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- Publikacje 1977 wyników po odfiltrowaniu
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Wyniki wyszukiwania dla: BIAŁKO DRAC
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Cold atmospheric plasma-induced chemical vapor generation in trace element analysis by spectrometric methods
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Determination of aminoglycoside antibiotics: Current status and future trends
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Element analysis of bee-collected pollen and bee bread by atomic and mass spectrometry – Methodological development in addition to environmental and nutritional aspects
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Quality problems in determination of organic compounds in environmental samples, such as PAHs and PCBs
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Standard gas mixtures – indispensable reference materials in the analysis of gaseous media
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Gaseous standard mixtures – the challenge of obtaining small amounts of measurands
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Validation of a sampling procedure
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Molecularly imprinted polymers for the detection of volatile biomarkers
PublikacjaIn the field of cancer detection, the development of affordable, quick, and user-friendly sensors capable of detecting various cancer biomarkers, including those for lung cancer (LC), holds utmost significance. Sensors are expected to play a crucial role in the early-stage diagnosis of various diseases. Among the range of options, sensors emerge as particularly appealing for the diagnosis of various diseases, owing to their cost-effectiveness,...
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Natural/bio-based sorbents as greener extractive materials for endocrine disrupting compounds in samples of different matrix composition
PublikacjaEndocrine-disrupting compounds (EDCs) are a group of chemicals that interfere with the endocrine system, leading to adverse effects on human health and the environment. Increasing concerns over the EDCs presence in various environmental compartments has driven the search for greener extraction materials. Recently, the use of polymers of natural origin (biopolymers) has been demonstrated to be an effective and promising research...
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Microextraction by packed sorbent: Uncommon detection techniques, sorbents, samples and analytes
PublikacjaAmong sample preparation approaches, the most desirable are procedures that ensure high efficiency and reproducibility, that are cheap, fast and simple, that minimize the number of operational steps and that require a small amount of sample and solvent and are thus environmentally friendly. Microextraction by packed sorbent (MEPS) is a miniaturized form of solid-phase extraction, the use of which has been continuously expanding...
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Passive sampling
PublikacjaPrzedstawiono możliwości wykorzystania technik pasywnych (opartych na swobodnym ruchu cząsteczek analitu do medium zatrzymującego) w analityce środowiskowej. Omówiono przykłady wykorzystania zarówno organizmów żywych (biomonitoring) jak i urządzeń pasywnych do pobierania próbek analitów z badanego medium (powietrze, woda, gleba).
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Novel sorptive extraction techniques in bioanalysis evaluated by Blue Applicability Grade Index: The paradigm of fabric phase sorptive extraction and capsule phase microextraction
PublikacjaFabric phase sorptive extraction (FPSE) and capsule phase microextraction (CPME) are two sol-gel derived microextraction techniques that emerged in the last decade towards the minimization of the environmental impact of conventional sample preparation approaches. Complementary to the well-established green metric tools, Blue Applicability Grade Index (BAGI) was recently proposed for the evaluation of method’s practicability. In...
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Polymeric porous membranes as solid support and protective material in microextraction processes: A review
PublikacjaPolymeric porous membranes have proven to be a versatile and efficient material for microextraction processes. In analytical practice, they are used both as a solid support and as a protective medium for improved sample preparation in various analytical applications. Polymeric porous membranes offer unique advantages in microextraction due to their large surface area and controllable pore size, eliminating interfering effects from...
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Sorbents modified by deep eutectic solvents in microextraction techniques
PublikacjaIn recent years, considerable attention has been directed towards the employment of green solvents, specifically deep eutectic solvents (DES), in liquid phase microextraction techniques. However, comprehensive and organized knowledge regarding the modification of sorbent surface structures with DES remains limited. Therefore, this paper reviews the application of DES in modifying and improving the properties of sorbents for microextraction...
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Analytical progress on emerging pollutants in the environment: An overview of the topics
PublikacjaThis overview discusses the ideas behind a collection of articles by invited authors on a diverse range of complex chemical mixtures and analytical methods which represent some of the most relevant and interesting issues on emerging contaminants of environmental health concerns. These chemicals, including those in high volume production, are released on an ongoing basis as a result of various human activities. Moreover, these emerging contaminants...
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Molecularly imprinted polymers based on deep eutectic solvents as a greenest materials for selective extraction of emerging contaminants from complex samples
PublikacjaSome of the reagents applied in the synthesis of molecularly imprinted polymers (MIPs) may impact on health and the environment. Thus, a new generation of promising green chemicals are nowadays introduced and investigated, including deep eutectic solvents (DESs). DESs seems to be a reasonable choice as they are characterized as non-toxic, low cost, easy to prepare and biodegradable chemicals. This review presents the information...
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Lab-in-syringe as a practical technique for automatic microextraction: Evaluation by Blue Applicability Grade Index
PublikacjaLab-in-syringe (LIS) is a powerful automatic technique that is derived from sequential injection analysis. In LIS, a computer-controlled syringe pump is employed, and its syringe barrel serves as a mixing, reaction, and/or extraction chamber. Until now, the LIS concept has been efficiently employed for the automation of solid-phase microextraction and liquid-phase microextraction protocols as a front-end to a plethora of chromatographic...
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Investigation of stability of aqueous solutions containing trace amounts of volatile organic analytes
PublikacjaOznaczając lotne związki chlorowcoorganiczne w matrycy wodnej należy uwzględnić specyficzne właściwości, którymi charakteryzują się te związki, a mianowicie:- niska temperatura wrzenia; - wysoka prężność pary nad roztworem; - stosunkowo niska rozpuszczalność w wodzie.Właściwości te należy uwzględnić w trakcie przygotowania wodnych roztworów wzorcowych wykorzystywanych na etapie kalibracji i badań modelowych. Ze względu na istotność...
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Miniaturized solid phase extraction techniques for different kind of pollutants analysis: State of the art and future perspectives – PART 2
PublikacjaDetermination of pollutants present in environmental samples at a low concentration level very often requires the analytical protocol that includes analytes isolation and/or enrichment prior to the final quantification. Miniaturized SPE offers an interesting alternative to LLE. Nowadays, many types of sorbents are available and can be used as selective materials for extraction of varied analytes in different kinds of samples. The...
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Miniaturized Solid Phase Extraction techniques for different kind of pollutants analysis: State of the art and future perspectives – PART 1
PublikacjaSolid Phase Extraction (SPE) has been practiced in a modern form for more than half a century. It was constantly developing, driven by the analysts needs. These needs are coming from the importance to select an appropriate analytical method, which should have satisfactory accuracy, precision and sensitivity. In the case of sorbent-based microextraction techniques, the choice of miniaturized variants that meet these requirements...
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Applications of metal organic framework adsorbents for pipette-tip micro solid-phase extraction
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Analytical studies on the environmental state of the Svalbard Archipelago provide a critical source of information about anthropogenic global impact
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Recent breakthroughs in the stability testing of pharmaceutical compounds
PublikacjaPharmaceutical development is mostly focused on the research leading to approval of a new and viable active substance. However, there is a number of old generation compounds that are still being used in contemporary medicinal practice. So that new analytical developments should cover not only the safety of newly developed drug substances, which is obvious, but should also be directed into the search of individual stability issues...
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Complementarity of electronic and vibrational circular dichroism based on stereochemical studies of vic-diols
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Analytical procedures for determination of cocaine and its metabolites in biological samples
PublikacjaThe dangerous effects and increased usage of illicit drugs have inspired the development of analytical methodologies. We based our review of analytical procedures for determination of cocaine (COC) and its metabolites on literature from the past two decades. Our main aim was to compare the capabilities of different analytical techniques. The diversity of matrices from which COC is determined (e.g., blood, hair, saliva, plasma,...
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Standard gas mixtures- indispensable reference materials in the analysis of gaseous media
PublikacjaIn recent years the need for the quality control and assurance of analytical measurement results has been particularly strongly emphasised. Certified reference materials play an invaluable role in this process. The article characterises the basic types of reference materials, focusing in particular on those in the gaseous state. It also reviews the literature on the techniques of preparing standard gas mixtures over the last ten...
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Monitoring of volatile organic compounds (VOCs) in atmospheric air. Part I. On-line gas analyzers
PublikacjaThe paper reviews the subject literature concerning the analytical instruments routinely used for monitoring volatile organic compounds in atmospheric air. The analyzers are classified as stationary or mobile according to their ease of transport. Stationary DOAS (Differential Optical Absorption Spectroscopy) analyzer is characterized, as are MIMS (Membrane Introduction Mass Spectrometry), MESI (Membrane Extraction with Sorbent...
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Isotope-labeled substances in analysis of persistent organicpollutants in environmental samples
PublikacjaUltratrace analysis of persistent organic pollutants (POPs) in environmental samples requires very sophisticated methods for both sample preparation and instrumental analysis. The complex matrix requires a multi-stage procedure. Each stage is a potential source of error, as a consequence of which the final result of analysis could be a source of misinformation rather than information. The individual stages and the procedure as...
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Determination of organophosphorus and organonitrogen pesticides in water samples
PublikacjaPesticides are among the most dangerous environmental pollutants because of their stability, mobility and long-term effects on living organisms. Their presence in sources of drinking water, essential to life, is a particular danger. In water, these compounds can undergo transformations, leading to the production of substances of even greater toxicity. Legal regulations are in force, stipulating the highest permissible level of...
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Quality problems in the determination of organic compounds in environmental samples, such as PAHs and PCBs
PublikacjaPrzedstawiono i skomentowano wyniki badań międzylaboratoryjnych w zakresie oznaczania wybranych związków organicznych w próbkach środowiskowych. Oznaczenia wykonane były przez niezależne laboratoria analityczne, które stosowały różne procedury przygotowania próbek do analizy.Badania wskazują, że wynik oznaczania poszczególnych analitów zależny był od stosowanej przez laboratorium procedury izolacji i oznaczania. Stwierdzono różnice...
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Monitoring of volatile organic compounds (VOCs) in atmospheric air. Part II. Sample collection and preparation
PublikacjaThe paper reviews literature information on air sampling techniques commonly used for monitoring volatile organic compounds (VOCs) levels in atmospheric air. It describes containers for collecting samples of atmospheric air, such as vacuum canisters and bags made from synthetic materials. It discusses dynamic, passive and denudational techniques for sampling analytes from air combining isolation with preliminary enrichment, and...
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Review of the determination of pesticide residues in ambient air
PublikacjaW publikacji dokonano przeglądu najważniejszych metodyk oznaczania pozostałości pestycydów w powietrzu zewnętrznym. W publikacji przedstawiono także techniki używane do oznaczeń końcowych. Obecnie najpopularniejszą techniką oznaczeń końcowych jest chromatografia gazowa bądź cieczowa sprzężona ze spektrometrem mas.
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Evolution of models for sorption of PAHs and PCBs on geosorbents.
PublikacjaWiedza o tym gdzie są zlokalizowane zanieczyszczenia obecne w osadzie oraz z jaką siłą związane są one z osadem jest niezbędna do oszacowania stopnia i skuteczności procesów remediacjyjnych oraz określenia dostępności, mobilności i toksyczności osadów. Dlatego, aby zrozumieć i poznać procesy zachodzące w tak skomplikowanej matrycy, jaką stanowią osady denne/gleby konstruowane są teoretyczne modele matematyczne opisujące prawdopodobny...
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Analytical methodologies for determination of artificial sweeteners in foodstuffs- a review
PublikacjaArtificial high-intensity sweeteners are more and more frequently used for food production. Food industry tends to highlight beneficial aspects of their use, such as tooth-friendliness, rising-up quality of life of those suffering from different forms of diabetes and possibility of weight control without sacrificing favorite unhealthy drinks or snacks. On the other hand some of the consumers are deeply concerned about safety of...
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Green analytical chemistry in sample preparation for determination of trace organic pollutants
PublikacjaW pracy przedstawiono przyjazne środowisku techniki analityczne, stosowane w celu izolacji i wzbogacania analitów. Ilość używanych rozpuszczalników jest ograniczana przez stosowanie alternatwnych rozpuszczalników, technik bezrozpuszczalnikowych, ekstrakcji wspomaganych czynnikami zewnętrznymi oraz przez wprowadzanie mikrosystemów analitycznych.
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Challenges in preparing honey samples for chromatographic determination of contaminants and trace residues
PublikacjaThe determination of contaminations and residues in honey is of growing concern over past few years, especially that these compounds can not only diminish beneficial properties of honey but more importantly, if present in significant amounts, can pose serious threat to human health. Since honey is characterized by complex composition of the matrix sample, it is often necessary to apply clean-up step, in order to eliminate interfering...
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Application of ecotoxicological studies in integrated environmental monitoring: possibilities and problems
PublikacjaPodstawowym celem badań stanu środowiska i procesów w nim zachodzących jest oszacowanie wpływu różnego typu zanieczyszczeń na organizmy żywe, w tym także na organizm człowieka. Jeszcze do niedawna do oceny ryzyka środowiskowego wykorzystywano wyniki uzyskane w trakcie badań analitycznych z wykorzystaniem typowych metod chemicznych i fizykochemicznych. Niestety, miały one charakter badań rutynowych i ograniczały się do oznaczania...
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Sediment-quality assessment by intelligent data analysis
PublikacjaCoraz powszechniej do oceny jakości próbek środowiskowych osadów wykorzystuje się analizy chemometryczne. Ich głównym zadaniem jest znalezienie zależności pomiędzy wynikami analiz chemicznych oraz oszacowanymi parametrami toksyczności.Zastosowanie chemometrii w ocenie jakości próbek środowiskowych umożliwiłoby zredukowanie kosztów biomonitoringu prowadzonego na badanym obszarze poprzez optymalizację procedury badawczej.
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Investigation of matrix-free generation of methyl chloride as a reference material
PublikacjaW pracy opisano badania nad wykorzystaniem włókien szklanych do otrzymywania bezmatrycowych materiałów odniesienia zawierających chlorek metylu. Chlorek metylu jest uzyskiwany w wyniku termicznego rozkładu związku powierzchniowego. Przedstawiono wyniki badań dla trzech różnych włókien szklanych (o różnej grubości), pokrytych warstwą glinu.
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Analytical techniques in studies of the environmental fate of pharmaceuticals and personal-care products
PublikacjaW pracy przedstawiono dane literaturowe odnośnie źródeł emisji, dróg transportu, przemian i metabolizmu, pomiomu stężeń ksenobiotyków z grupy farmaceutyków i środków higieny osobistej w próbkach pobranych z różnych elementów środowiska (woda, gleba, osady denne) oraz próbek bioty. Szczególną uwagę zwrócono na techniki analityczne wykorzystywane w badaniach losu środowiskowego w/w zanieczyszczeń.
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Trends in biomedical analysis of red blood cells – Raman spectroscopy against other spectroscopic, microscopic and classical techniques
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Gradient reversed-phase high-performance chromatography of ionogenic analytes
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Critical approach to PLE technique application in the analysis of secondary metabolites in plants
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New insights into the application of MSPD in various fields of analytical chemistry
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Perspectives and challenges in extracellular vesicles untargeted metabolomics analysis
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Properties and determination of pesticides in fruits and vegetables
PublikacjaThe intensive development of agriculture means that more and more toxic organic and inorganic compounds are entering theenvironment. Because of their widespread use, stability, selective toxicity and bioaccumulation, pesticides are among the mosttoxic substances contaminating the environment. They are particularly dangerous in fruit and vegetables, by which people areexposed to them. It is therefore crucial to monitor pesticide...
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Determination of antibiotic residues in honey
PublikacjaHoney produced by honeybees is a valuable food product. The presence of xenobiotics in honey may harm its quality and constitute a danger to human health. Antibiotics are commonly applied by beekeepers to eliminate disease among honeybees. Moreover, ubiquitous administration of antibiotics may cause bacteria to become resistant to many drugs and spread antibioticresistant strains of bacteria. Appropriate sample preparation and...
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Common methods for the chiral determination of amphetamine and related compounds I. Gas, liquid and thin-layer chromatography
PublikacjaThis article reviews the most common, useful methods for the chiral determination of amphetamine (AM) and AM-deriveddesigner drugs in different of matrix, including blood, hair, urine, medicaments or standard solutions, taking into considerationarticles published in the past 15 years. We consider chromatographic methods (e.g., gas, liquid, high-performance liquid, and thinlayer). We describe several types of chiral derivatization...
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Pharmaceutical and forensic drug applications of chiral supercritical fluid chromatography
PublikacjaTHE SUPERCRITICAL FLUID IS AN EXCELLENT CHOICE AS THE CHROMATOGRAPHIC MOBILE PHASE BECAUSE IT ALLOWS RAPID SEPARATION WITH HIGH EFFICIENCY AND APPLICATIONS INVOLVING ENANTIORESOLUTION ARE COMMON. SUPERCRITICAL FLUID CHROMATOGRAPHY (SFC) IS INCREASINGLY USED FOR ANALYTICAL, SEMI-PREPARATIVE AND PREPARATIVE PURIFICATION OF CHIRAL COMPOUNDS, INCLUDING PRODUCTION OF ENANTIOMERS THAT ARE MAINLY ENCOUNTERED DURING DRUG DEVELOPMENT. SFC...
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Application of magnetic nanoparticles for magnetic solid-phase extraction in preparing biological, environmental and food samples
PublikacjaThe need to obtain meaningful results as the basis for determining the content of trace amounts of analytes has become the driving force behind the development of modern analytical techniques, including sample-preparation techniques, such as solid-phase extraction (SPE). Recently, great interest was aroused in the use of magnetic nanoparticles (MNPs) in SPE. These materials exhibit high selectivity, and, in small amounts, can provide...