determination of flow properties of a serial connection of a pressure relief valve (C=6.2, b=0.38) and a silencer (C=1.4) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...
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Determination of flow properties of a serial connection of a pressure relief valve (C=3.3, b=0.40) and a silencer (C=3.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...
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Determination of flow properties of a serial connection of a directional control valve (C=2.0, b=0.11) and a silencer (C=3.4) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a pressure relief valve (C=4.4, b=0.42) and a silencer (C=1.4) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...
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Determination of flow properties of a serial connection of a pressure relief valve (C=7.3, b=0.49) and a silencer (C=6.8) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...