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- Publikacje 1358 wyników po odfiltrowaniu
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- Kursy Online 252 wyników po odfiltrowaniu
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- Dane Badawcze 271 wyników po odfiltrowaniu
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Wyniki wyszukiwania dla: in-tube extraction
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Sorbents modified by deep eutectic solvents in microextraction techniques
PublikacjaIn recent years, considerable attention has been directed towards the employment of green solvents, specifically deep eutectic solvents (DES), in liquid phase microextraction techniques. However, comprehensive and organized knowledge regarding the modification of sorbent surface structures with DES remains limited. Therefore, this paper reviews the application of DES in modifying and improving the properties of sorbents for microextraction...
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Multivariate Assessment of Procedures for Molecularly Imprinted Polymer Synthesis for Pesticides Determination in Environmental and Agricultural Samples
PublikacjaIn the case of quantitative and qualitative analysis of pesticides in environmental and food samples, it is required to perform a sample pre-treatment process. It allows to minimalize the impact of interferences on the final results, as well as increase the recovery rate. Nowadays, apart from routinely employed sample preparation techniques such as solid-phase extraction (SPE) or solid-phase microextraction (SPME), the application...
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Investigation of vortex assisted magnetic deep eutectic solvent based dispersive liquid–liquid microextraction for separation and determination of vanadium from water and food matrices: Multivariate analysis
PublikacjaA new and simple vortex assisted magnetic deep eutectic solvent dispersive liquid–liquid microextraction procedure (VA-MDES-DLLME) was developed for the determination of vanadium (V) in food and water samples by flame atomic absorption spectrometry (FAAS). In the extraction medium, a bis(acetylpivalylmethane) ethylenediimine (H2APM2en) was used for the complexation of V(V) in sample solution at pH 6. The VA-MDES-DLLME was optimized...
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Spatial development in the EU in the global context
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Physics of Strongly-coupled Dopant-atoms in Nanodevices
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Comparison of Methods for Real and Imaginary Motion Classification from EEG Signals
PublikacjaA method for feature extraction and results of classification of EEG signals obtained from performed and imagined motion are presented. A set of 615 features was obtained to serve for the recognition of type and laterality of motion using 8 different classifications approaches. A comparison of achieved classifiers accuracy is presented in the paper, and then conclusions and discussion are provided. Among applied algorithms the...
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Thermal Imaging in Wound Healing Diagnostics
PublikacjaResults of a project searching for objective, quantitative evaluation of postoperative wound healing in cardiosurgery are presented. We propose simple thermal models of the healing processes after cardiosurgery interventions as objective descriptors allowing classification of patients for extraction and following recovery at home or for prolonged treatment in a hospital. Classification of healing as the normal process or as a process...
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Oxidation step in the preparation of benzocamalexin: The crystallographic evidence
PublikacjaThe study of oxidation step in the preparation of benzocamalexin by the α-amidoalkylation–oxidation sequence revealed the formation of perchloro-1,2-phenylene dibenzoate as the product of transformation of tetrachloro- 1,2-benzoquinone applied as the oxidant. The structures of benzocamalexin and perchloro-1,2-phenylene dibenzoate were confirmed by X-ray diffraction analysis. The extraction step in the final isolation of benzocamalexin...
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Mucinous carcinoma - Female, 73 - Tissue image [3160630007336501]
Dane BadawczeThis is the histopathological image of BREAST tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Mucinous carcinoma - Female, 73 - Tissue image [3160630007334621]
Dane BadawczeThis is the histopathological image of BREAST tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Mucinous carcinoma - Female, 73 - Tissue image [3160630007334121]
Dane BadawczeThis is the histopathological image of BREAST tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Mucinous carcinoma - Female, 73 - Tissue image [3160630007332211]
Dane BadawczeThis is the histopathological image of BREAST tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Mucinous carcinoma - Female, 73 - Tissue image [3160630007337261]
Dane BadawczeThis is the histopathological image of BREAST tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Geometrically nonlinear analysis of shells - Benchmark problems for Autocad Robot Analysis Professional
PublikacjaThe aim of this work is to verify the suitability of commercial engineering software for geometrically nonlinear analysis of shells. This paper deals with the static, geometrically nonlinear analysis of shells made of an isotropic material. The Finite Element Method (FEM) is chosen to solve the problem. The results of the commercial software Autocad Robot Structural Analysis Professional (ARSAP) are compared with the litera-ture...
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OVARY, Ovary - Female, 62 - Tissue image [3220630024678001]
Dane BadawczeThis is the histopathological image of OVARY tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Chemical diffusion coefficient of oxygen (D*) of the SrxTi0.30Fe0.70O3 (x=0.90, 0.95 and 1.00) at different temperatures
Dane BadawczeIn this dataset are presented D* values designated based on the electrical conductivity relaxation (ECR) mesurement of the SrxTi0.30Fe0.70O3 (x=0.90, 0.95, 1.00) materials. The applied temperatures were 800 °C, 750 °C, 700 °C, 650 °C, and 600 °C. Studies were performed in a small tube furnace (internal diameter ~20 mm) with 64 cm3 gas volume. During...
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Chemical oxygen surface exchange coefficient (k*) of the SrxTi0.30Fe0.70O3 (x=0.90, 0.95 and 1.00) at different temperatures
Dane BadawczeIn this dataset are presented k* values designated based on the analysis of the electrical conductivity relaxation (ECR) mesurement of the SrxTi0.30Fe0.70O3 (x=0.90, 0.95, 1.00) materials. The applied temperatures were 800 °C, 750 °C, 700 °C, 650 °C, and 600 °C. Studies were performed in a small tube furnace (internal diameter ~20 mm) with 64 cm3 gas...
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Determination of volatile organic compounds in water samples using membrane-solid phase microextraction (M-SPME) (headspace version)
PublikacjaThe results of a study on the use of membrane-solid phase microextraction (M-SPME) for sampling volatile organic compounds (VOCs) from the headspace above the liquid medium are presented. The sampled VOCs were subsequently quantified by gas chromatography (GC). Two systems were compared in this study, i.e. a novel two-phase sorption system (M-SPME), and a commercial fibre. Headspace sampling using SPME was optimized with respect...
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Preconcentration and Analytical Methods for Determination of Methyl Tert-Butyl Ether and Other Fuel Oxygenates and Their Degradation Products in Environment: A Review
PublikacjaFuel oxygenates (FOs) are mainly ethers or alcohols which are added to gasoline either to boost the octane number or to make the fuel burning process more "cleaner" with increasing the oxygen content, or to obtain a combination of both effects. FOs are water soluble with high mobility in the environment which presence even at very low concentrations lower the quality of water making it unsafe or unpleasant due to their objectionable...
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Enhancing voice biometric security: Evaluating neural network and human capabilities in detecting cloned voices
PublikacjaThis study assesses speaker verification efficacy in detecting cloned voices, particularly in safety-critical applications such as healthcare documentation and banking biometrics. It compares deeply trained neural networks like the DeepSpeaker with human listeners in recognizing these cloned voices, underlining the severe implications of voice cloning in these sectors. Cloned voices in healthcare could endanger patient safety by...
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EFFECT OF NANOFLUID CONCENTRATION ON TWO-PHASE THERMOSYPHON HEAT EXCHANGER PERFORMANCE
PublikacjaAn approach – relaying on application of nanofluid as a working fluid, to improve performance of the two-phase thermosyphon heat exchanger (TPTHEx) has been proposed. The prototype heat exchanger consists of two horizontal cylindrical vessels connected by two risers and a downcomer. Tube bundles placed in the lower and upper cylinders work as an evaporator and a condenser, respectively. Distilled water and nanofluid water-Al2O3...
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Free Convection Heat Transfer from Horizontal Cylinders
PublikacjaThe results of experimental investigation of free convection heat transfer in a rectangular container are presented. The ability of the commonly accepted correlation equations to reproduce present experimental data was tested as well. It was assumed that the examined geometry fulfils the requirement of no-interaction between heated cylinder and bounded surfaces. In order to check this assumption recently published correlation equations...
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Manufacturing of Lightweight Aggregates as an Auspicious Method of Sewage Sludge Utilization
Publikacja: Sewage sludge is a high-volume and low-cost waste commonly generated worldwide, so its utilization is a vital issue. The application of this waste in the manufacturing of lightweight aggregates was investigated. The process was performed using intensive mixers with volumes of 5 and 30 L, as well as the industrial 500 L mixer. Then, granulates were sintered in a tube furnace. The influence of composition and mixer size on the...
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The interaction of the pulsed laser irradiation with titania nanotubes - Theoretical studies on the thermal effect
PublikacjaThis paper reports temperature dispersion simulations of titania nanotubes irradiated by the 355 nm, pulsed, nanosecond laser. The modelling with the use of Finite Elements Method concerns titania nanotubes of the length and the wall thickness in the range of 0.5–2 μm and 5–20 nm, respectively. The uniqueness of the morphology was preserved by ensuring the wall thickness variation along the height of the tube, which was determined...
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GIS Solution for Weather Forecast Data Analysis
PublikacjaIn this paper authors present the GIS system for the analysis of the numerical weather prediction data. This kind of data has multidimensional character (three dimensions and time) and its analysis should consider all the available factors. Proposed GIS system consists of RASDAMAN application with implemented OLAP cube mechanism, which enables the user to process data in the spatial-time domain. It also simplifies the meteorological...
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Spatial development in EU in a global context (2022/2023).
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Determination of flavanols by liquid chromatography with fluorescence detection. Application to the characterization of cranberry-based pharmaceuticals through profiling and fingerprinting approaches
PublikacjaIn this work, a new method based on reversed-phase high-performance liquid chromatography (HPLC) with fluorescence detection (FLD) was established for the determination of catechins and related oligomeric proanthocyanidins (PACs) in cranberry-based pharmaceuticals. Compounds were recovered by liquid extraction using methanol/water/hydrochloric acid (60:39:1, v:v:v) as the extraction solvent. The chromatographic separation was carried...
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Semantic URL Analytics to Support Efficient Annotation of Large Scale Web Archives
PublikacjaLong-term Web archives comprise Web documents gathered over longer time periods and can easily reach hundreds of terabytes in size. Semantic annotations such as named entities can facilitate intelligent access to the Web archive data. However, the annotation of the entire archive content on this scale is often infeasible. The most efficient way to access the documents within Web archives is provided through their URLs, which are...
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Investigation of tetrabutylammonium bromide-glycerol-based deep eutectic solvents and their mixtures with water by spectroscopic techniques
PublikacjaDeep eutectic solvents (DES) are formed by an acceptor and a donor of hydrogen bonds. They are generally considered as a possible alternative to hazardous organic solvents in various fields. Very recently they have also appeared in analytical chemistry, used mainly for the separation of analytes before instrumental quantification. For the development of new extraction procedures, it is important, among other things, to understand...
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Influence of Storage Time and Temperature on the Toxicity, Endocrine Potential, and Migration of Epoxy Resin Precursors in Extracts of Food Packaging Materials
PublikacjaThe aim of the present study was to establish a standard methodology for the extraction of epoxy resin precursors from several types of food packages (cans, multi-layered composite material, and cups) with selected simulation media (distilled water, 5% ethanol, 3% dimethyl sulfoxide, 5% acetic acid, artificial saliva) at different extraction times and temperatures (factors). Biological analyses were conducted to determine the acute...
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Magnetic hydrophobic deep eutectic solvents for orbital shaker-assisted dispersive liquid-liquid microextraction (MAGDES-OS-DLLME) - determination of nickel and copper in food and water samples by FAAS
PublikacjaIn this work, a cheap and widely applicable dispersive liquid-liquid microextraction (DLLME) method was developed for the extraction of Ni(II) and Cu(II) from water and food samples and analysis using flame atomic absorption spectrometry. DLLME was assisted by orbital shaker, while ferrofluid as an extractant was based on deep eutectic solvent (DES). This ferrofluid was made of hydrophobic DES (hDES), composed of lauric acid and...
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Developments in ultrasound-assisted microextraction techniques for isolation and preconcentration of organic analytes from aqueous samples
PublikacjaThe great potential of ultrasonic assistance in sample preparation, especially extraction, is being recognized. In this review, we discuss the applications of ultrasonic radiation in assisting microextraction. Topics covered include ultrasound-assisted emulsification microextraction, ultrasound-assisted-emulsification-dispersive liquid-liquid microextraction, and ultrasound-assisted hollow-fiber liquid-phase microextraction with...
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Modeling in Machine Design
Kursy OnlineThe course is meant to show the students how to build calculation models in machine design
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Internet Technologies in Infosystems
Kursy OnlineThe aim of the course "Internet technologies in infosystems" is to familiarize students with issues related to the use of Internet technologies in the implementation of infosystems, including languages and web development tools, as well as application and transmission protocols.
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Management in modern organizations_2022_2023
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Image Processing in Robotics
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CAE in design calculations
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ICT in Management 2020
Kursy OnlineICT in Management for Bachelor in Management students
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Management in modern organizations_2024_2025
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Contemporary Theories in Architecture
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CAE in Design Calculations
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Advances in Human Genetics
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Conthemporary Theories in Architecture
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Mathematical methods in engineering
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Microscopy methods in nanotechnology
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Management in modern organizations_2023_24
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LAW IN INVESTMENT PROCESS
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Laboratory in organic chemistry
Kursy OnlineSupport for the laboratory in organic chemistry.
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Microscopy methods in nanotechnology
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Models in Spatial Development
Kursy Online