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Search results for: NITROGEN-DOPED CARBON SPHERES
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X-ray diffraction spectra of nitrogen-doped carbon in hybrid materials containing praseodymium oxide
Open Research DataX-ray powder diffraction patterns of samples were carried out by Philips X’Pert diffractometer, which was radiated by graphite monochromatized Cu Kα (l equal 1.540598). The operating voltage was maintained at 40 kV, the current was maintained at 30 mA and analyzed in the range from 20° to 90°. The data presented confirmed the presence of the PrBSCF...
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Electrical and noise responses of carbon nanotube networks enhanced by UV light for nitrogen dioxide sensing
Open Research DataNetworks consisting of randomly oriented carbon nanotubes (CNN) were investigated toward nitrogen dioxide detection by means of electrical and low-frequency noise measurements. UV-activation of CNN layers improved gas sensitivity and reduced the limit of detection, especially by employing 275 nm-LED. This data set includes DC resistance measurements...
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Nitrogen (N2) adsorption/desorption isotherms of PC-X (porous carbon materials obtained at various temperatures)
Open Research DataThese data contain nitrogen (N2) adsorption/desorption isotherms of PC-700 (porous carbon obtained at 700 °C), PC-800 (porous carbon obtained at 800°C), PC-900 (porous carbon materials obtained at 900°C). Data showed typical type-I isotherms, indicating the presence of micropores in their structures. PC-900, compared with PC-700 and PC-800, showed a...
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Scanning electron microscopy (SEM) images of the boron-doped carbon nanowalls surfaces
Open Research DataThe dataset contains the scanning electron micrographs (SEM), revealing the surface morphology of boron-doped carbon nanowalls electrodes on silicon substrates. The surface is characterized by nano-walled structures. The obtained electrodes were doped with boron at the level of [B]/[C] = 5000ppm in the gas atmosphere during the synthesis.
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Scanning electron microscopy (SEM) images of the boron-doped carbon nanowalls surfaces
Open Research DataThe dataset contains the scanning electron micrographs (SEM), revealing the surface morphology of boron-doped carbon nanowalls electrodes on silicon substrates. The surface is characterized by nano-walled structures. The obtained electrodes were doped with boron at the level of [B]/[C] = 2000ppm in the gas atmosphere during the synthesis.
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SEM micrographs of boron-doped nanocrystalline diamond-carbon nanospikes
Open Research DataThis dataset contains the Scanning Electron Microscopy (SEM) micrographs taken for rich boron-doped carbon crystalline nanospikes/nanograss structures, at different magnifications, encoded in the labels of the images. The micrographs were made using Hitachi S-3400N SEM microscope in secondary electron mode under 20 kV accelerating voltage. No additional...
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SEM micrographs of diamond-phase (sp3-C) rich boron-doped carbon nanowalls (sp2-C)
Open Research DataThis dataset contains the Scanning Electron Microscopy (SEM) micrographs taken for rich boron-doped carbon nanowalls structures, with different boron addition during the synthesis process and different CVD synthesis duration. The [B]/[C] ratios in the plasma were set to 0k, 1.2k, 2k and 5k ppm. The time of growth was ranging between 4 and 9 hours. This...
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Topography studies of screen-printed carbon electrodes (SPCE) with boron-doped diamond foils
Open Research DataThis dataset contains topography examination of SPCE containing boron-doped diamond BDD foils done with scanning electron microscope. Different points mark different electrode spots: A) working electrode, B) reference electrode, C) counter electrode, D) pads.
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Electrochemical studies for screen-printed carbon electrodes (SPCE) with boron-doped diamond foils
Open Research DataThis dataset contains electrochemical examination of SPCE paste and SPCE containing boron-doped diamond BDD foils. The studies include kinetics analyses with cyclic voltammetry and electrochemical impedance spectroscopy with different redox probes: hexacyanoferrate(III) and Hexaammineruthenium(III) and potentiostatic open circuit potential at different...
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Chemical and structural studies of screen-printed carbon electrodes (SPCE) with boron-doped diamond foils
Open Research DataThis dataset contains chemical analyses and structural studies by XPS and Raman spectroscopy, carried out for SPCE containing boron-doped diamond BDD foils done with scanning electron microscope. Different points for XPS analysis mark different electrode spots: A) working electrode, B) reference electrode, C) counter electrode, D) pads.
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Performance of Haemophilus influenzae impedimetric biosensors based on screen-printed carbon electrodes (SPCE) with boron-doped diamond foils
Open Research DataThis dataset contains electrochemical impedance spectroscopy studies of SPCE electrodes containing boron-doped diamond BDD foils and functionalized towards detection of Protein D and Haemophilus influenzae.
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Pore size distribution of PC-X (porous carbon materials obtained at various temperatures)
Open Research DataThese data contain pore size distribution of PC-700 (porous carbon materials obtained at 700°C), PC-800 (porous carbon materials obtained at 800°C) and PC-900 (porous carbon materials obtained at 900°C) analyzed by the nitrogen adsorption/desorption technique.
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Scanning electron microscopy (SEM) images of the boron-dopied carbon nanowalls surfaces
Open Research DataThe dataset contains the scanning electron micrographs (SEM), revealing the surface morphology of boron-doped carbon nanowalls electrodes on silicon substrates. The surface is characterized by nano-walled structures. The obtained electrodes were doped with boron at the level of [B]/[C] = 1200ppm in the gas atmosphere during the synthesis.
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Thermal stability analysis of poly(lactic acid)-carbon black-nanodiamond composite
Open Research DataThis dataset contains thermal stability tests carried out on new 3D printing-dedicated composites with poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Two types of nanodiamonds were studied: detonation nanodiamonds (DND) and boron-doped carbon nanowalls (BCNW). The investigated techniques include: thermogravimetric analysis (TGA)...
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Physicochemical studies (BET) of nanoparticles used for 3D printable conductive composites
Open Research DataThis dataset contains physico-chemical examination of fillers used to fabricate new 3D printing-dedicated composites with poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Geometric surface area of the nanoparticles was studied by Brunauer–Emmett–Teller (BET) adsorption/desorption isotherms. Investigated samples: CB Ensaco 250G, detonation...
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Suspended matter, composition and fluxes, Gdansk Deep, late spring 2001
Open Research DataParticulate organic carbon (POC) and nitrogen (PON) concentrations and fluxes were measured in the Gdańsk Deep (Gulf of Gdansk) from 30.05 to 06.06.2001. The vertical profiles of POC and PON were characterised by the highest values in the euphotic layer, a gradual decrease with depth, and an increase below the halocline. The hydrophysical conditions...
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Physicochemical studies (Raman, XRD) of poly(lactic acid)-carbon black-nanodiamond composites
Open Research DataThis dataset contains physico-chemical examination of a new 3D printing-dedicated composites with poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Two types of nanodiamonds were studied: detonation nanodiamonds (DND) and boron-doped carbon nanowalls (BCNW). The investigated techniques include Raman spectroscopy and X-ray diffraction...
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Rheology studies of poly(lactic acid)-carbon black-nanodiamond composites
Open Research DataThis dataset contains rheology measurements carried out on new 3D printing-dedicated composites with poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Two types of nanodiamonds were studied: detonation nanodiamonds (DND) and boron-doped carbon nanowalls (BCNW). The investigated techniques was performed by melt mass-flow rates (MFR)....
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Mechanical studies of poly(lactic acid)-carbon black-nanodiamond composites
Open Research DataThis dataset contains mechanical tests carried out on new 3D printing-dedicated composites with poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Two types of nanodiamonds were studied: detonation nanodiamonds (DND) and boron-doped carbon nanowalls (BCNW). The investigated techniques was dynamic mechanical analysis (DMA). The measurements...
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Electrochemical studies of poly(lactic acid)-carbon black-nanodiamond composites
Open Research DataThis dataset contains electrochemical investigation on electrodes 3D printed using a new composite composed of poly-lactic acid (PLA), carbon black (CB) and nanodiamond fillers. Two types of nanodiamonds were studied: detonation nanodiamonds (DND) and boron-doped carbon nanowalls (BCNW). The presented results contain:1. electrochemical characterisation...
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Research 1: Heterojunction of (P, S) co-doped g-C3N4 and 2D TiO2 for improved carbamazepine and acetaminophen photocatalytic degradation
Open Research DataThe first research article consisted on the synthesis of phosphorus and sulfur co-doped graphitic carbon nitride incorporated in 2D TiO2 structure for solar-driven degradation of emerging pollutants from the group of pharmaceuticals not susceptible to biodegradation. The hybrid photocatalysts with different loadings of (P, S)-doped g-C3N4 were characterized...
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XPS analysis of the GO based materials
Open Research DataGraphene oxides samples were measured by XPS method. The X-ray photoemission spectroscopy measurements were carried out with Omicron NanoTechnology UHV equipment. The hemispherical spectrophotometer was equipped with a 128-channel collector. The XPS measurements were performed at room temperature at a pressure below 1.1 × 10−8 mBar. The photoelectrons...
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The XAS spectra of O-K edges, Fe-L edges in pristine, La-, and Nb-doped SFM in 3 states: as-prepared, reduced and reoxidized
Open Research DataThis dataset contains the normalized and exported to *.txt spectra for x-ray absorption spectroscopy. The samples analyzed were strontium ferrite molybdate based, doped with lanthanum and niobium. The powders were measured in as-prepared state (denoted in filename as AP), reduced (red) and reoxidized (reox). The filenames are written accordingly: Edge_(optional:...
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Graphene oxide thin films deposited on a PCB board - chemical analysis
Open Research DataGraphene oxides based films were measured by X-ray photoemission spectroscopy (XPS) method. TheXPS measurements were carried out with the Omicron NanoTechnology UHV equipment. The hemispherical spectrophotometer was equipped with a 128-channel collector. The XPS measurements were performed at room temperature at a pressure below 1.1 × 10−8 mBar. The...
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Distance measurement by the low coherent interferometer
Open Research DataThe obtained data was acquired by the interferometric fiber-optic sensor of distance. The setup was constructed of a broadband light source working at the central wavelength of 1560 nm, an optical spectrum analyzer and a fiber-optic 2x1 coupler (with the power split 50:50). All elements were connected by standard single-mode optical fibers. The measurement...
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Distance measurement by the low coherent interferometer with NND layer (the source wavelegth 1310 nm)
Open Research DataThe obtained data was acquired by the interferometric fiber-optic sensor of distance. The setup was constructed of a broadband light source working at the central wavelength of 1310 nm, an optical spectrum analyzer, and a fiber-optic 2x1 coupler (with the power split 50:50). All elements were connected by standard single-mode optical fibers. The measurement...
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The biotic and abiotic mercury at the coastal zone of Gulf of Gdańsk
Open Research DataConcentration of neurotoxin Hg (mercury) was determined monthly form 01.2012 to 05.2013 (total and suspended) in the surface microlayer and the surface water as well as in: phytoplankton, zooplankton, epilithon, epifithon, phytobenthos (macroalgae and angiosperms), zoobenthos, and in the sediment. The study was conducted in the coastal zone of the Puck...
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Thermogravimetric analysis data of hydration in air and nitrogen for BaCe0.6Zr0.2Y0.1M0.1O3-δ (M = Fe, Pr, Tb)
Open Research DataThe dataset consists of 6 files of thermogravimetric analysis (TGA) data. The TGA experiments of hydration for BaCe0.6Zr0.2Y0.1Fe0.1O3-δ (BCZYFe), BaCe0.6Zr0.2Y0.1Pr0.1O3-δ (BCZYPr), and BaCe0.6Zr0.2Y0.1Tb0.1O3-δ (BCZYTb) were conducted on Netzsch STA 449.
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New 3D printable filaments with nanodiamonds, physicochemical additives characteristics and electrochemical activity
Open Research DataThis dataset contains the physicochemical analyses (XRD, Raman spectroscopy, BET analyses) and electrochemical analyses (CV, EIS) for a new 3D-printable composite has been developed dedicated to electroanalytical applications. Two types of diamondised nanocarbons - detonation nanodiamonds (DNDs) and boron-doped carbon nanowalls (BCNWs) - were added...
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The BDD electrodes wettability modification by anodic polarization treatment
Open Research DataThe dataset contains the raw images, photographs obtained for the contact angle measurement at the surface of the boron-doped diamond (BDD) electrode. The measurements were carried out on after potentiodynamic polarization procedure, at various anodic polarization scan range (no polarization - HTBDD; 1.0 V; 1.4 V; 1.9 V; 2.5 V vs Ag|AgCl, scan rate...
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Nutrients, oxygen and suspended matter - Gdansk Deep (2001-2005)
Open Research DataThe results show short-term changes in the concentration of nutrients (nitrates, nitrites, ammonium ions, phosphates and total forms of nitrogen and phosphorus), dissolved oxygen and suspended particulate matter - SPM and its main components (organic carbon - POC, nitrogen - PON, phosphorus - TPP) in the water column of the Gdańsk Deep (Gdańsk Bay).
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The luminescence study of Sr2TiO4:Sm3+ coumpounds.
Open Research DataA luminescent material based on the strontium orthotitanate (Sr2TiO4) matrix doped with 1% of a mole of samarium was obtained using the typical solid-state synthesis method under a neutral atmosphere of nitrogen. The sample was investigated using powder X-ray diffraction (XRD) and several luminescence techniques to study the phase composition, luminescence...
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AFM investigation of electrode fabricated by 3D printing
Open Research Data3D printing, also known as additive manufacturing, has enjoyed great interest in recent years due to the versatility of this method of producing various shapes and details. Due to the possibility of precise control of the shape and composition of the printed elements, the discussed technique can be widely used in electrochemistry, including electrochemical...