Wyniki wyszukiwania dla: SYNTHESIS

• Elżbieta Luboch prof. dr hab. inż.

  Osoby

• Wojciech Wojnowski dr inż.

  Osoby

  Katedra Chemii Analitycznej

  Ukończył V Liceum Ogólnokształcące w Gdańsku w klasie o profilu matematyczno-fizycznym z wykładowym językiem angielskim. W 2009 roku rozpoczął studia na Wydziale Chemicznym PG na kierunku technologia chemiczna, uzyskując w 2012 roku tytuł inżyniera, a w 2013 tytuł magistra. W latach 2013–2015 studiował sinologię na Uniwersytecie w Nankinie dzięki uzyskaniu Stypendium Rządu ChRL. Po powrocie do Polski w 2015 roku rozpoczął studia...

• Krzysztof Karwowski dr hab. inż.

  Osoby

  Katedra Inżynierii Elektrycznej Transportu

• Monika Wilamowska-Zawłocka dr hab. inż.

  Osoby

  Katedra Konwersji i Magazynowania Energii

  Dr hab. inż. Monika WILAMOWSKA-ZAWŁOCKA jest absolwentką Wydziału Chemicznego Politechniki Gdańskiej. Studia doktoranckie ukończyła w 2011 r., następnie odbyła roczny staż na Technicznym Uniwersytecie w Darmstadt w Niemczech. Pracuje w Politechnice Gdańskiej od 2013 r., od 2019 r. na stanowisku profesora uczelni. Specjalność –materiały elektrodowe w zastosowaniu do ogniw litowo-jonowych, sodowo-jonowych, kondensatorów elektrochemicznych...

• Janusz Rachoń prof. dr hab. inż.

  Osoby

  Biuro Praw,Wartości Akademickich i Równego Traktowania

  Sprawował urząd rektora w latach 2002-2008 Urodził się 11 sierpnia 1946 r. w Nowym Sączu. Studia wyższe ukończył w 1969 r. na Wydziale Chemicznym Politechniki Gdańskiej, uzyskując tytuł magistra inżyniera chemika. W 1969 r. rozpoczął pracę na Wydziale Chemicznym Politechniki Gdańskiej, na którym uzyskał w 1975 r. doktorat, a w 1985 r. habilitację. Na stanowisko docenta został powołany w 1989 r., na stanowisko profesora nadzwyczajnego...

• Stanisław Szczepański prof. dr hab. inż.

  Osoby

  Katedra Systemów Mikroelektronicznych

• FTIR spectra and IGC chromatograms for chemically reduced graphene oxide aerogels (rGOA)

  Dane Badawcze

  open access

  • G. Boczkaj
  • R. Castro Munoz
  • M. Plata Gryl

  The effect of selected synthesis parameters on reduced graphene oxide aerogels properties was investigated using Fourier-transform infrared spectroscopy and dynamic adsorption method (Inverse Gas Chromatography, IGC). Samples were synthesized by sol-gel method by reduction induced self-assembly of graphene oxide. As a reductant l-ascorbic acid was used....

• Non-Isocyanate-Based Waterborne Polyurethanes

  Publikacja

  • M. Włoch
  • I. Carayon

  - Rok 2022

  Non-isocyanate polyurethanes (NIPUs) are a greener alternative for the conventional polyurethanes synthesized using toxic and moisture-sensitive di- or polyisocyanates. The most often described method of NIPU synthesis involves the reaction of five-membered cyclic carbonates with amines, and resulting polymers containing primary and secondary hydroxyl groups (so they are also known as polyhydroxyurethanes), which can be further...

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• Andrzej Okuniewski dr inż.

  Osoby

  Politechnika Gdańska, Katedra Chemii Nieorganicznej

   Wykształcenie 2010-2014: Katedra Chemii Nieorganicznej, Wydział Chemiczny, Politechnika Gdańskadoktor nauk chemicznych (nauki chemiczne – chemia, chemia nieorganiczna) 2009-2010: Wydział Chemiczny, Politechnika Gdańskamagister chemii (chemia stosowana) 2005-2009: Wydział Chemiczny, Politechnika Gdańskainżynier chemik (chemia stosowana) 2002-2005: II Liceum Ogólnokształcące im. Władysława Pniewskiego w Gdańskuprofil biologiczno-chemiczno-fizyczny...

• Chemistry and Nanochemistry 2024

  Kursy Online

  • M. Prześniak-Welenc
  • A. Manohar
  • M. Bobrowski

  We start from General Chemistry, including: calculus in chemistry, bonds, balancing the chemical reactions, redox reactions, electrochemistry, pH, acids, bases, salts, oxides, organic molecules, and many informations about synthesis, analysis and applications in nanochemistry.

• Chemistry and Nanochemistry 2023

  Kursy Online

  • M. Prześniak-Welenc
  • M. Bobrowski

  We start from General Chemistry, including: calculus in chemistry, bonds, balancing the chemical reactions, redox reactions, electrochemistry, pH, acids, bases, salts, oxides, organic molecules, and many informations about synthesis, analysis and applications in nanochemistry.

• X-ray diffraction (XRD) of silica-coated bismuth oxide/gadolinium oxide (Bi2O3+Gd2O3) structures

  Dane Badawcze

  open access

  • T. Kędzierski
  • E. Mijowska
  • P. Sikora

  Data contain results from X-ray diffraction (XRD) measurements of pristine Bi2O3 and Gd2O3 structures using Aeris diffractometer (Malvern Panalytical, Malvern, UK) with Cu-Kα radiation (λ = 1.544 Å)

• Kinga Kaniewska-Laskowska dr inż.

  Osoby

  Katedra Chemii Nieorganicznej

  Wykształcenie Studia I stopnia - inżynierskie, kierunek CHEMIA 2013: Politechnika Gdańska, Wydział Chemiczny, Katedra Chemii Nieorganicznej Tytuł pracy inżynierskiej: „Kompleksy żelaza z ligandami fosfinidenowymi” Promotor: dr hab. inż. Rafał Grubba Studia II stopnia - magisterskie, kierunek TECHNOLOGIA CHEMICZNA, spec. Technologia Organiczna 2014: Politechnika Gdańska, Wydział Chemiczny, Katedra Chemii Nieorganicznej Tytuł pracy...

• Microstructural Design of Ba0.5La0.5Co0.5Fe0.5O3 Perovskite Ceramics

  Publikacja

  • D. Balcerzak
  • I. Szpunar
  • F. Oseko
  • J. Pośpiech
  • M. Nadolska-Dawidowska
  • M. Pieragowska
  • K. Reniecka
  • K. Waniek
  • K. Leszczyński
  • A. D. Mielewczyk-Gryń... i 2 innych

  - Materials - Rok 2021

  Ba0.5La0.5Co0.5Fe0.5O3 was synthesized in the solid-state reaction route. The influence of ball milling parameters (such as milling media size, angular velocity, and time), pelletizing pressure, and annealing parameters on the microstructure was studied. The grain size distribution and density or specific surface area changes were investigated in each approach while the individual parameters were changed. The evaluation of BLCF...

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• Ewa Wagner-Wysiecka dr hab. inż.

  Osoby

  Katedra Chemii i Technologii Materiałów Funkcjonalnych

  Ewa Wagner-Wysiecka absolwentka Wydziału Chemicznego PG (Kierunek Technologia Chemiczna, kierunek dyplomowania: Technologia Nieorganiczna, specjalność: Analityka Techniczna i Przemysłowa). Pracę magisterską pt. ”Identyfikacja zanieczyszczeń występujących w farmakopealnej sulfachinoksalinie” zrealizowała pod kierunkiem prof. dr hab. inż. Jana F. Biernata. Po ukończeniu studiów magisterskich (1997 r.) rozpoczęła studia doktoranckie....

• Jarosław Chojnacki prof. dr hab. inż.

  Osoby

  Katedra Chemii Nieorganicznej

  Urodzony w 1961 w Bydgoszczy, absolwent Technikum Chemicznego im. I. Łukasiewicza w Bydgoszczy. Studia chemiczne ukończył na Wydziale Chemicznym Politechniki Gdańskiej w 1986 roku, broniąc pracy dotyczącej elektrod jonoselektywnych. Późniejsze badania związane były z syntezą organiczną i krzemoorganiczną a od 2002 roku z krystalografią. Praca doktorska dotyczyła silanotiolanów miedziowców, a dysertacja habilitacyjna (2010) opisywała...

• Organic syntheses greenness assessment with multicriteria decision analysis

  Publikacja

  • M. Tobiszewski
  • W. Przychodzeń
  • M. Bystrzanowska
  • M. J. Milewska

  - GREEN CHEMISTRY - Rok 2021

  Green chemistry requires a metrics system that is comprehensive by the criteria included and simple in the application at the same time. We propose the application of multicriteria decision analysis for com- parative greenness assessment of organic synthesis procedures. The assessment is based on 9 criteria (the reagent, reaction efficiency, atom economy, temperature, pressure, synthesis time, solvent, catalyst and reactant) for...

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• X-ray diffraction patterns of BaCe0.6Zr0.2Y0.1M0.1O3-δ (M = Fe, Pr, Tb)

  Dane Badawcze

  wersja 1.1 open access

  • J. Budnik
  • M. Gazda

  - seria: Data used in article "Water uptake kinetics and electrical transport in BaCe0.6Zr0.2Y0.1M0.1O3-δ (M = Tb, Pr, Fe) protonic conductors"

  The dataset consists of three raw X-ray diffraction (XRD) files collected using a Phillips X’Pert Pro diffractometer (CuKα radiation (𝜆 = 1.541 Å), under 40 kV and 30 mA). The diffraction patterns of BaCe0.6Zr0.2Y0.1Fe0.1O3-δ (BCZYFe), BaCe0.6Zr0.2Y0.1Pr0.1O3-δ (BCZYPr), and BaCe0.6Zr0.2Y0.1Tb0.1O3-δ (BCZYTb) were collected at room temperature. Collected...

• SEM micrographs of diamond-phase (sp3-C) rich boron-doped carbon nanowalls (sp2-C)

  Dane Badawcze

  open access

  • J. Ryl
  • M. Sobaszek
  • R. Bogdanowicz
  • M. Ficek

  This dataset contains the Scanning Electron Microscopy (SEM) micrographs taken for rich boron-doped carbon nanowalls structures, with different boron addition during the synthesis process and different CVD synthesis duration. The [B]/[C] ratios in the plasma were set to 0k, 1.2k, 2k and 5k ppm. The time of growth was ranging between 4 and 9 hours. This...

• Ambiphilic phosphorous compounds

  Dane Badawcze

  open access

  • N. Szynkiewicz

  - seria: Synthesis of ambiphilic P-based compounds via functionalization of diphosphanes

  Results of theoretical and experimental studies on ambiphilic phosphorous compounds:

• Polyurethanes

  Publikacja

  • H. Janik
  • M. Sienkiewicz
  • J. Kucińska-Lipka

  - Rok 2014

  The chapter content is devoted to Polyurethanes and consists of the following items: general characteristics of polyurethanes, raw materials used in the synthesis of crosslinked polyurethanes, synthesis and crosslinking reactions of polyurethanes, morphology of liniear and branched PU, manufacturing methods and functional properties.

• BET adsorption-desorption isotherm of nano-MgO

  Dane Badawcze

  open access

  • P. Błaszczak
  • B. Bochentyn

  The dataset includes the isotherms of adortion and desorption of N2 at LN2 temperature. The sorption isotherms were obtained using Quatachrome NovaTouch LX1 equippment. The ceramic measured powder was composed of nanometric MgO (CA-assisted method of synthesis)

• BET adsorption-desorption isotherm of nano-ZrO2

  Dane Badawcze

  open access

  • P. Błaszczak
  • B. Bochentyn

  The dataset includes the isotherms of adortion and desorption of N2 at LN2 temperature. The sorption isotherms were obtained using Quatachrome NovaTouch LX1 equippment. The ceramic measured powder was composed of nanometric ZrO2 (CA-assisted method of synthesis)

• BET adsorption-desorption isotherm of nano-SrTiO3

  Dane Badawcze

  open access

  • P. Błaszczak
  • B. Bochentyn

  The dataset includes the isotherms of adortion and desorption of N2 at LN2 temperature. The sorption isotherms were obtained using Quatachrome NovaTouch LX1 equippment. The ceramic measured powder was composed of nanometric SrTiO3 (CA-assisted method of synthesis)

• BET adsorption-desorption isotherm of CeO2 pure

  Dane Badawcze

  open access

  • P. Błaszczak
  • B. Bochentyn

  The dataset includes the isotherms of adortion and desorption of N2 at LN2 temperature. The sorption isotherms were obtained using Quatachrome NovaTouch LX1 equippment. The ceramic measured powder was composed of nanometric pure CeO2 (CA-assisted method of synthesis)

• Transmission electron microscope (TEM) and optical microscope images of pristine and silica-coated bismuth oxide and gadolinium oxide particles

  Dane Badawcze

  open access

  • T. Kędzierski
  • E. Mijowska
  • P. Sikora

  Collection of raw transmission electron microscope (TEM) micrographs and optical microscope images used in the associated manuscript. All data in accessible *.tif format. Zip package contains:

• Ambiphilic phosphorous compounds 2

  Dane Badawcze

  open access

  • N. Szynkiewicz

  - seria: Synthesis of P(V)-P(III) and P(V)-CH2-P(III) compounds

  Results of theoretical and experimental studies on ambiphilic phosphorous compounds:

• Neurocontrolled Car Speed System

  Publikacja

  • M. Nakonechnyi
  • O. Ivakhiv
  • D. Świsulski

  - Journal of Automation, Mobile Robotics and Intelligent Systems - JAMRIS - Rok 2023

  The features of the synthesis of neural controllers for the car speed control system are considered in this article. The task of synthesis is to determine the weight coefficients of neural networks that provide the implementation of proportional and proportional-integralderivative control laws. The synthesis of controllers is based on an approach that uses a reversed model of the standard. A model of the car speed control system with...

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• Linear impedance of V2O5 nanorods obtained at 923K

  Dane Badawcze

  open access

  • M. Prześniak-Welenc
  • N. Wójcik
  • J. Ryl

  - seria: Vanadium oxides

  The DataSet contains the linear electrical properties of V2O5 nanorods which were measured by the impedance spectroscopy method. V2O5 nanorods were obtained by the sol-gel method. The information about xerogel powder synthesis is described in the Journal of Nanomaterials. The precursor powder was pressed into the disk-shaped pellets (12mm in diameter...

• Scanning electron microscopy (SEM) images of the boron-dopied diamond surfaces

  Dane Badawcze

  open access

  • M. Ficek
  • R. Bogdanowicz
  • J. Ryl

  The dataset contains the scanning electron micrographs (SEM), revealing the surface morphology of diamond electrodes on silicon substrates. The diamond surface is characterized by ultra-crystalline diamonds obtained by CVD synthesis. 

• The electronic characterization of the cubic Laves-phase superconductor CaRh2

  Publikacja

  • K. Górnicka
  • R. J. Cava
  • T. Klimczuk

  - JOURNAL OF ALLOYS AND COMPOUNDS - Rok 2019

  We present the synthesis and experimental characterization of the electronic properties of the cubic Laves phase superconductor CaRh2. Its crystal structure was confirmed by powder X-ray diffraction and its ambient temperature lattice parameter (a = 7.5326(6) Å) is in good agreement with the literature. Magnetization, resistivity and heat-capacity measurements indicate that CaRh2 is a moderate-coupling type-II superconductor (λe-p = 0.89)...

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• Thermal stability of V2O5 nanorods under oxidizing atmosphere

  Dane Badawcze

  open access

  • M. Prześniak-Welenc
  • J. Ryl

  - seria: Vanadium oxides

  The DataSet contains the TGA curves of V2O5 nanorods obtained at 650°C. The information about nanorods synthesis is described in the Journal of Nanomaterials.

• Recent developmentsinthesynthesisand biological activityofacridine/acridoneanalogues

  Publikacja

  • M. Gensicka-Kowalewska
  • G. Cholewiński
  • K. Dzierzbicka

  - RSC Advances - Rok 2017

  Many people in the world struggle with cancer or bacterial, parasitic, viral, Alzheimer's and other diseases. Therefore, many scientists seek new, more effective, more selective and less toxic drugs. Acridine/acridone derivatives constitute a class of compounds with a broad spectrum of biological activity and are of great interest to scientists. Todate, many acridine/acridone analogues have been obtained,which, inter alia, exhibit...

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• Accurate design of pseudoelliptic inline SIW filters with frequency-dependent couplings

  Publikacja

  • A. Jędrzejewski
  • Ł. Szydłowski
  • M. Mrozowski

  - Rok 2014

  This paper presents an accurate synthesis method for inline SIW (Substrate Integrated Waveguide) generalized Chebyshev bandpass filters with frequency-dependent couplings. The technique is based on the synthesis of a coupling matrix that takes into account the impedance of the frequency-dependent stub. Thus, a loading effect compensation in adjacent resonators (via resonant frequency adjustment) and coupling elements (via coupling-value...

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• Renewable natural resources as green alternative substrates to obtain bio-based non-isocyanate polyurethanes-review

  Publikacja

  • K. Rohde
  • J. Datta

  - CRITICAL REVIEWS IN ENVIRONMENTAL SCIENCE AND TECHNOLOGY - Rok 2019

  Commercially available polyurethanes are synthesized by the polyaddition of diisocyanates with polyols and low molecular weight chain extenders. A new approach to polyurethanes synthesis is realized via non-isocyanate routes. Negative impacts of petroleum-based chemicals on the environment and human health as well as gradual reduction of fuel-based resources, which leads to an increase in their prices, are an incentive to looking...

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• TEM micrographs of V2O5 nanostructures

  Dane Badawcze

  open access

  • M. Prześniak-Welenc
  • J. Ryl

  - seria: Vanadium oxides

  The DataSet contains the TEM images of V2O5 nanostructures obtained by the sol-gel method. 

• Changes in heat flow of V2O5 nanorods under oxidizing atmosphere

  Dane Badawcze

  open access

  • M. Prześniak-Welenc
  • J. Ryl

  - seria: Vanadium oxides

  The DataSet contains the DSC curves of V2O5 nanorods obtained at 650°C. The information about nanorods synthesis is described in the Journal of Nanomaterials.

• In vitro evaluation of novel lipopeptides with potential therapeutic application

  Publikacja

  • M. Kukowska
  • K. Dzierzbicka
  • W. Januchta

  - JOURNAL OF PEPTIDE SCIENCE - Rok 2014

  The synthesis of derivatives of Gly-His-Lys was elaborated followed by their antimicrobial activity investigation.

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• Controlling the europium oxidation state in diopside through flux concentration

  Publikacja

  • N. Górecka
  • T. Lesniewski
  • S. Mahlik
  • M. S. Łapiński
  • Y. Tsai
  • A. Bielicka-giełdoń
  • K. Szczodrowski

  - DALTON TRANSACTIONS - Rok 2024

  This paper explores the connection between the H3BO3 flux concentration and the co-existence of Eu2+ and Eu3+ dopants within CaMgSi2O6 crystals (diopside). The samples were synthesised using a solid-state synthesis method under varying atmospheric conditions, including oxidative (air), neutral (N2), and reductive (H2/N2 mixture) environments. Additionally, some materials underwent chemical modification by partially substituting...

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• Ion recognition properties of new pyridine-2,6-dicarboxamide bearing propeller-like pendant residues: multi-spectroscopic approach

  Publikacja

  • E. Wagner-Wysiecka
  • N. Łukasik
  • A. Okuniewski
  • B. Galiński

  - MONATSHEFTE FUR CHEMIE - Rok 2020

  The synthesis and ion binding properties of new amide derived from propeller-like tris(2-pyridyl)amine and 2,6-pyridinedicarboxylic acid chloride were described. Amide binds divalent metal cations: copper(II), nickel(II), zinc(II), and lead(II) in acetonitrile. In acetonitrile:water mixture (9:1 v/v) amide interacts only with copper(II) and nickel(II) cations forming complexes of 1:1 stoichiometry. It was found that the introduction...

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• Alkanethiolates of Group 1,2, and 13-15 Metals

  Publikacja

  • D. Witt

  - Rok 2011

  This manuscript is an update to the earlier Science of Synthesis contribution describing methods for the synthesis of alkanethiolates of group 1, 2, and 13-15 metals. Alkanethiolates can be converted into S-alkyl thiocarboxylic acid esters, 1-thioglycosides, S-alkyl thiosulfinates, tetrahydro-1,4-thiazine-3-ones, sulfides, disulfides, sulfonium salts, dithioacetals and dithioketals, etc. These transformations are accomplished by...

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• Decomposition kinetics of vanadium xerogel powder

  Dane Badawcze

  open access

  • M. Prześniak-Welenc
  • J. Ryl

  - seria: Vanadium oxides

  The DataSet contains the TGA curves of vanadium As-prepared xerogel powder with different heating rates. The information about sol synthesis is described in the Journal of Nanomaterials.

• XRD patterns of nickel-modified V2CTx

  Dane Badawcze

  open access

  • I. Frąckiewicz

  The set includes data for XRD pattern preparation of nickel-modified V2CTx samples.

• Nowe monomery pochodzenia roślinnego w syntezie termoplastycznych elastomerów poliuretanowych

  Publikacja

  • P. Kasprzyk
  • J. Datta

  - Elastomery - Rok 2018

  Jak dotychczas w syntezie termoplastycznych elastomerów poliuretanowych (TPU) są powszechnie wykorzystywane surowce pochodzenia petrochemicznego. Sytuacja jednak zmienia się dynamicznie i w wielu gospodarkach świata widoczne są już trendy, polegające na coraz większym wykorzystaniu substancji pochodzenia roślinnego w produkcji surowców, np. glikoli, izocyjanianów czy polioli, jako zamienników analogów syntetycznych. Praca obejmuje...

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• Isocyanate-Free Polyurethanes

  Publikacja

  • M. Włoch
  • K. Rohde

  - Rok 2021

  Isocyanate-free polyurethanes (also called non-isocyanate polyurethanes, or NIPUs) are alternatives to the conventional (commercially used) polyurethanes synthesized using di- or polyisocyanates, polyols, and chain extenders with low molecular weight. The major routes of NIPUs’ synthesis involve polyaddition of cyclic carbonates and di- or polyamines, polycondensation of carbamates, and diols. The most important intermediates are...

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• The enantiomeric determination of chloro-precursors of methamphetamine

  Publikacja

  • J. Płotka-Wasylka
  • M. Biziuk
  • C. Morrison

  - Rok 2011

  Impurity profiling and classification of seized methamphetamine may supply valuable information with respect to the conditions and the chemicals used in the illicit methamphetamine manufacture and may provide information on the original source of the sample. Determination of the stereochemical makeup of forensic samples is important as well for the same reasons. Laboratories in many places are engaged in clandestine manufacture...

• Thermal behaviour of vanadium xerogel powder under different inert atmosphere

  Dane Badawcze

  open access

  • M. Prześniak-Welenc
  • J. Ryl

  - seria: Vanadium oxides

  The DataSet contains the results of the thermal behavior of the vanadium xerogel powder. The information about xerogel powder synthesis is described in the Journal of Nanomaterials.

• Thermal stability of V2O5 nanorods under inert atmosphere

  Dane Badawcze

  open access

  • M. Prześniak-Welenc
  • J. Ryl

  - seria: Vanadium oxides

  The DataSet contains the TGA curves of V2O5 nanorods obtained at 650°C. The information about nanorods synthesis is described in the Journal of Nanomaterials.

• Crystallization kinetics of V2O5 nanorods

  Dane Badawcze

  open access

  • M. Prześniak-Welenc
  • J. Ryl

  - seria: Vanadium oxides

  The DataSet contains the DSC curves of As-prepared xerogel powder with different heating rates. The information about sol synthesis is described in the Journal of Nanomaterials.

• Non-isocyanate Polyurethanes

  Publikacja

  • M. Włoch
  • J. Datta

  - Rok 2017

  The main aim of this chapter is to present a general overview of the NIPU synthesis method (i.e., polycondensation and polyaddition), and to describe structure and properties of selected intermediates and final polymeric products. The focus is on five-membered ring cyclic carbonate intermediates, which were obtained by cycloaddition of carbon dioxide to selected glycidyl ethers and thiol-ene coupling of unsaturated cyclic carbonates...

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