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Search results for: chromatografia wykluczania (gpc/sec)
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Multidimensional Gas Chromatography in Essential Oil Analysis. Part 1: Technical Developments
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Comparison of Air-Assisted, Vortex-Assisted and Ultrasound-Assisted Dispersive Liquid–Liquid Microextraction for the Determination of BTEX Compounds in Water Samples Prior to GC-FID Analysis
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Synthesis and characterization of modified silica gel as an intermediate in the generation of gaseous standard mixtures
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Preparation and evaluation of 1,3-alternate 25,27-bis[p-nitrobenzyloxy]-26,28-bis[3-propyloxy]-calix[4]arene-bonded silica gel stationary phase for LC
PublicationPrzeprowadzono syntezę nowej fazy stacjonarnej na bazie sililowej pochodnej 25,27-bis[p-nitrobenzyloksy]-26,28-bis-[3-propyloksy]kaliks[4]arenu zablokowanego w konformacji 1,3-naprzemianległej. Zbadano selektywność i sprawność fazy w stosunku do szeregu klas związków organicznych techniką wysokosprawnej chromatografii cieczowej.
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Application of Headspace Solid-phase Microextraction with Poly(1-vinyl-3- Hexylimidazolium Chloride) Polymeric Ionic Liquid Coating using GC - MS to Determine Volatile Fatty Acids in Dairy Wastewater
PublicationVolatile fatty acids were determined in this study using headspace solid-phase microextraction (HS-SPME) with a poly(1-vinyl-3-hexylimidazolium chloride) polymeric ionic liquid coated fiber followed by gas chromatography - mass spectrometry. Experimental parameters such as extraction time and temperature, sample volume as well as desorption time and temperature were optimized. Detection limits of the method were in the range of...
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Possibilities of Production of New Reference Material ? Preparation of Gaseous Standard Mixtures Using Thermal Decomposition of Immobilized Compounds ? the Effect of Selected Parameters on the Amount of Released Analyte
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Riboflavin binding protein—Chiral stationary phase: Investigation of retention mechanism
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Polyfunctional chemically bonded stationary phase for reversed phase high-performance liquid chromatography
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Paraffin-Embedded Tissue as a Novel Matrix in Metabolomics Study: Optimization of Metabolite Extraction Method
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Comparative study of surface topography of high performance liquid chromatography columns in terms of hydrophobicity
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Enantioselective Extraction System Containing Binary Chiral Selectors and Chromatographic Enantioseparation Method for Determination of the Absolute Configuration of Enantiomers of Cyclopentolate
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Separation of Monovinyl and Divinyl Protochlorophyllides Using C30 Reverse Phase High Performance Liquid Chromatography Column: Analytical and Preparative Applications
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Selected concentration techniques for gas chromatographic analysis of environmental samples
PublicationThe paper describes the role and tasks of environmental analysis and monitoring. It emphasises the leading role played by gas chromatography, especially when coupled with suitable sample preparation. This is demonstrated by some literature evidence and mainly by the author's original work on the design of sample preparation apparatus and development of GC-based methods of determination of a wide variety of organic pollutants in...
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Determination of non-steroidal anti-inflammatory drugs in natural waters using off-line and on-line SPE followed by LC coupled with DAD-MS
PublicationOpisano dwie metody pozwalające na jednoczesne oznaczanie zawartości niesterydowych leków przeciwzapalnych (difluisal, diklofenak, naproksen, tolmetin, fenoprofen, ibuprofen) w próbkach wodnych. Próbki przygotowywano do analizy z użyciem techniki ekstrakcji do fazy stałej (off-line i on-line). Natomiast oznaczeń końcowych dokonano z użyciem LC-DAD-MS. Sprawdzono kilka różnych kolumienek ekstrakcyjnych i wybrano RP-18 jako najlepsze...
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The 12 principles of green analytical chemistry and the SIGNIFICANCE mnemonic of green analytical practices
PublicationThe current rapid development of green analytical chemistry (GAC) requires clear, concise guidelines in the form of GAC principles that will be helpful in greening laboratory practices. The existing principles of green chemistry and green engineering need revision for their use in GAC because they do not fully meet the needs of analytical chemistry. In this article we propose a set of 12 principles consisting of known concepts...
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Bacteriological and physicochemical monitoring of coastal sea waters – Gulf of Gdańsk (Baltic Sea) in 2004
Open Research DataThe dataset contains the results of a bacteriological and physicochemical studies of Gdansk Bay coastal waters within the administrative boundaries of Gdańsk city in 2004. The examined material consisted of water samples collected from 15 sampling points. Number of Escherichia coli, number of intestinal enterococci, presence of Salmonella sp., pH, temperature,...
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Bacteriological and physicochemical monitoring of coastal sea waters – Gulf of Gdańsk (Baltic Sea) in 2006
Open Research DataThe dataset contains the results of a bacteriological and physicochemical studies of Gdansk Bay coastal waters within the administrative boundaries of Gdańsk city in 2006. The examined material consisted of water samples collected from 15 sampling points. Number of Escherichia coli, number of intestinal enterococci, presence of Salmonella sp., pH, temperature,...
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Bacteriological and physicochemical monitoring of coastal sea waters – Gulf of Gdańsk (Baltic Sea) in 2007
Open Research DataThe dataset contains the results of a bacteriological and physicochemical studies of Gdansk Bay coastal waters within the administrative boundaries of Gdańsk city in 2007. The examined material consisted of water samples collected from 15 sampling points. Number of Escherichia coli, number of intestinal enterococci, presence of Salmonella sp., pH, temperature,...
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SEM images of MXene catalysts
Open Research DataData contain results SEM measurements of the Ti3C2Tx MXenes produced via acidic etching aluminum from MAX Phase (Ti3C2-Al-Ti3C2-Al-Ti3C2) using different etching agents, HF/HCl and HF/H2SO4 with different weight ratios (1:3, 1:4, and 1:5). The samples were labeled as MXene HF/HCl X:Y and MXene HF/H2SO4 X:Y, where X:Y means the acids weight ratios. MAX...
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SEM micrographs of NH4VO3 crystals
Open Research DataThe DataSet contains the scanning electron microscopy (SEM) micrographs of NH4VO3 crystals obtained by the LPE-IonEx method. The SEM images clearly show that the morphology of the end product can be nicely tuned by changing the type of ammonium salt and the solvent. It can be concluded that the used solvent affected crystal shapes and their size was...
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SEM inwestigation of the silver nanostructures
Open Research DataSilver thin films with a thickness of 1nm, 3nm, 5nm, 7nm and 9nm were deposited by a table-top magnetron sputtering unit in a pure argon plasma from a high-purity silver target. Silicon wafers was used as a substrates. As-deposired films were annealed in Ar atmosphere at 550 Celsius degree for 15 minutes.As a result of annealing, Ag nanostructures formed...
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Alkali-activated slag (AAS) and OPC-based composites containing crumb rubber aggregate: Physico-mechanical properties, durability and oxidation of rubber upon NaOH treatment
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Global defensive sets in graphs
PublicationIn the paper we study a new problem of finding a minimum global defensive set in a graph which is a generalization of the global alliance problem. For a given graph G and a subset S of a vertex set of G, we define for every subset X of S the predicate SEC ( X ) = true if and only if | N [ X ] ∩ S | ≥ | N [ X ] \ S | holds, where N [ X ] is a closed neighbourhood of X in graph G. A set S is a defensive alliance if and only if for...
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Jerzy Demkowicz dr inż.
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ACM/SPEC International Conference on Performance Engineering
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Agnieszka Pladzyk dr hab. inż.
PeopleAgnieszka Pladzyk, born in 1973 in Pisz, graduated in 1998 in Biotechnology from the Faculty of Chemistry GUT. Her MSc thesis entitled Production of recombinant human calcitonin in bacterial system and its purification with the use of metal affinity chromatography was done under the supervision of professor Józef Kur. In 2003 she defended the PhD with distinctions and her PhD thesis entitled Cobalt tri-tert-butoxysilanethiolates...
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Has EGNOS its own place in maritime navigation?
PublicationGNSS (in fact it usually means GPS) is at the moment the fundamental means of positioning for any variants of navigation. However some attributes of it can be not sufficient for every users or in some tasks, so there are any cases when this system needs support. From the mariner point of view pure GPS properties perfectly fulfils expectations of sailors at the open sea, however there are lot of cases, when accuracy of the system...
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Role of Src Kinases in Neu-Induced Tumorigenesis: Challenging the Paradigm Using Csk Homologous Kinase Transgenic Mice
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Podstawy zarzadzania operacyjnego / pod redakcją Zdzisława Jasińskiego. - Kraków : Oficyna Ekonomiczna, 2005. - Rec.: Ludmiła Zawadzka.
PublicationKsiążka prof. Zdzisława Jasińskiego przedstawia uporządkowanie terminologii i wiedzy, podstawę do realizacji prac dyplomowych i naukowych. Jest również cennym źródłem wiedzy dla praktyków z zakresu zarządzania operacyjnego.
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2013 Practice guidelines for the management of arterial hypertension of the European Society of Hypertension (ESH) and the European Society of Cardiology (ESC)
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Probabilistic Assessment of Correlations of Water Levels in Polish Coastal Lakes with Sea Water Level with the Application of Archimedean Copulas
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Modeling of TEC Variations Based on Signals from Near Zenith GNSS Satellite Observed by Dense Regional Network
PublicationCurrently the substantial successes in high-resolution ionospheric mapping is declared in many publications. Nevertheless, up to now there are no examples of dynamic visualization of TEC disturbances on regional scale with as high resolution as tropospheric models. Over the years, ionosphere has been modeling basing on the simple assumption, that it is a thin layer, which surrounds the Earth at some arbitrary height. However, the...
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Influence of Aggregating Window Size on Disparity Maps Obtained from Equal Baseline Multiple Camera Set (EBMCS)
PublicationThis paper is concerned with obtaining disparity maps on the basis of images from Equal Baseline Multiple Camera Set (EBMCS). EBMCS consists of a central camera and side cameras. Algorithms for obtaining disparity maps with the use of EBMCS take advantage of aggregating windows similarly to stereo matching algorithms for a stereo camera, a camera matrix or a camera array. The paper analyzes the influence of aggregating window size...
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Determination of probabilities defining safety of a sea-going ship during performance of a transportation task in stormy weather conditions
PublicationThe paper presents the possibility of applying the theory of semi-Markov processes to determine the limiting distribution for the process of changes of technical states being reliability states of the systems of sea-going ships significantly affecting safety of such ships, which include main engine, propeller and steering gear. The distribution concerns the probabilities of occurrence of the said states defined for a long time...
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Mobility and bioavailability of mercury in sediments of the southern Baltic sea in relation to the chemical fractions of iron: Spatial and temporal patterns
PublicationMarine sediments play a significant role as reservoirs for mercury (Hg), a bioaccumulative toxic pollutant that poses risks to human and ecosystem health. Iron (Fe) has been recognized as an influential factor in the complexation and bioavailability of Hg in sediments. However, limited studies have investigated the interactions between the chemical fractions of these elements in natural settings. This study aims to examine the...
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Experimental EMI study of a 3-phase 100kW 1200V Dual Active Bridge Converter using SiC MOSFETs
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Empirical Model for Phycocyanin Concentration Estimation as an Indicator of Cyanobacterial Bloom in the Optically Complex Coastal Waters of the Baltic Sea
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Recent trends in prevalence of neoplasia in the Baltic clam Macoma balthica (L.) from the Gulf of Gdańsk (Baltic Sea).
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Habitat-related patterns of soft-bottom macrofaunal assemblages in a brackish, low-diversity system (southern Baltic Sea)
PublicationCoastal areas provide a high variety of sedimentary habitats that influence the structure of resident fauna even on small geographical scales. Therefore, examinations of spatial variations in benthic assemblages require background knowledge of the environmental and biotic heterogeneity of habitats in order to understand ecological processes in such areas. The effect of habitat-related abiotic and biological variables on macrofaunal...
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Phosphate exchange across the sediment-water interface under oxic and hypoxic/anoxic conditions in the southern Baltic Sea
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Benthic fluxes of oxygen and nutrients under the influence of macrobenthic fauna on the periphery of the intermittently hypoxic zone in the Baltic Sea
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Porewater dissolved organic and inorganic carbon in relation to methane occurrence in sediments of the Gdańsk Basin (southern Baltic Sea)
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Mobility and bioavailability of mercury in sediments of the southern Baltic sea in relation to the chemical fractions of iron: Spatial and temporal patterns
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Pore water alkalinity below the permanent halocline in the Gdańsk Deep (Baltic Sea) - Concentration variability and benthic fluxes
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A Comparative Study of Fuzzy SMC with Adaptive Fuzzy PID for Sensorless Speed Control of Six-Phase Induction Motor
PublicationMulti-phase motors have recently replaced three-phase induction motors in a variety of applications due to the numerous benefits they provide, and the absence of speed sensors promotes induction motors with variable speed drives. Sensorless speed control minimizes unnecessary speed encoder cost, reduces maintenance, and improves the motor drive’s reliability. The performance comparison of the fuzzy sliding mode controller (FSMC)...
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A framework for risk assessment for maritime transportation systems—A case study for open sea collisions involving RoPax vessels
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Estimation of Potential Leakage from Dumped Chemical Munitions in the Baltic Sea Based on Two Different Modelling Approaches
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Deep submarine groundwater discharge indicated by pore water chloride anomalies in the Gulf of Gdańsk, southern Baltic Sea
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Emerging Role of Balloon Pulmonary Angioplasty in Chronic Thromboembolic Pulmonary Disease—Insights from the 2022 ESC Guidelines
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Prevalence and Factors Associated With Intertwin Birth Weight Discordance Among Same-Sex Twins in Lombardy, Northern Italy
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