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Wyniki wyszukiwania dla: LIQUID-STRUCTURE INTERACTION
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Effect of hydroxylated soybean oil and bio-based propanediol on the structure and thermal properties of synthesized bio-polyurethanes
PublikacjaThe aim of this work was to obtain bio-polyurethanes using synthetic compounds and bio-components, i.e. bio-glycols. Bio-polyurethanes were prepared by means of the prepolymer method. Prepolymers were synthesized from 4,4′-diphenylmethane diisocyanate (MDI) and a polyol mixture containing 75% by weight of commercial polyether and 25% by weight of hydroxylated soybean oils (H2 or H3), the latter being obtained in the reaction with...
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Structure of the register of immovable monuments in terms of the number of monuments by voivodeship – comparison of 2016 and 2024
Dane BadawczeThis dataset compares the structure of the register of immovable monuments in Poland regarding the number of monuments by voivodeship for 2016 and 2024. Over eight years, the number of immovable monuments has increased (over 9000 monuments increase). The historical regions impact the fact that the most immovable monuments are located in Lower Silesia,...
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Effect of chemical structure on complexation efficiency of aromatic drugs with cyclodextrins: The example of dibenzazepine derivatives
PublikacjaIt is widely believed that the hydrophobic effect governs the binding of guest molecules to cyclodextrins (CDs). However, it is also known that high hydrophobicity of guest molecules does not always translate to the formation of stable inclusion complexes with CDs. Indeed, a plethora of other factors can play a role in the efficiency of guest–CD interactions, rendering structure-based prediction of the complexation efficiency with...
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Prediction of protein structure with the coarse-grained UNRES force field assisted by small X-ray scattering data and knowledge-based information
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Fe local structure in Pt-free nitrogen-modified carbon based electrocatalysts: XAFS study
PublikacjaThe paper presents a new results on the bonding environment (coordination number and geometry) and on oxidation states of Fe in nitrogen-modified Fe/C composites used as Pt-free catalysts for oxygen reduction in Direct Hydrogen Fuel Cells. Starting from glucose or fructose, two catalysts displaying different electrochemical performance were prepared and studied in the form of pristine powder and thin catalytic layer of electrode...
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Green thermoplastic poly(ether-urethane)s – synthesis, chemical structure and selected properties investigation
PublikacjaThis work aimed to characterize the effect of the monomers chemical structure on the selected properties of the green thermoplastic poly(ether-urethane)s. During synthesis two types of polyether biopolyols, 4,4′-diphenylmethane diisocyanate and bio-based 1,3-propanediol were employed. Materials were synthesized with the use of two step method and two different prepolymers, which were mixed together in equimolar quantities. Obtained...
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IFAC Conference on System Structure and Control
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From Structure to Luminescent Properties of B2O3-Bi2O3-SrF2 Glass and Glass-Ceramics Doped with Eu3+ Ions
PublikacjaGlass-ceramics with the composition B2O3 -Bi2O3 -SrF2 were synthesized by the conventional melt-quenching technique and subsequent crystallization of the parental glasses. The temperature at which the ceramization was carried out was selected based on differential scanning calorimetry (DSC) analysis. The structure of the studied materials and the formation of SrF2 nanocrystals were confirmed by the Fourier-transform infrared spectroscopy...
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Design of Structure of Tension Leg Platform for 6 MW Offshore Wind Turbine Based On Fem Analysis
PublikacjaThe article presents the calculation and design stages of the TLP platform serving as a supporting construction of a 6 MW offshore wind turbine. This platform is designed to anchor at sea at a depth of 60 m. The authors presented the method of parameterization and optimization of the hull geometry. For the two selected geometry variants, the load and motion calculations of the platform subjected to wind, wave and current under...
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Mass spectrometry based identification of geometric isomers during metabolic stability study of a new cytotoxic sulfonamide derivatives supported by quantitative structure-retention relationships
PublikacjaA set of 15 new sulphonamide derivatives, presenting antitumor activity have been subjected to a metabolic stability study. The results showed that besides products of biotransformation, some additional peaks occurred in chromatograms. Tandem mass spectrometry revealed the same mass and fragmentation pathway, suggesting that geometric isomerization occurred. Thus, to support this hypothesis, quantitative structure-retention relationships...
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Structure and hyperfine interactions in Bi1−xNdxFeO3 solid solutions prepared by solid-state sintering
PublikacjaThe series of polycrystalline ceramic powders, Bi1xNdxFeO3 (x = 0.11) was successfully synthesized by mixed oxide method followed by pressureless sintering. X-ray diffraction and Mössbauer spectroscopy were used as complementary methods to study structure and hyperfine interactions of the samples. It was found that with an increase of Nd content, within the range of x = 0.20.3 a structural phase transition from rhombohedral to...
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Modular Ceramic-Polymeric Device for Analysis of Selected Elements in Liquid Using Microplasma
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Review of the applicability of ionic liquid matrices for the quantification of small molecules by MALDI MS
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On the inappropriate fit of diffusion functions at thermal decomposition of some azomonoethers in liquid state
PublikacjaW celu analizy rozkładu termicznego tytułowych barwników azowych zastosowano mechanizmy D1, D2, D3 i D4. W wyniku przeprowadzonych badań stwierdzono, że rozkład zachodzi w fazie ciekłej, zaś w celu wyznaczenia parametrów aktywacji oraz wyznaczenia funkcji przemiany zastosowano koncepcje homo- i heterogeniczne.
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About nutrient liquid flow between potential flow and cartilage surface in bioreactor
PublikacjaW niniejszej pracy wyznaczony został przepływ cieczy odżywczej o właściwościach nienewtonowskich w cienkiej warstwie granicznej w pobliżu powierzchni komórek chrząstki (chondrocytu) podczas hodowli w bioreaktorze. Ruch cieczy w warstwie granicznej jest wywołany wydatkiem przepływu dostarczanej cieczy do bioreaktora. Ponadto prędkość przepływu cieczy w warstwie granicznej wokół hodowanych komórek chrząstki stawowej jest uzależniona...
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Influence of rotating magnetic field on gas-liquid volumetric mass transfer coefficient
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Headspace liquid phase microextraction for quantitation of hexanal in potato crisps by gas chromatography
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Gas to liquid mass transfer in mixing system with application of rotating magnetic field
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Turbulent heat transfer in thin liquid films at low and high heat fluxes
PublikacjaW pracy przedstawiono rozważania turbulentnej wymiany ciepła w cienkich filmach cieczowych powstałych w wyniku uderzenia strugi przy małych i dużych strumieniach ciepła. W ostatnim przypadku może dojść do wrzenia filmu cieczowego. Oba zjawiska zamodelowano i uzyskano odpowiednie rozkłady temperatury i pedkosci.
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On the Mechanism of Coupled Transport of Cu(II) Ions Through Bulk Liquid Membranes.
PublikacjaTransport jonów Cu(II) przez ciekłe membrany za pomocą 5 - nonylosalicyloaldoksimu jako przenośnika wymaga obecności kompleksu o stosunku metalu do przenośnika 1:2. Zbadano dwie możliwości mechanizmu jego tworzenia. Roztrzygnięcie, który mechanizm jest prawidłowy nie jest możliwe w oparciu jedynie o kinteykę chemiczną.
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Balance of pesticides mass in gas, liquid and solid phase after their chemical degradation.
PublikacjaOpisano metodę usuwania pestycydów z wody przy zastosowaniu fotodegradacji (UV) i katalizatora (TiO2). Efektywność procesu usuwania pestycydów była kontrolowana przy zastosowaniu chromatografu gazowego z detektorem wychwytu elektronów. Oznaczano zawartość pestycydów w wodzie, a także zaadsorbowanych na powierzchni stałej, oraz w fazie gazowej. Największa zawartość pestycydów znajdowała się na fazie stałej, następnie w cieczy i...
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Kinetics of spinodal decomposition in the Ising model with dynamic lattice liquid (DLL) dynamics
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From the Dynamic Lattice Liquid Algorithm to the Dedicated Parallel Computer – mDLL Machine
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The utilization of sludge generated in coagulation of fish processing wastewater for liquid feed production
PublikacjaWykorzystano koagulację do wydzielenia ze ścieków z przemysłu rybnego białek i tłuszczów. Uzyskany osad pokoagulacyjny dodawano do produkcji rybnych hydrolizatów białkowych. Zmodyfikowano proces wytwarzania rybnych hydrolizatów z wykorzystaniem kwasów siarkowego (VI) oraz ortofosforowego (V).
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Silicon polypodands: a new class of efficient solid–liquid phase-transfer catalysts
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Application of a new class B-podands in solid–liquid phase transfer catalysis
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A new type of B-podand catalysts for solid–liquid phase transfer reactions
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Deep Learning-Based, Multiclass Approach to Cancer Classification on Liquid Biopsy Data
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Experimental Determination of Limit Adhesive Shear Strtess between Solid Wall and Liquid
PublikacjaTheoretically slip of a fluid with respect to the solid wall should occur even at a very low velocity of motion. However theoretical analysisand some empirical data suggest that there must be a limit value of shear stress, below which the slip does not appear. A simple metyhod of this stress determination was proposed in the paper.
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High resolution liquid chromatography and time of flight mass spectrometry in perfume analysis
PublikacjaPerfumes consist of a wide range of natural and synthetic compounds that belongs to different chemical classes. Most of these compounds are generally determined by GC. However, in this study RP-HPLC-Q-TOF-MS and HILIC-Q-TOF-MS technique was applied for the determination of ingredients of original perfumes and their imitations. Antioxidants and compounds specific to fragrances of animal \origin were found in original...
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Effect of bio-polyol molecular weight on the structure and properties of polyurethane-polyisocyanurate (PUR-PIR) foams
PublikacjaThe increasing interest in polyurethane materials has raised the question of the environmental impact of these materials. For this reason, the scientists aim to find an extremely difficult balance between new material technologies and sustainable development. This work attempts to validate the possibility of replacing petrochemical polyols with previously synthesized bio-polyols and their impact on the structure and properties...
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Dipole-bound anions supported by charge-transfer interaction: valence- and dipole-bound anionic states of H3N→BF3
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Non-Targeted Metabolite Profiling Reveals Host Metabolomic Reprogramming during the Interaction of Black Pepper with Phytophthora capsici
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Preliminary performance evaluation of a high resolution small animal PET scanner with monolithic crystals and depth-of-interaction encoding
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In vivo study on borophene nanoflakes interaction with Tenebrio molitor beetle: viability of hemocytes and short-term immunity effect
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In vivo study on borophene nanoflakes interaction with Tenebrio molitor beetle: viability of hemocytes and short-term immunity effect
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The EU European contribution to global coastal zone research: an ELOISE (European Land-Ocean Interaction Studies) project
PublikacjaW artykule omówiono strukturę oraz cele i zadania programu ELOISE, finansowanego przez Wspólnotę Europejską. W ramach projektu realizowane są 4 główne zadania badawcze:1. cykle biochemiczne i strumienie zanieczyszczeń,2. struktura i funkcjonowanie ekosystemów,3. modelowanie i zarządzanie informacjami o środowisku,4. integracja nauk przyrodniczych i socjoekonomicznych.
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Site-selective cation–π interaction as a way of selective recognition of the caesium cation using sumanene-functionalized ferrocenes
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Poly(3,4-ethynenedioxythiophene)-Prussian Blue hybrid material evidence of direct chemical interaction betwenn PB andpEDOT
PublikacjaPrzedstawiono syntezę materiału złożonego z poli(3,4-etylenodioksytiofenu) oraz analogu błękitu pruskiego. Sieć struktury BP utworzona została wewnątrz matrycy polimerowej pEDOT-u za pomocą metody polaryzacji multicyklicznej. Chemiczne oddziaływania Fe z BP oraz siarki z pEDOT zostały potwierdzone metodą XPS. Obecność BP potwierdzono FTiR - stwierdzono obecność drgań rozciągających Fe-C oraz Fe-N. Metoda cyklowoltamperometryczna...
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Study on the effect of the metal–support (Fe-MgO and Pt-MgO) interaction in alcohol-CVD synthesis of carbon nanotubes
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The effect of Sr and Mg substitutions on structure, mechanical properties and solubility of fluorapatite ceramics for biomedical applications
PublikacjaIonic substitutions play important role in the modifications of biological apatites. Recently, attention has been focused on the co-doping effects on the functional properties of apatite-based biomaterials. In this research work, the dense samples of fluorapatites, Ca10(PO4)6F2 and Ca8MgSr(PO4)6F2, were produced after sintering at 1250 °C for 6 h in air. Structural characterization carried out with XRD, IR, Raman and SEM, confirmed...
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Effect of Nb and Al on in vitro dissolution behavior and structure of Na2O-MgO CaO-P2O5 glasses
PublikacjaIn vitro dissolution, structure, and thermal properties of the glass series Na2O-MgOsingle bondCaOsingle bondNb2O5 -Al2O3-P2O5 were studied. The dissolution behavior in phosphate-buffered saline (PBS) confirmed the potential bioactive properties of tested glasses. The dissolution process was found to depend on the Al, Nb, and Mg contents. Al, respectively, suppresses the Nb and accelerates the Mg release process from the glasses....
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Chemical structure, thermal and mechanical characterization of bio-based polyurethane composites filled with microcrystalline cellulose
PublikacjaOver the past several decades, the interest in replacing the synthetic components used in the production of polymers and composites with their natural counteparts has been growing. Biocomposites belong to the group of materials produced with the use of renewable raw materials. There has been a recent surge of interest in the industrial applications of composites containing natural fibres reinforced with biopolymers. Biopolymers...
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Polypropylene structure alterations after 5 years of natural degradation in a waste landfill
PublikacjaUp to 25% of plastic waste in Europe is still disposed of in landfills, despite recycling efforts. The plastic waste in the landfill plot may be exposed both to abiotic and biotic degradation processes, although it is thought that most of the plastic materials tend to be resistant to biodegradation or biodeterioration even after a long time. To verify if polypropylene (PP) can undergo the process of short-term biodegradation and...
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The valance state of vanadium-key factor in the flexibility of potassium vanadates structure as cathode materials in Li-ion batteries
PublikacjaPotassium hexavanadate (K2V6O16·nH2O) nanobelts have been synthesized by the LPE-IonEx method, which is dedicated to synthesis of transition metal oxide bronzes with controlled morphology and structure. The electrochemical performance of K2V6O16·nH2O as a cathode material for lithium-ion batteries has been evaluated. The KVO nanobelts demonstrated a high discharge capacity of 260 mAh g−1, and long-term cyclic stability up to 100...
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Modification of cellulosic filler with diisocyanates – volatile organic compounds emission assessment and stability of chemical structure over time
PublikacjaThis paper investigated the impact of type and content of diisocyanate on the structure of modified cellulose fillers. Four the most popular isocyanates were applied – isophorone, hexamethylene, toluene and methylene diphenyl diisocyanate – at loadings of 1–15 wt%. Chemical structure, and its short-term storage stability, were investigated for eight weeks. Moreover, the main volatile organic compounds detected during modification,...
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The effect of calcination temperature on structure and photocatalytic properties of Au/Pd nanoparticles supported on TiO2
PublikacjaBimetallic nanoparticles, composed of two different metal elements, can exhibit peculiar electronic, optical, and catalytic or photocatalytic properties that are absent in the corresponding monometallic nanoparticles. We show the effect of calcination temperature (from 350 to 700°C) on the structure and the photocatalytic properties of Au/Pd-modified TiO2. The composition of the bimetallic Au/Pd nanoparticles in relation to their...
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Structure and properties of the exopolysaccharides produced by Pseudomonas mutabilis T6 and P. mutabilis ATCC 31014
PublikacjaThis paper presents a study on the purification, primary structure, and rheological properties of exopolysaccharides isolated from cultures of Pseudomonas mutabilis T6 and P. mutabilis ATCC 31014. Both polymers are exopolysaccharides of D-mannose. The mannan isolated from P. mutabilis T6 contains on average about 5% of residual b-D-glucose, in contrast to the mannan from P. mutabilis ATCC 31014, which contained only trace amounts...
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Hyperfine Structure Study of Several Lines of207Pb I
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Structure-Activity Relationships in Two-Electron Reduction of Quinones
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