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Search results for: THIN FILM MICROEXTRACTION
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Test-supported numerical analysis for evaluation of the load capacity of thin-walled corrugated profiles
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ALD thin ZnO layer as an active medium in a fiber-optic Fabry–Perot interferometer
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Quality increase for single-welded joints of thin-walled structures by means of simulation modelling
PublicationThe Simulation calculation module and the SolidWorks software package have helped to define the optimal shape and dimensions of single-welded joints which may serve the basis for calculating the process parameters of welding. Having compared the models with different weld cross-sections the authors have defined that the weld height and width do not significantly affect the stress concentration, and the stress concentration and...
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Distortional buckling of composite thin-walled columns of a box-type cross section with diaphragms
PublicationDistortional buckling of axially compressed columns of box-like composite cross sections with andwithout internal diaphragms is investigated in the framework of one-dimensional theory. The channel membersare composed of unidirectional fibre-reinforced laminate. Two approaches to the member orthotropic materialare applied: homogenization based on the theory of mixture and periodicity cells, and homogenization basedon the Voigt–Reuss...
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Graphene oxide, reduced graphene oxide and composite thin films NO2 sensing properties
PublicationA graphene oxide (GO), reduced graphene oxide (RGO) and poly(3,4-ethylenedioxytiophene)- reduced graphene oxide (PEDOT-RGO composite) gas sensors were successfully fabricated using an electrodeposition method. The electrodeposition was carried out in aqueous GO dispersions. In order to obtain RGO and PEDOT-RGO, the electrochemical reduction of GO and PEDOT-GO was carried out in 0.1 M KCl at constant potential of −0.85 V. The GO, RGO...
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Graphene oxide, reduced graphene oxide and composite thin films NO2 sensing properties
PublicationA graphene oxide (GO), reduced graphene oxide (RGO) and poly(3,4-ethylenedioxytiophene)-reduced graphene oxide (PEDOT-RGO composite) gas sensors were successfully fabricated using an electrodeposition method. The electrodeposition was carried out in aqueous GO dispersions. To obtain RGO and PEDOT-RGO, the electrochemical reduction of GO and PEDOT-GO was carried out in 0.1 M KCl at a constant potential of −0.85 V. The GO, RGO and PEDOT-RGO...
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SURFACE AND SPECTROSCOPIC PROPERTIES OF 1,8-DIAZAFLUOREN-9-ONE IN TITANIUM DIOXIDE THIN FILMS
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Cuprous Oxide Thin Films Implanted with Chromium Ions - Optical and Physical Properties Studies
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Wear of Ultra-thin DLC or Tungsten-modified DLC Coatings under Reciprocating Sliding
PublicationIn the paper results are presented from tests in reciprocating sliding of self mated specimens of DLC and tungsten modified DLC coatings on stainless steel substrate. The contact geometry chosen for the research task was ball on flat. The contacts were lubricated either with distilled water or medical saline solution. Results are presented with regard to wear resistance as a function of material type and lubricant used.
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Analysis of magnetic field distribution inside ferromagnetic thin shells during degaussing process
PublicationAnalysis of the demagnetization of a large ferromagnetic object like a ship, was conducted. The approximate mathematical model in the form of a long cylindrical shell of constant magnetic permeability was applied. The discrete degaussing winding was assumed and the current density and magnetic flux density distribution in the ferromagnetic shell wall were determined. Based on the frequential and temporal analysis the recommended...
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Deposition of thin titanium–copper films with antimicrobial effect by advanced magnetron sputtering methods
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The Problems of Application of PVD/CVD Thin Hard Coatings for Heavy-Loaded Machine Components
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Second and third harmonic nonlinear optical process in spray pyrolysed Mg:ZnO thin films
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Enhancement of defects induced optical nonlinearity in Al: ZnO thin films by electron beam
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ALD thin ZnO layer as an active medium in a fiber-optic Fabry-Perot interferometer
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A simple and efficient hybrid discretization approach to alleviate membrane locking in isogeometric thin shells
PublicationThis work presents a new hybrid discretization approach to alleviate membrane locking in isogeometric finite element formulations for Kirchhoff–Love shells. The approach is simple, and requires no additional dofs and no static condensation. It does not increase the bandwidth of the tangent matrix and is effective for both linear and nonlinear problems. It combines isogeometric surface discretizations with classical Lagrange-based...
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The microstructure effect on the electrical and optical properties of undoped and Sr-doped SmCoO3 thin films.
PublicationW pracy przedstawiono elektryczne i optyczne właściwości niedomieszkowanego i domieszkowanego Sr SmCoO3 cienkich filmów. Gęste i przezroczyste filmy o grubościach 80-100nm były przygotowane na szafirze metodą nanoszenia wirowego ciekłych polimerów. Filmy były syntezowane w temperaturach od 500 do 800C co umożliwiło otrzymanie różnych mikrostruktur. Elektryczne właściwości filmów były mierzone w funkcji temperatury. Domieszkowanie...
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The effect of nonlinear restraint on torsional buckling and post-buckling behaviour of a thin-walled column
PublicationW pracy rozważa się wyboczenie skrętne i zachowanie pokrytyczne osiowo ściskanego swobodnie podpartego pręta cienkosciennego o przekroju otwartym ze sprężytą nieliniową podporą w środku rozpietości. Rozwiązanie problemu wyznaczono za pomocą metody małego parametru. W przykładzie numerycznym wyznaczono siłę krytyczną i ścieżkę początkowego zachowania pokrytycznego dwuteowego pręta z podporą sprężystą o charakterystyce składającej...
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Copper oxide thin films as components for heterojunction formation with TiO2 for photocatalytic CO2 reduction
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Application of the LPE-Grown LuAG: Ce Film/YAG Crystal Composite Thermoluminescence Detector for Distinguishing the Components of the Mixed Radiation Field
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Michał Sobaszek dr hab. inż.
PeopleMichał Sobaszek was born in Gdansk in 1984. In the summer of 2009, he received a Master degree in Materials Engineering at Gdansk University of Technology. Currently, he is an Assistant Professor at the Faculty of Electronics at the Gdańsk University of Technology. In 2018 he was honoured with the scholarship for the outstanding young researches by the Minister of Science and Higher Education of Poland. For more than 7 years, he...
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Marcin Perzanowski dr inż.
PeopleHello, I work in the Department of Magnatic Materials and Nanostructures in the Institute of Nuclear Physics Polish Academy of Sciences in Kraków, Poland. My current research is focused on: (1) exchange bias in multilayers and nanostructures, (2) supermagnetic effects in low-dimensional materials, (3) perpendicular magnetic anisotropy in thin films and nanostructures. Collaborations, comments, and suggestions are welcomed! If...
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Tomasz Mikulski dr hab. inż.
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Development of a vortex-assisted switchable-hydrophilicity solvent-based liquid phase microextraction for fast and reliable extraction of Zn (II), Fe (II), Pb (II), and Cd (II) from various baby food products
PublicationThis manuscript describes the development of a novel liquid phase microextraction (LPME) method for the extraction and determination of Zn (II), Fe (II), Pb (II), and Cd (II) in various infant/baby food and supplements products. The method is based on vortex-assisted extraction combined with a switchable-hydrophilicity solvent (SHS) sample preparation. The SHS, which undergoes reversible phase changes triggered by pH change, enables...
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Ultrasound-Assisted Dispersive Liquid-Liquid Microextraction Using Deep Eutectic Solvents (DESs) for Neutral Red Dye Spectrophotometric Determination
PublicationDeep eutectic solvents (DES), which have low toxicity and are low cost, biodegradable, and easily synthesized, were used for the extraction of neutral red (NR) dye before its spectrophotometric analysis. DES, containing choline chloride as a hydrogen bond acceptor and phenol as a hydrogen bond donor with a molar ratio of 1:2, was used for the extraction of NR dye from aqueous media. The possible interaction of different DESs with...
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Rapid and sensitive determination of acrylamide in potato crisps using reversed-phase direct immersion single drop microextraction-gas chromatography
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Salt saturated single drop microextraction of gold from water samples and its determination by graphite furnace atomic absorption spectrometry
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Determination of selenium by X-ray fluorescence spectrometry using dispersive solid-phase microextraction with multiwalled carbon nanotubes as solid sorbent
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Czesław Kazimierz Szymczak prof. dr hab. inż.
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<title>An optical low-coherence system for 2-dimensional visualization of thin polymer layers</title>
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The Luminescence of 1,8-Diazafluoren-9-One/Titanium Dioxide Composite Thin Films for Optical Application
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The Thin-Layer Microchromatography (μTLC) and TLC–FID Technique as a New Methodology in the Study of Lubricating Oils
PublicationThis paper concerns the possibility of using TLC coupled with a flame ionization detector (FID) and micro-TLC (μTLC) as precursors for microfluidized devices of analytical techniques to identify and determine the presence and content of the petroleum/vegetable oil base in the lubricating oils applied in cutting devices (chainsaws). This research is related to the problem of ensuring, in compliance with the requirements of environmental...
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CdS thin films obtained by thermal treatment of cadmium(II) complexprecursor deposited by MAPLE technique
PublicationCienkie warstwy kompleksu [Cd{SSi(O-But)3}(S2CNEt2)]2 zostały osadzone na podłożach Si przy użyciu techniki MAPLE (ablacja laserowa z zamrożoną matrycą). Otrzymanie warstw CdS było możliwe dzięki zastosowaniu obróbki termicznej podłoży z naniesionym prekursorem. Powierzchnia filmów była analizowana pod kątem morfologii przy użyciu mikroskopii sił atomowych (AFM) oraz pomiarów elipsometrycznych (SE).
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Preparation and characterization of collagen/chitosan/hyaluronic acid thin films for application in hair care cosmetics
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Compression and Fatigue Testing of High-Strength Thin Metal Sheets by Using an Anti-Buckling Device
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Design of polymeric thin films with nanovolcanoes for trapping hydroxyapatite nanoparticles to promote or inhibit cell proliferation
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The study of salting-out thin-layer chromatography and their application on QSRR/QSAR of some macrolide antibiotics
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Quantitative determination of diazepam, nitrazepam and flunitrazepam in tablets using thin-layer chromatography–densitometry technique
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Small signal admittance spectroscopy applied for extraction of charge carrier mobility in thin organic layers
PublicationPraca przedstawia nowy sposób wyznaczania ruchliwości nośników ładunku w cienkich warstwach organicznych w oparciu o pomiary widm małosygnałowej admitancji.
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Circular Dichroism Imaging: Mapping the Local Supramolecular Order in Thin Films of Chiral Functional Polymers
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The Physicochemical, Antioxidant, and Color Properties of Thin Films Based on Chitosan Modified by Different Phenolic Acids
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Highly efficient conversion of waste plastic into thin carbon nanosheets for superior capacitive energy storage
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Determination of polyphenolics in extracts of Potentilla species by high‐performance thin‐layer chromatography photodensitometry method
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Chromatic monitoring technique for thickness measurementof thin transparent films.IV Workshopon Atomic and Molecular Physics.
PublicationW pracy opisano nową technikę monitorowania grubości cienkich warstw podczas procesu ich syntezy. Jest to optyczna metoda oparta na zdegenerowanej analizie widmowej tzw. modulacji chromatycznej. Umożliwia ona precyzyjny ciągły pomiar zmian grubości wzrastających warstw stosowanych w optyce.
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Structural investigations of the LTO:Cu thin films
Open Research DataLithium titanate (Li1+xTi2-xO4) doped with Cu2+ ions was synthesized by sol-gel processing method. The structure was characterized by X-ray Diffraction (XRD). All samples revealed presence of LTO spinel phase. X-ray pattern of undoped LTO was free of any impurities and other crystal phases. Similarly, samples with low amount of copper dopant (x = 0.05...
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Ultrasound-assisted deep eutectic solvent-based liquid–liquid microextraction for simultaneous determination of Ni (II) and Zn (II) in food samples
PublicationA new approach was developed for the simultaneous pre-concentration and determination of Ni (II) and Zn (II) in food samples. This method is based on ultrasound-assisted liquid–liquid micro extraction using hydrophobic deep eutectic solvent (DES) and 1,10-phenanthroline as chelating agent. The effect of several parameters, such as pH, selection and volume of DES, amount of chelating agent, time of sonication and centrifugation,...
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Determination of methylcyclopentadienyl-manganese tricarbonyl in gasoline and water via ionic-liquid headspace single drop microextraction and electrothermal atomic absorption spectrometry
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A rapid spectrofluorimetric method for the determination of malondialdehyde in human plasma after its derivatization with thiobarbituric acid and vortex assisted liquid–liquid microextraction
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Technika mikroekstrakcji do fazy stacjonarnej (SPME) w badaniach analitycznych żywności. Solid-phase microextraction (SPME) in food analysis-review
PublicationW pracy przedstawiono studium literaturowe dotyczące zastosowania technik SPME, jako metody izolacji i wzbogacania zanieczyszczeń, związków zapachowych i smakowych oraz dodatków funkcjonalnych z próbek żywności. Przedstawiono także czynniki wpływające na efektywność procesu mikroekstrakcji do fazy stacjonarnej, wybrane chromatogramy obrazujące ten wpływ oraz tabelaryczne zestawienie przykładów zastosowań SPME do badań żywności.
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Load-carrying capacity of axially loaded concrete-filled steel tubular columns made of thin tubes
PublicationAn experimental investigation was conducted on 30 CFST columns. An influence of the following factors on load-carrying capacity of the investigated columns was analyzed: the column slenderness (l1 = 42, l2 = 27 and l3 = 15), the tube thickness (the reinforcement ratio was equal to 4% or 6%), the way of applying the load to CFST columns (through the concrete core or through the entire cross-section), the bond strength between a...