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Search results for: HYDROXYL%20RADICALS
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TG-hydroxyl groups in TiO2-P25
Open Research DataTG analyses were performed for powdered TiO2 - commercial P25 sample, which was heat-treated from room temperature to 500 C in the nitrogen atmosphere. Mass loss at lower temperature such as 120 C was related to the physisorbed water, and that one occurring at 500 C to the chemisorbed hydroxyl groups.
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TiO2-TG analyses -OH groups
Open Research DataTG analyses of TiO2 were performed under nitrogen flow to monitor desorption of hydroxyl groups. Physisorbed weak-bonded hydroxyl groups were desorbed totally at around 120oC, whereas chemisorbed ones at around 500oC. The mass loss at these temperatures was used as concentration of hydroxyl groups on TiO2 surface. The amount of analysed TiO2 was 10...
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The influence of chitosan hydrogel coating on different redox probes kinetics
Open Research DataThis dataset contains cyclic voltammetry studies of three redox probes: 1 mM K3[Fe(CN)6], [K4Fe(CN)6], C12H14FeO2, and [Ru(NH3)6]Cl2 dissolved in 0.1 M KCl or PBS as the primary electrolyte. The studies are made for glassy carbon electrode (GC) and glassy carbon electrode covered with thin chitosan hydrogel membrane (C2A2). Cyclic voltammograms were...
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The viscometric evaluation of the gelation rate the chitosan-metal oxide hydrogel systems.
Open Research DataThe dataset shows the change in the viscosity of a hydrogel medium over time. Viscometric measurement was used as a universal method for determining the cross-linking rate of chitosan hydrogel using metal oxides or other solutions with a negative net charge. The method was prepared as a method of predicting the kinetics of additive manufacturing using...
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The influence of chitosan hydrogel cross-linking by agarose on coating physico-chemical properties
Open Research DataThis dataset contains various physicochemical analyses showing the effect of different concentration of chitosan and the cross-linking agent agarose. Each sample is labeled by C and A representing chitosan and agarose concentrations, respectively, while the exact amounts are depicted in the attached table. Fourier-transform infrared (FT-IR) spectroscopy...
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Determination of changes in viscosity of hydrogel depending on shear rate (1.1 to 55 s-1).
Open Research DataThe rheological characteristics of hydrogel were made on the basis of a viscosity measurement using a Brookfield viscometer, using LV SC4 - 25 spindle and shear rates from 1.1 to 55 s-1.
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Determination of changes in viscosity of hydrogel depending on shear rate (1.7 to 34 s-1).
Open Research DataThe rheological characteristics of hydrogel were made on the basis of a viscosity measurement using a Brookfield viscometer, using LV SC4 - 27 spindle and shear rates from 1.7 to 34 s-1.
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Determination of changes in viscosity of hydrogel depending on shear rate (6.6 to 330 s-1).
Open Research DataThe rheological characteristics of hydrogel were made on the basis of a viscosity measurement using a Brookfield viscometer, using LV SC4 - 18 spindle and shear rates from 6.6 to 330 s-1.
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Data on hydrogen migration in cation-induced dissociation of furan molecules
Open Research DataThe data include furan luminescence spectra obtained in collisions with H3+ and C+ cations and theoretical spectra of OH and CH radicals published in [1].
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Valorisation of bioplastics synthesised by liquefaction of celluloseusing hetero- and homogeneous catalysts
Open Research DataThe purpose of the present study was to test the effectiveness of a heterogeneous catalyst such as Nafion ion-exchange resin on the cellulose liquefaction process. The results obtained were compared with the bio-polyols obtained in a conventional way, using a homogeneous catalyst (sulfuric acid (VI)). Depending on the catalyst used and the temperature...
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Photocatalytic degradation of acetaldehyde in high temperature reaction chamber
Open Research DataThis dataset contains chromatograms recorded during the decomposition of acetaldehyde in a high-temperature reaction chamber under UV irradiation using TiO2 (titanium dioxide) as photocatalysts. It includes data on the influence of flow rate, TiO2 (titanium dioxide) filling the entire reactor, a thin layer of TiO2 (titanium dioxide) supported on KBr...
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Bio based PUR-PIR foams thermal degradation (TG) and isoconversional kinetics
Open Research DataIn the present work, we perform a thorough thermogravimetric (TG) analysis of the bio-based polyurethane – polyisocyanurate (PUR-PIR) foams in both nitrogen and oxygen atmosphere. A sustainable element of the foam was a biopolyol obtained via acid-catalyzed liquefaction of Zostera Marina and Enteromorpha Algae biomass. Based on isoconversional analysis...
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Determination of changes in viscosity of pectin gel depending on shear rate (1.1 to 55 s-1).
Open Research DataThe rheological characteristic of pectin gel (with concetration 0,45% m/m, in three independent repetition of sample) was made on the basis of a viscosity measurement using a Brookfield viscometer, using LV SC4 - 25 spindle and shear rates from 1.1 to 55 s-1.The data allowed to characterize the used hydrogel preparations and assess their functional...
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The effect of changes in the concentration of hydroxypropylcellulose on the rheological stability of pectin hydrogels.
Open Research DataThe rheological characteristics of the pectin hydrogel modified by hydroxypropylcellulose (added in a concetration range from 0.1 to 0.55% m/m) were made on the basis of the viscosity assessment using a Brookfield viscometer with an LV SC4 - 25 spindle and a shear rate of 0,22 s-1 in the temperature range 19-96 ° C.The data allowed selection of optimal...
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Determination of changes in viscosity of pectin gel depending on shear rate (1.7 to 85 s-1).
Open Research DataThe rheological characteristic of pectin gel (with concetration 0,25% m/m, in two independent repetitions) wasmade on the basis of a viscosity measurement using a Brookfield viscometer, using LV SC4 - 27 spindle and shear rates from 1.7 to 85 s-1, in temperature of 25 C degee .The data allowed to characterize the used hydrogel preparations and assess...
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FTIR spectra and IGC chromatograms for chemically reduced graphene oxide aerogels (rGOA)
Open Research DataThe effect of selected synthesis parameters on reduced graphene oxide aerogels properties was investigated using Fourier-transform infrared spectroscopy and dynamic adsorption method (Inverse Gas Chromatography, IGC). Samples were synthesized by sol-gel method by reduction induced self-assembly of graphene oxide. As a reductant l-ascorbic acid was used....