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  • Impedance spectroscopy of the lithium titanate doped by copper thin films

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    Lithium titanate doped by copper thin films were derived by sol-gel method. Prepared gel was deposited by spin-coating technique. Samples with various content of Cu were measured by impedance spectroscopy method in a wide range of temperature, from -120 up to 150 deg.

  • Investigation of the uniformity of TeO2:Eu layer

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    TeO2 doped by Eu thin films manufactured by magnetron sputtering method were measured by XPS method.  Te-Eu mosaic target with diameter of 50.8 mm was sputtered for about 45 min in argon-oxygen atmosphere what resulted in 300 nm film thickness deposition. The pressure in the deposition chamber was below 0.2 Pa and substrate was heated  at 200 oC during...

  • Study of the chemical state of Gd in a Ba-La-Gd-Co based ceramic

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    Barium, Lanthanum, Gadolinium and Cobaltium precursors were used for production of ceramic materials. Samples were produced by standard solid state reaction.  Samples were annealed at 300 Celsius degree in wet and dry atmosphere. Annealing takes 72h or 2h. Results of annealing on a Gadolinum were observed by X-Ray photoemission spectroscopy (XPS), OmicronNanotechnology....

  • X-Ray photoemission spectroscopy measurements of the Nb-V-Sr-O ceramics

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    Niobium doped strontium vanadate based perovskite SrV1-xNbxO3-δ materials were prepared via conventional solid state reaction (SSR) method. For comparison, different samples with a various amount of niobium dopant in the structure were synthesized; x = 0; 0,2; 0,5; 0,8 and 1. Samples were sintered by two-steps: first under a pure hydrogen (purity >99.999%)...

  • Chemical investigation of the Al2O3 ultra-thin films

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    Ultra-thin layers of oluminum oxide (Al2O3) were deposited by ALD method.  Atomic layer deposition provides precise thickness control down to a single atomic layer. The precursors used were trimethylaluminum (Sigma-Aldrich) and purified water. The deposition of the atomic layer was carried out at 200 °C. Samples with a thickness of 2 and 8 nm of alumina...

  • XPS analysis of the GO based materials

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    Graphene oxides samples were measured by XPS method. The X-ray photoemission spectroscopy measurements were carried out with Omicron NanoTechnology UHV equipment. The hemispherical spectrophotometer was equipped with a 128-channel collector. The XPS measurements were performed at room temperature at a pressure below 1.1 × 10−8 mBar. The photoelectrons...

  • Chemical properties of bismuth telluride – carbon composites.

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    Carbon nanotubes and amorphous carbon have been introduced into bismuth telluride matrix (in 0.15 and 0.30 wt % ratio) in order to investigate influence of carbon on composite’s thermoelectric properties. Composites with well-dispersed additives have been obtained by sonication and ball-milling. Chemical composition of materials was confirmed by XPS...

  • Lanthanum investigations in ceramics annealed in a dry and wet atmosphere

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    Ceramics based on Barium, Lanthanum, Gadolinium and Cobaltium were produced by standard solid state reaction from oxides and carbonate powders. After sintring, samples were annealed for 2 hours or 72 hours at 300 Celsius degree in a both: wet and dry atmosphere. Results of annealing on a chemical composition and valence state of lanthanum were observed...

  • Formation of gold nanostructures detected by XPS method

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    Gold nanostructers were manufactured by thermal dewetting of thin film. Film with thickness of 2.8 nm was deposited by magnetron sputtering method. As a result of annealing at 550 deg, nanostructures appear. Bulk gold, as-deposited gold film and metallic nanostructures were measured by XPS method. 

  • Morphology of the sol-gel derived LTO:Cu films

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    Morphology of the lithium titanate doped by Cu thin films were investigated by SEM microscope. Films were deposited by spin-coater from sol-gel derived sol. SEM images showed a high porous structure, tipaciall for sol-gel based films. For measurements samples with a various content of Cu were selected.

  • Mn-Co nanofilms on nickel foam measured by XPS mehod

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    Manganium-Cobaltium based thin films were electrochemically deposited on a Ni based subsrates in a one-step process at −1.1 V vs. Ag/AgCl in an aqueous solution of differently concentrated Mn(NO3)2·4H2O and Co(NO3)2·6H2O with the deposition time limited by charges of 60, 120, and 200 mC at 25 °C. The concentration ratios of Mn(NO3)2·4H2O to Co(NO3)2·6H2O...

  • Depth XPS profile of Fe-S layers on a titanium substrate

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    Depth XPS profile of Fe-S layers on a titanium substrate was measured. Material was etched by Argon ion gun and measured by XPS method. For each sample, three times per 10 minutes each was sputtered.

  • Tellurite based glass doped by Eu3+ ions - XPS measurements

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    Eu3+ doped tellurite glass ceramics containing SrF2 nanocrystals were prepared using melt quenching technique and subsequent heat treatment of glass in 370 °C for different time periods. Thermal properties of glass matrix have been determined based on DSC measurements. XRD and XPS results confirmed formation of SrF2 nanocrystals in glass matrices after...

  • XPS analysis of TBBO glass

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    Glasses and glass-ceramics with nominal composition 73 TeO2– 4BaO– 3Bi2O3–18SrF2-2RE2O3 (where RE = Eu, Dy) have been synthesized by conventional melt-quenching technique and subsequent heat treatment at 370 °C for 24 h in air atmosphere. Various Eu3+ to Dy3+ molar ratio have been applied to investigate luminescence properties in both glass and glass-ceramic...

  • Dewetting of silver films detected by XPS method

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    Dewetting of silver thin films was detected by XPS method. Thin metallic films were deposited by magnetron sputtering method. Formation of nanostructures , as a result of thermal annealing, was confirmed by SEM microscope. For comparision three samples were measured. Bulg gold, as-deposited silver film with thickness of 3 nm and nanostructures.

  • Hydrogenation process ofTiO2/BiVO4/PEDOT:PSS observed by XPS method

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    Titania nanotubes synthesis was based on a two-stage anodization process at water/ethylene glycol (5%/95%) electrolyte containing 0.27 M NH4F and 1 M H3PO4 described previously. Anodization process was performed in two-electrode cell compartment using platinum mesh as a cathode. The distance between electrodes was about 2 cm. The anodization voltage...

  • XPS study of the YST ceramics

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    Yttrium-doped strontium titanate  was prepared via conventional solid-state reaction method from Y2O3 (Sigma Aldrich, 99,9%), TiO2 (Sigma Aldrich, 99%) and SrCO3 (Sigma Aldrich,98%). For comparision, two other techniques were used for synthesis: Pechini and wet methods. Both kind of samples were measured, after and before reduction process (in a hydrogen)....

  • Analysis of the properties of the YSTF ceramics materials before and after reduction

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    The valence of titanium in reduced YSTF ceramics materials was investigated. Ceramics were reduced by annealing in a hydrogen atmosphere. For comparison unreduced sample was also measured. Valance state was measured by XPS method.

  • Detection of the Ag nanoparticles in Te-Bi-Ba-Oa glass

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    The influence of the manufacturing parameters of tellurium-bismuth-barium glasses on the presence of silver nanoparticles was investigated. Glasses were annealed at 330, 335, 340, 345 and 350 degrees Celsius for 24 and 48 hours. Presence of the Ag nanoparticles was measured by XPS method. The growth of nanoparticles was observed along with the extension...

  • XRD investigations of the lithium titanate thin films

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    Nanocrystalline thin films with 800 nm thickness were prepared by sol–gel method. To examine the influence of the annealing temperature on as-prepared films crystallization, the coatings were heated at temperature from 500 °C up to 600 °C  for 20h. Structure of manufactured thin films was investigated using X-ray diffraction (XRD). The most visible...

  • Investigations of the valence state of Co in a MnCoO ceramics

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    McCoO ceramics materials were produced by solid state reaction and sintred in a furnance in air atmosphere for 20h. Annealing temperature was 600 Celsius degree. For investigations a series of samples, with a various composition was chosen: MnCoO, Mn, Co2O and Mn2CoO. Chemical behaviour of the Cobaltium was measured by XPS method.  The analyses were...

  • XPS measurement of the Fe-Ti based materials

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    The mono‐ and bimetal‐modified (Pd, Cu) titanium(IV) oxide and iron oxide (III) photocatalysts were prepared by chemical reduction method and characterized using XPS method. The composition of elements incorporated in the surface layer of mono- and bimetallic photocatalysts was determined by XPS analysis, as well as the valence state of elements. Measurements...

  • SPTNO ceramics measured by XPS method

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    SPTNO (Sr-Pr-Ti-Ni-O) ceramic were manufactured by solid state reaction, from oxides compounds. Synthesis conducted in air atmosphere at temperature in a range of 800-900 deg. Chemical composition of prepared materials were measured by XPS (X-Ray photoemision spectroscopy) method. UHV OmicronNanotechnology system with 128 channel Argus hemispherical...

  • SEM images of dewetted gold films

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    Gold nanostructures were prepared on silicon - Si(111) as a substrate. as a result of dewetting process. Thin golds films were deposited using a table-top dc magnetron sputtering coater under pure Ar plasma conditions . The Au target had 99.99% purity, the rate of Au layer deposition was about 0.4 nm·s−1 and the incident power was 32 W. The thickness...

  • XPS study of the lithium titanate doped by copper

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    Lithium titanate doped by copper was measured by X-ray photoemission spectroscopy. For sol-gel synthesis lithium acetate dehydrate from Alfa Aesar GmbH &Co and titanium (IV) butoxide 97% from Aldrich were used as reagents. Copper (II) nitrate from Alfa Aesar was used as a source of Cu dopant. It was added in the proper weight to get an x index equal...

  • Formation of gold anostructures detected by SEM microscope

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    Gold nanostructures were prepared on silicon - Si(111) as a substrate. The substrates (1 × 1 cm2  of area) were cleaned with acetylacetone and then rinsed in ethanol. Thin Au films (with thicknesses in a range of 1.7–5.0 nm) were deposited using a table-top dc magnetron sputtering coater (EM SCD 500, Leica) under pure Ar plasma conditions (Argon, Air...

  • SEM images of tge gold nanostructures on silicon

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    Au nanostructures were prepared on Si(111) as a substrate. The substrates (1 × 1 cm2  of area) were cleaned with acetylacetone and then rinsed in ethanol. Thin Au films (with thicknesses in a range of 1.7–5.0 nm) were deposited using a table-top dc magnetron sputtering coater (EM SCD 500, Leica) under pure Ar plasma conditions (Argon, Air Products 99.999%)....

  • Oxidation of silver nanostructures

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    Silver nanostructures were prepared on  Si substrate. Thin Ag films (2 and 6 nm thickness) were deposited using a tabletop dc magnetron sputtering coater (EM SCD 500, Leica) in pure Ar plasma. The Ag target was of 99.99% purity, the rate of layer deposition was about 0.4 nm·s−1 , and the incident power was in the range of 30–40 W. The layer thickness...

  • Surface modifcation of PMMA polymer detected by XPS

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    In order to obtain the experimental specimens, four PMMA/PC61BM samples with the following  mass proportions were prepared: 10%, 20%, 30%, and 40%. In addition, as a reference, a PMMA sample without  PC61BM was prepared as well. For the fabrication process, PC61BM 99.5% (Solenne BV), chloroform HPLC  (Sigma Aldrich), and PMMA (commercially available...

  • Chemical analysis of the Au-Ag nanoaloys

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    The nanostructures of AuAg nanoalloys were prepared by sequential sputtering of gold and silver thin films.  Single layer thickness was usually 2.8 nm were deosted by magnetron sputtering method in a Ar plasma. As deposited layers were annealed in Ar atmosphere at 550 degress for 15 minutes. For XPS measurements five samples were selected: pure gold...

  • Measurements of the chemical composition of LTO:Cu powders

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    Lithium titanate doped by copper was measured by X-ray photoemission spectroscopy (XPS). For sol-gel synthesis lithium acetate dehydrate and titanium (IV) butoxide 97% and copper (II) nitrate from Alfa Aesar were used as a reagents. Cu precursor was added in the proper weight to get an x index equal 0, 0.1 and 0.2. In the first step lithium acetate...

  • Comparison of XPS spectra of Ag3d for silver nanostructures and bulk material

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    Ag nanostructures were prepared on borosilicate glass (Corning 1737F) and Si substrates. In both cases, the substrateswere cleaned with acetylacetone and then rinsed in ethanol. Thin Ag films (2 and 6 nm thickness) were deposited using a tabletop dc magnetron sputtering coater (EM SCD 500, Leica) in pure Ar plasma (argon, Air Products 99.999%). The...

  • Sol-gel derived lithium titanate powders measured by XPS method

    Open Research Data
    open access

    For sol-gel synthesis lithium acetate dehydrate from Alfa Aesar GmbH &Co and titanium (IV) butoxide 97% from Aldrich were used as reagents. Copper (II) nitrate from Alfa Aesar was used as a source of Cu dopant. It was added in the proper weight to get an x index equal 0, 0.1 and 0.2. In the first step lithium acetate and copper nitrate were dissolved...

  • Video traffic data - Interchanges Podwarpie (S1-86) - Entry + exit lanes, Poland

    The data includes video traffic data registered with 4 video cameras on entry or exit lanes of the Podwarpie interchange within S1 expressway  in Poland (interchange of expressway  S1 and national road 86), located in the Silesian Agglomeration). The data covers the one day: 23.05.2017 (expressway  S1).

  • Video traffic data - Interchange Podwarpie (S1-86) - weaving, Poland

    The data includes video traffic data registered with 4 video cameras at weaving area (weaving section type A) of the Podwarpie interchange within S1 expressway  in Poland (interchange of expressway  S1 and national road 86), located in the Silesian Agglomeration. The data covers the one day: 23.05.2017 (road 86).

  • Video traffic data - Interchanges Grota Roweckiego (S86 - Grota Roweckiego)

    The data includes video traffic data registered with 2 video cameras at entry and exit lanes of the Grota Roweckiego interchange within S86 expressway in Poland (interchange of expressway S86 and Grota Roweckiego street), located in the Silesia Agglomeration. The data covers the one days: 23.05.2017 (expressway S86). The video cameras installed on the...

  • PIT revenues in 2012-2021 in PLN billion

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    Taxes are the primary source of income for the state budget and local government units. Tax issues play an important role in the economy of each country, its citizens and economic entities that operate on the market. Taxes are the main instrument of the state's influence on the economy, as they cover almost all natural and legal persons operating on...

  • Microorganisms in the air within the Gdańsk-Szadółki landfill and adjacent area in 2015

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    This data set contains the results of microbiological examination of air samples collected at Gdańsk Szadółki Landfill (Poland) in 2015. The range of examination included qualitative and quantitative assesment of selected species of bacteria and mold fungi, with particular focus on pathogenic  and potentially pathogenic fungi and bacteria. The collected...

  • Microorganisms in the air within the Gdańsk-Szadółki landfill and adjacent area in 2018

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    This data set contains the results of microbiological examination of air samples collected at Gdańsk Szadółki Landfill (Poland) in 2018. The range of examination included qualitative and quantitative assesment of selected species of bacteria and mold fungi, with particular focus on pathogenic  and potentially pathogenic fungi and bacteria. The collected...

  • Microorganisms in the air within the Gdańsk-Szadółki landfill and adjacent area in 2016

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    The data collection contains the results of microbiological examination of air samples collected at Gdańsk Szadółki Landfill (Poland). The Gdańsk Szadółki Landfill is one of the biggest of facilities of this type in the country. It occupies an area of 75 hectares and serves around 500 thousand of local residents. The landfill receives around 250 million...

  • Microorganisms in the air within the Gdańsk-Szadółki landfill and adjacent area in 2017

    Open Research Data
    open access

    This data set contains the results of microbiological examination of air samples collected at Gdańsk Szadółki Landfill (Poland) in 2017. The range of examination included qualitative and quantitative assesment of selected species of bacteria and mold fungi, with particular focus on pathogenic  and potentially pathogenic fungi and bacteria. The collected...

  • Microorganisms in the air within the Gdańsk-Szadółki landfill and adjacent area in 2019

    Open Research Data
    open access

    This data set contains the results of microbiological examination of air samples collected at Gdańsk Szadółki Landfill (Poland) in 2019. The range of examination included qualitative and quantitative assesment of selected species of bacteria and mold fungi, with particular focus on pathogenic  and potentially pathogenic fungi and bacteria. The collected...

  • Bacteria in water and bottom sediments in Puck Bay area (Baltic Sea)

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    The samples for testing were collected from 5th of November 2007 to 14th of December 2007. In total, there were 147 samples collected from 30 sites, including 57 water samples and 90 sediment samples. Water was sampled from the surface and directly above the layer of bottom sediment. Sediments, regardless of length of the sample core were sampled from...

  • Bacteriological monitoring of coastal sea waters – Gulf of Gdańsk (Baltic Sea) in 2009

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    The dataset contains the results of a bacteriological and physicochemical studies of Gdansk Bay coastal waters within the administrative boundaries of Gdańsk city in 2009. The examined material consisted of water samples collected from 15 sampling points. The aim of this study was to determine the number of Escherichia coli and the number of intestinal...

  • The results of physico – chemical and microbiological testing of watercourses around the municipality of Gdańsk in 2009

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    The dataset contains the results of a bacteriological and physico-chemical study of watercourses waters within the administrative boundaries of Gdańsk city in 2009. The examined material consisted of water samples collected from 16 watercourses within the administrative boundaries of Gdańsk, Poland.

  • The results of physico – chemical and microbiological testing of watercourses around the municipality of Gdańsk in 2011

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    The dataset contains the results of a bacteriological and physico-chemical study of watercourses waters within the administrative boundaries of Gdańsk city in 2011. The examined material consisted of water samples collected from 16 watercourses within the administrative boundaries of Gdańsk, Poland.

  • The results of physico – chemical and microbiological testing of watercourses around the municipality of Gdańsk in 2009

    Open Research Data
    open access

    The dataset contains the results of a bacteriological and physico-chemical study of watercourses waters within the administrative boundaries of Gdańsk city in 2009. The examined material consisted of water samples collected from 16 watercourses within the administrative boundaries of Gdańsk, Poland.

  • Bacteriological and physicochemical monitoring of inland surface waters within the administrative boundaries of Gdańsk city in 2010

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    The dataset containst the results of a bacteriological and physico-chemical study of inland surface waters within the administrative boundaries of Gdańsk city in 2010.The examined material consisted of water samples collected from four lakes located within the administrative boundaries of Gdańsk, Poland.

  • Bacteriological monitoring of coastal sea waters – Gulf of Gdańsk (Baltic Sea) in 2010

    Open Research Data
    open access

    The dataset contains the results of a bacteriological and physicochemical studies of Gdansk Bay coastal waters within the administrative boundaries of Gdańsk city in 2010. The examined material consisted of water samples collected from 15 sampling points. The aim of this study was to determine the number of Escherichia coli and the number of intestinal...

  • The results of physico – chemical and microbiological testing of watercourses around the municipality of Gdańsk in 2010

    Open Research Data
    open access

    The dataset contains the results of a bacteriological and physico-chemical study of watercourses waters within the administrative boundaries of Gdańsk city in 2010. The examined material consisted of water samples collected from 16 watercourses within the administrative boundaries of Gdańsk, Poland.