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Wyniki wyszukiwania dla: STANISŁAW
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Results of nanoindentation test to calculate residual stress in an eyelet of undercarriage drag strut after laser treatment
Dane BadawczeIn order to determine the residual stress in the laser-processed an eyelet of undercarriage drag strut, a nanoindentation test was performed before and after stress relief annealing. For this purpose, after the hardness test, the sample was subjected to stress relief annealing at 270 °C for 2 hours. Annealing was performed in a vacuum furnace. Hardness...
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Results after grinding C45 steel
Dane BadawczeThe database contains results from nanoindenter, scanning microscope and also X-ray diffractometer. To determine the residual stresses and the size of the crystallites in the ferrite grains in the grinded surface layer, the Williamson Hall analysis of the X-ray diffraction patterns was performed. XRD diffraction patterns were also used to perform a...
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Results of nanoindentation, XRD and microscopic studies of bacterial cellulose
Dane BadawczeThe archive contains the results of research on BNC bacterial biocellulose, which was modified in two ways. When BNC was synthesized, it was subjected to in situ modification involving the addition of hyuloronic acid to the bacterial medium. The second way of ex situ modification consisted of soaking the BNC in water and then convectionally drying it...
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SEM examination of surface layer of C45 steel after grinding on defferent depth
Dane BadawczeFerrite examination for the medium carbon structural steel with low content of Mn, Si, Cu, Cr and Ni after its grinding to a depth of 2 µm, 8 µm, 14 µm and 20 µm, at constant wheel circumferential speed of vs = 25 m/s and constant feed rate vft = 1 m/min. It was shown that the grinding of C45 steel causes strong work hardening of ferrite in surface...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,75 V at 241 mA. Sample 24, run #3.
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,75 V and discharged to 10 mV by constant current 241 mA, experiment run #3The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,75 V at 241 mA. Sample 24, run #5.
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,75 V and discharged to 10 mV by constant current 241 mA, experiment run #5.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,8 V at 241 mA. Sample 24, run #1.
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,8 V and discharged to 10 mV by constant current 241 mA, experiment run #1.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,0 V at 250 mA. Sample 24.
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,0 V and discharged to 10 mV by constant current 250 mA. Last experiment with sample 24The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,5 V at 180 mA. Sample 24
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,5 V and discharged to 10 mV by constant current 180 mA. The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface emission....
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 80 mA. Sample 41.
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 80 mA. Sample 41.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,75 V at 241 mA. Sample 24, run #2.
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,75 V and discharged to 10 mV by constant current 241 mA, experiment run #2The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,0 V at 250 mA. Sample 23, run #1.
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,0 V and discharged to 10 mV by constant current 250 mA. Sample 23, experiment run #1.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,8 V at 241 mA. Sample 24, run #2.
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,8 V and discharged to 10 mV by constant current 241 mA, experiment run #2.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,8 V at 241 mA. Sample 24, run #3.
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,8 V and discharged to 10 mV by constant current 241 mA, experiment run #3.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,9 V at 241 mA. Sample 24, run #1.
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,9 V and discharged to 10 mV by constant current 241 mA, experiment run #1.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,5 V at 241 mA. Sample 24
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,5 V and discharged to 10 mV by constant current 241 mA. The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface emission....
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,0 V at 250 mA. Sample 23, run #2.
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,0 V and discharged to 10 mV by constant current 250 mA. Sample 23, experiment run #2.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,5 V at 80 mA. Sample 24
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,5 V and discharged to 10 mV by constant current 80 mA. The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface emission....
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,75 V at 241 mA. Sample 24, run #4.
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,75 V and discharged to 10 mV by constant current 241 mA, experiment run #4.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,75 V at 241 mA. Sample 24, run #1.
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,75 V and discharged to 10 mV by constant current 241 mA. The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface emission....
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,9 V at 241 mA. Sample 24, run #2.
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,9 V and discharged to 10 mV by constant current 241 mA, experiment run #2.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,5 V at 301 mA. Sample 24
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,5 V and discharged to 10 mV by constant current 301 mA. The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface emission....
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 160 mA. Sample 41.
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 160 mA. Sample 41.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,5 V at 120 mA. Sample 24
Dane BadawczeDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,5 V and discharged to 10 mV by constant current 120 mA. The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface emission....
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Optical properties of tellurium dioxide thin films
Dane BadawczeTeO2 and TeO2 doped by Eu thin films manufactured by magnetron sputtering method were measured by optical spectroscopy. Metallic Te target and Te-Eu mosaic target with diameter of 50.8 mm were sputtered for about 45 min in argon-oxygen atmosphere what resulted in 300 nm film thickness deposition. The pressure in the chamber was below 0.2 Pa and substrate...
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Optical measurements of lithium titanate sol-gel derived thin films
Dane BadawczeNanocrystalline thin films with 800 nm thickness were prepared by sol–gel method. To examine the influence of the annealing time on as-prepared films crystallization, the coatings were heated at 550 °C for 10, 20 and 80 h. On the basis of transmission characteristic optical properties were calculated. It was found that transmission through the thin...
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TEM imaging of Ag-Au nanoalloys
Dane BadawczeThe nanostructures of AuAg nanoalloys were prepared by sequential sputtering of metal thin layers (Au/Ag or Ag/Au) followed by annealing under 550 Celsius degree in an argon atmosphere. The basic single layer thickness was usually ca. 3 nm. For investigations two samples wih 50% Au and 50% Ag were selected and samples 1/3 Ag - 2/3 Au and 2/3 Ag - 1/3...
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Depth profile of the gold-silver bimetallic structures
Dane BadawczeSilver and gold bimetallic layers were deposited on a silicon substrate by magnetron sputtering method. Both, Au and Ag layers had 3 nm of thickness. That prepared nanostructures were measured by XPS method. To obtain a depth profile of chemical composition, an Argon ion (Ar+) gun was used for etching surface of sample. Each cycle of etching takes 30...
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Chemical composition of tellurium oxides thin films deposited by magnetron sputtering method
Dane BadawczeThin films were prepared by radio frequency reactive magnetron sputtering technique. Metallic Te target was sputtered for about 45 min in argon-oxygen atmosphere what resulted in 300 nm film thickness deposition. The pressure in the chamber was below 0.2 Pa and substrate was heated at 200 °C. The distance between sputtered target and the Corning 1737...
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Depth profile of the chemical composition of the Au-Ag multilayers
Dane BadawczeSilver and gold multilayers were deposited on a silicon substrate by magnetron sputtering method. Both type, Au and Ag thin films had 2 nm of thickness. Totally structure had thickness of 6 nm (Au-Ag-Au). That prepared multilayers were measured by XPS method. To obtain a depth profile of chemical composition, an Argon ion (Ar+) gun was used for etching...
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SEM analysis of the TiO2 layers deposited on a FTO substrates
Dane BadawczeTitanium dioxide layers were deposited on a FTO conducting glass by sol-gel method. For sol gel synthesis butoxy titanium and ethanol were used as a reagents. Samples were sintered in a furnace at temperature of 600 deg. SEM measurements were performed by FEI Quanta FEG250 microscope. SEM images of a cross-section of samples exhibit a porous structures...
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Interface diffusion between metallic nanoparticles and silicon substrate
Dane BadawczeInterface diffusion between metallic nanoparticles and silicon substrate was detected by EDX method. Metallic nanostructures were manufactured by thermal annealing of thin films. Gold and silver nanostructures were chosen for measurements. Samples were annealed for 15 and 60 minutes at 550 deg.
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XPS study of the TiO2-WO2 composites
Dane BadawczeValence state of W and Ti was measured in a TiO2-WO3 composites with a various composition.Powder samples of pure titanium dioxide, tungsten oxide and mix of 50% titanium oxide and 50% od tungsten oxide were measured. Oxides were annealed at the temperature in the range of 300 Celsius degree up to 900 deg. Measurements were performed by XPS UHV Omicron...
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XPS measurements of the iron elements covered by chromium
Dane BadawczeAnticorrosive coatings are an important issue in modern materials engineering. One of the most commonly used, for that coating materials, is chrome. Three metal elements were measured, named as Turcja, WB Tech and Nomet. Names were given according to producer of elements. XPS measurements of the Cr 2p region give an ansver concering on surface chemical...
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XPS investigations of tge tin/tin oxides - CNT composites
Dane BadawczeThe composite of tin/tin oxide nanoparticles with graphene oxide and CMC based on laser ablation technique as an electrode material for energy storage devices were manufactured. The material exhibited a three-dimensional conducting graphene oxide network decorated with tin or tin oxide nanoparticles. The presence of tin/tin oxide in composites was...
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TEM and EDX study of the Al2O3 ultra thin films
Dane BadawczeThe ultra-thin layers of Al2O3 were deposited on a silicon substrates. The method of atomic layer deposition (Beneq TFS 200 ALD system) was chosen as the proper method of dielectric layer deposition. This method provides precise thickness control down to a single atomic layer. The precursors used were trimethylaluminum (Sigma-Aldrich) and purified water....
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Structural analysis of the tellurium dioxide thin films
Dane BadawczeTeO2 thin films were deposited by magnetron sputtering method. After deposition, amorphous samples were annealed at various temperatures. Influence of annealing temperature on a presence of crystalline phase was investigated.
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Optical properties of MnO-B2O3 based glass
Dane BadawczeMnO-B2O3 based glass with Au nanoparticles samples were annealing for a various time (in a range of 24-96 hours) at various temperatures (from 340 up to 350 deg.). Presence of silver nanoparticles was detected by UV-VIS measurements. On the basis of change optical bandgap, Ag NPs was detected.
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Valence state of Manganium in a MnCoO ceramics
Dane BadawczeManganium -cobalt based ceramics materials were produced by solid state reaction and sintred in a furnance in air atmosphere for 20h. Annealing temperature was 600 Celsius degree. For investigations a series of samples, with a various composition was chosen: MnCoO, Mn, Co2O and Mn2CoO. In order to determine valence states of the Mn, X-Ray photoemission...
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Reduction of the strontium titanate doped by Ytrium ceramics observed by X-ray photoemission spectroscopy method
Dane BadawczeYtrium-doped strontium titanate (YSTF) ceramics materials were manufactured by three various methods: 1) standard solid-state reaction method from Y2O3 (Sigma Aldrich, 99,9%), TiO2 (Sigma Aldrich, 99%) and SrCO3 (Sigma Aldrich,98%), 2) Pechini method, 3) wet method.
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Depth XPS profile of vanadium pentoxide
Dane BadawczeVanadium pentoxide sample was manufactured by sol-gel method and deposited on a substrate by spin coating technique. To determine depth profile of chemical composition of thin film, etching by Argon ion gun was used. Thin film was etched three times. Chemical composition was measured by XPS method.
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XPS analysis of strontium titanate ceramics
Dane BadawczeThe chemical composition of the strontium titanite doped with yttrium and iron ceramic samples was investigated. Samples of Y0.07Sr0.93Ti0.8Fe0.2 were prepared by solid phase reaction and sintered for 24 and 48 hours. Chemical composition was measured by UHV OmicronNanotechnology XPS system. The analysis confirmed the chemical composition of the ceramics...
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Sol-gel derived TeO2:RE powders
Dane BadawczeTellurium dioxide powders doped by Europium or Dysprosium were prepared by sol-gel method. Samples were annealed in ix of Ar and O2 atomosphere at 600 degrees. Presence of rare earth dopants and Te4+ phase was confirmed by X-Ray Photoemission Spectroscopy method (XPS). For XPS measurements samples with 1 atomic % and 5 atomic % of dopand were selected.
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Plasmon resonance in gold-silver nanoalloys
Dane BadawczeSurface plasmon resonance (SPR) can lead to improve or formation a new linear or nonlinear optical phenomena. Especially it can enhance a light emission from luminescence materials. The presence of metal nanostructures or nanoparticles is necessary to excitation of the SPR. It is well known that gold and silver nanostructures exhibit plasmon resonance...
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Morphology of the gold nanoislands
Dane BadawczeDewetting of the thin metallic films leads to formation of an isolated islands. morphology of nanostructures was measured by SEM microscope. Thin gold films with a thickness of 1.2 nm, 1.5 nm and 3.4 nm were anealed at 550, 600 and 650 Celcius degress.
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Investigation of plasmon resonance in a silver nanoparticles
Dane BadawczeSilver nanostructures were prepared on borosilicate glass (Corning 1737F) substrates. Thin Ag films (1–9 nm thickness) were deposited using a table-top dc magnetron sputtering coater (EM SCD 500, Leica) in pure Ar plasma (argon, Air Products 99.999%). The Ag target was of 99.99% purity, the rate of layer deposition was about 0.4 nm·s−1, and the incident...
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SEM inwestigation of the silver nanostructures
Dane BadawczeSilver thin films with a thickness of 1nm, 3nm, 5nm, 7nm and 9nm were deposited by a table-top magnetron sputtering unit in a pure argon plasma from a high-purity silver target. Silicon wafers was used as a substrates. As-deposired films were annealed in Ar atmosphere at 550 Celsius degree for 15 minutes.As a result of annealing, Ag nanostructures formed...
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XPS measurements of the Fe-Pb-Si based glass
Dane BadawczeGlass samples with nominal compositions of xFe2O3-(50-x)PbO–50SiO2, where x = 12.5, 15, 17.5 (mol%) were prepared. Analytical grade substrates were used: Fe2O3, SiO2, and PbO. The appropriate amounts of reagents were mixed in an agate mortar. The powders obtained were melted in porcelain un-enamelled crucibles in an electric furnace at a temperature...
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XPS measurements of the Fe-Bi based glass
Dane BadawczeFe-Si-O and Fe-Si-Pb-O glass was measured by XPS method. The influence of Pb dopand on the glass structure, including the valence of iron, was investigated. The influence of the annealing temperature on the behavior of iron in glass was also investigated. Studies have confirmed the mixed valence of iron in glasses and a high proportion of metallic Fe.
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Analysis of the chemical composition of MnO-B2O3 glass
Dane BadawczeStructural and thermal properties of xMnO−(100−x)B2O3 (where x = 40, 50 and 60 mol%) glass samples have been investigated with the employment of various techniques. Fourier transform infrared spectroscopy results revealed the influence of MnO on glass matrix. Decrease of B–O bond-related band intensities has been observed. MnO addition was found to...