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Wyniki wyszukiwania dla: c=p-p systems
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General route for the synthesis of terminal phosphanylphosphido complexes of Zr(IV) and Hf(IV): Structural investigations of the first zirconium complex with a phosphanylphosphido ligand
PublikacjaReactions of R2P-P(SiMe3)Li with [Cp2MCl2] (M = Zr, Hf) in hydrocarbons yield the related terminal phosphanylphosphidocomplexes [Cp2M(Cl){(Me3Si)P-PR2-jP1}] (R = iPr and tBu). The solid state structures of [Cp2M(Cl){P(SiMe3)-PiPr2-jP1}] (M = Zr, Hf) were established by single crystal X-ray diffraction studies. The phosphido-P atoms adopt almost planar geometries and the phosphanyl P atoms adopt pyramidal geometries. The reaction...
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O centrum
PublikacjaPerypetie urbanistyczne Gdańska
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Phosphanylphosphido and phosphanylphosphinidene complexes of zirconium(IV) supported by bidentate N,N ligands
PublikacjaPhosphanylphosphido complexes of zirconium, [NacNacZrCl2(η2-R2P–PSiMe3)] (R = t-Bu, i-Pr), were synthesized in the reaction of R2P–P(SiMe3)Li·nTHF (R = t-Bu, i-Pr) with a β-diketiminate complex, [NacNacZrCl3], in toluene. Elimination of Me3SiCl from [NacNacZrCl2(η2-R2P–PSiMe3)] provided the phosphanylphosphinidene complexes [NacNacZrCl(η2-R2P–P)] (R = t-Bu, i-Pr). Moreover, the reaction of [NacNacZrCl2(η2-R2P–PSiMe3)] with R2P–P(SiMe3)Li·nTHF...
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Reactivity of Diimido Complexes of Molybdenum and Tungsten towards Lithium Derivatives of Diphosphanes and Triphosphanes
PublikacjaThe reaction of R2P–P(SiMe3)Li (R = tBu, iPr) with the diimido molybdenum complex [(ArN)2MoCl2·dme] (Ar = 2,6-iPr2C6H3; dme = 1,2-dimethoxyethane) yielded the side-oncoordinated phosphanylphosphinidene anionic complexes [(2,6-iPr2C6H3N)2Mo(Cl)(η2-P=PR2)]– (7Mo, 8Mo). The thermal decomposition of [(2,6-iPr2C6H3N)2M(Cl)(η2-P=PR2)]–[M = Mo (7Mo), W (8W)] to [(2,6-iPr2C6H3N)2M(Cl)(1,2-η-tBu2P=P–PtBu2)] [M = Mo (3Mo), W (3W)] was investigated...
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Polska, Niemcy czy Gdańsk?
PublikacjaTożsamość etniczno-kulturowa miasta
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Application of NIR and Raman Spectroscopy in Biotechnology
PublikacjaStudium Press LLC, U.S.A.
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Perceived Awareness of Clozapine associated with SocioDemographic status, clinical, and side effect profile among patients from Mental Health Hospital, Taif, Saudi Arabia
Publikacjahttps://indianmentalhealth.com/pdf/2022/vol9-issue4/7-OR3.pdf
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Application of Structural Control Systems for the Cables of Cable-Stayed Bridges: State-of-the-Art and State-of-the-Practice
PublikacjaStay cables are one of the key elements of cable-stayed bridges and are characterized by lightweight, low inherent damping, and high flexibility. They are continuously subjected to small-to large-amplitude vibrations due to various types of dynamic loads that may, in the long term, cause fatigue and fracture problems for the cable system, and may eventually compromise the safety of cable-stayed bridges. Thus, several countermeasures...
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The reactivity of 1,1-dichloro-2,2-di-tert-butyldiphosphane towards lithiated metal carbonyls: a new entry to phosphanylphosphinidene dimers
PublikacjaReactions of [Cp*(OC)3M]Li (Cp* = C5Me5, M = Mo, W) towards t-Bu2P–PCl2 lead to the formation of phosphanylphosphinidene dimers [Cp*(OC)3M(η2-t-Bu2P–P)]2 in fairly good yields. The formation of a tetraphosphorus ligand proceeds via reductive dimerization of t-Bu2P–P units. NMR, X-ray investigations and DFT calculations show that the resulting tetraphosphorus ligand has a structure of dication t-Bu2P+=P–P=P+t-Bu2.
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The new diphosphanylphosphido complexes of tungsten(VI) and molybdenum(VI). Their synthesis, structures and properties
PublikacjaWe report on the reactivity of R2P–P(Li)–PR’2 (R = tBu, iPr, R’ = NEt2, iPr) towards diimido complexes [(dippN)2MCl2·dme] (M = Mo, W and dipp = 2,6-iPr2C6H3). A series of new complexes with diphosphanylphosphido ligands R2P–P–PR’2 were isolated. The solid-state structures of [(dippN)2M(Cl)(1,2-η-iPr2P–P– PiPr2)] (2Mo and 2W) and [(dippN)2M(Cl){1,2-η-tBu2P–P–P(NEt2)2}] (3Mo and 3W) were established by single-crystal X-ray diffraction...
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Kod Carstena? Symbolika detali na gmachach Politechniki Gdańskiej
PublikacjaZnaczenie wystroju architektonicznego gmachów PG
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Założenia pierścieniowe w strukturze urbanistycznej miast polskich
PublikacjaOmówienie pracy doktorskiej Leszka Bugalskiego
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Charakterystyka systemów opadowych w Polsce
PublikacjaCharakterystyka systemów opadowych w Polsce
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Serum neurotrophin-3 and neurotrophin-4 levels are associated with asthma severity in children
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Conjugate of Enkephalin and Temporin Peptides as a Novel Therapeutic Agent for Sepsis
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Carbon catalysts from pine cones – Synthesis and testing of their activities
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Corrigendum to “Blood pressure disturbances and endothelial dysfunction markers in children and adolescents with type 1 diabetes” [Atherosclerosis 237 (2014) 129–134]
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Magnetic structure and properties of the S=5/2 triangular antiferromagnet - NaFeO2
PublikacjaWłaściwości magnetyczne związku NaFeO2 badane były za pomocą techniki dyfrakcji neutronowskiej i poprzez pomiar podatności magnetycznej.
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Magnetic structure and properties of theS=5∕2triangular antiferromagnetα−NaFeO2
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TH-D-BRB-06: Assessment of Proton Beam In-Vivo Dose Verification by Directly Comparing Doses Measured in Tissue-Equivalent Polymer Gels to Proton-Activated Positron-Emission Distributions in the Gels Post Irradiation
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Accuracy Analysis of Measurements in Electrochemical Biosensing
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Metrological analysis of surface quality aspects in minimum quantity cooling lubrication
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Positron Annihilation Studies of Silicon Oxides and Oxygen Precipitates in Silicon
PublikacjaTechniki pozytonowe dają możliwości badania defektów i zmian strukturalnych nie obserwowanych innymi metodami. W tej pracy zastosowano 3 różne techniki pozytonowe do badania zmian strukturalnych i tworzenia wydzieleń SiOx w krzemie.
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Structural studies of bismuth nanocrystals embedded in SiO2 or GeO2 matrices.
PublikacjaW wyniku wygrzewania w atmosferze wodoru szkieł bizmutowych i germanowych otrzymano warstwę nanogranul bizmutu w otoczeniu amorficznej matrycy oraz powierzchniową warstwę bizmutowych granul. Grubość i struktura tak otrzymanych warstw silnie zależy od czasu i temperatury redukcji.
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Modelling and analysis of medium frequency transformers for power converters
PublikacjaThe evolutions in power systems and electric vehicles, related to the economic opportunities and the environmental issues, bring the need of high power galvanically isolated DC-DC converter. The medium frequency transformer (MFT) is one of its key components, enabled by the increasing switching frequency of modern power semiconductors like silicon carbide transistors or diodes. The increased operating frequency offers small...
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Experiments and Analysis of the Limit Stresses of a Magnetorheological Fluid
PublikacjaPaper presents the results of a rheological test of a commercial magnetorheological (MR) fluid (MRF-132DG). The researchincludes the problem of measuring and interpreting limit stresses under conditions close to the magnetic saturation of the fluid. Fourdifferent limit stresses were determined, two related to the yield point and two related to the flow point. Methods for determining limitstresses, especially due to excitation...
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Wokół pewnego cytatu. Zbiór artykułów (książka)
PublikacjaKsięga jubileuszowa dedykowna Profesorowi Janowi Wawrzyńczykowi
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Adhezyjny opatrunek silikonowy, zawierający suchy wyciąg z cebuli i heparynę drobnocząsteczkową oraz sposób jego otrzymywania
PublikacjaPatent UPRP, PL. 220765
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The culture of excellence and its dimensions in higher education
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Computational aspects of greedy partitioning of graphs
PublikacjaIn this paper we consider a variant of graph partitioning consisting in partitioning the vertex set of a graph into the minimum number of sets such that each of them induces a graph in hereditary class of graphs P (the problem is also known as P-coloring). We focus on the computational complexity of several problems related to greedy partitioning. In particular, we show that given a graph G and an integer k deciding if the greedy...
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Validation and modification of HPLC method for monitoring acetaminophen plasma concentrations in patients with chronic pancreatitis
PublikacjaBackground. Pancreatitis is the inflammation of the pancreas. The infl ammation may occur suddenly and resolve in a few days with the treatment in case of acute pancreatitis (AP). Chronic pancreatitis (CP) is a persistent inflammation of the pancreas that results in irreversible morphological changes and impairment of both exocrine and endocrine functions. Abdominal...
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Architektura a dekonstrukcja. Przypadek Petera Eisenmana i Bernarda Tschumiego
PublikacjaArchitecture and Deconstruction Case of Peter Eisenman and Bernard Tschumi Introduction Towards deconstruction in architecture Intensive relations between philosophical deconstruction and architecture, which were present in the late 1980s and early 1990s, belong to the past and therefore may be described from a greater than...
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Skills Mismatch in the Context of Technological Change
PublikacjaThis dissertation examines the impact of technological change (TC) on skills and competences and how higher education’s role has changed along the way. Quantitative research was conducted to reveal the perceptions of students and employers in Poland on the relevance of particular skills in an ICT based economy. The results of this research show that there is generally a rather insignificant discrepancy in these perceptions....
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Dom gdański
PublikacjaTradycyjne gdańskie kamienice i ich późniejsze reminescencje
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Bibliografia publikacji pracowników Archiwum Państwowego w Lublinie za lata 2008–2016 z uzupełnieniami za lata 2000–2008.
PublikacjaBibliografia publikacji pracowników Archiwum Państwowego w Lublinie
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Neurotrophic factors in human milk in early lactation and the effect of Holder and microwave pasteurization on their concentrations
PublikacjaObjective: The objective of this study was to determine the level of brain-derived neurotrophic factor (BDNF) and glial cell line-derived neurotrophic factor (GDNF) in human milk in the first two weeks of breastfeeding and compare of the effects of Holder pasteurization (HoP, 62.5°C, 30 minutes) and microwave pasteurization (MP) at constant temperature (62.5°C) on the concentraion of both neurotrophic factors (NFs). Methods: Concentration...
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Sulfurization of phosphanylphosphinidene ligand: Access to phosphinothioyltrithiophosphonato platinum(II) complexes
PublikacjaThe reactivity of phosphanylphosphinidene Pt(0) complexes [DppePt(η2-P–PtBu2)] (1) and [(pTol3P)2Pt(η2-P–PtBu2)] (2) toward sulfur was studied. Reactions of 1 and 2 with an excess of sulfur led to the formation of the first transition metal complexes 3 and 4 with phosphinothioyltrithiophosphonato ligands with the formula [tBu2P(=S)–P(=S)S2]2-. In contrast to previous reports on the phosphanylphosphinidene moiety sulfurization,...
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O miejscu
PublikacjaPrzyczyny i konsekwencje lokalizacji Gdańska w określonej przestrzeni
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Overview of new product development strategies and models
PublikacjaMotivation: The motivation for the overview presented in this article is to provide a starting point for considering whether existing new product development methodology and its level of detail allows product teams to develop high-quality and business-effective product concepts. Aim: The aim of this article is recognise the current state of research into new product development methodology and to present the strategies...
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Structural and spectroscopic analysis of a new family of monomeric diphosphinoboranes
PublikacjaWe present a series of amino- and aryl(diphosphino)boranes R2PB(R’’)PR’2, where R2P, R’2P = tBu2P, tBuPhP, Ph2P, Cy2P, and R’’ = iPr2N, Ph, which were obtained via the metathesis reaction of iPr2NBBr2 or PhBBr2 with selected lithium phosphides. The structures of isolated diphosphinoboranes were characterized in the solid state and in solution by means of X-ray diffraction and NMR spectroscopy, respectively. The utility of these...
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Third harmonic generation studies of 1.06 μm Nd:YAG laser beam in Li2SO4–MgO–P2O5 glass system-influence of CuO
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Global wealth disparities drive adherence to COVID-safe pathways in head and neck cancer surgery
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Production of fuel briquette from solid waste biomass using natural resin as a binder
Publikacja10.34172/EHEM.2022.xx
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Armin Mikos von Rohrscheidt, Historia w turystyce kulturowej, Wydawnictwo PWN, Warszawa 2018, ss. 378.
PublikacjaRecenzja książki: A. Mikos von Rohrscheidt, Historia w turystyce kulturowej.
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The Reactivity of Phosphanylphosphinidene Complexes of Transition Metals Toward Terminal Dihaloalkanes
PublikacjaThe reactivities of phosphanylphosphinidene complexes [(DippN)2W(Cl)(η2-P−PtBu2)]− (1), [(pTol3P)2Pt(η2- P=PtBu2)] (2), and [(dppe)Pt(η2-P=PtBu2)] (3) toward dihaloalkanes and methyl iodide were investigated. The reactions of the anionic tungsten complex (1) with stochiometric Br(CH2)nBr (n = 3, 4, 6) led to the formation of neutral complexes with a tBu2PP(CH2)3Br ligand or neutral dinuclear complexes with unusual tetradentate...
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New pathways for functionalization of phosphorus ligands
PublikacjaThe presented dissertation consistsof two main partsand focuses on the synthesis and characterization of new low-valent phosphorus compounds. Thesestudies have already been fully described in three JCR-journals. The first partdescribes the utilization ofselectedphosphanylphosphinidene transition metal complexes as a source of diversified phosphorus ligands. For thispurposethree complexes...
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ALD thin ZnO layer as an active medium in a fiber-optic Fabry-Perot interferometer
Publikacja.
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On Computational Aspects of Greedy Partitioning of Graphs
PublikacjaIn this paper we consider a problem of graph P-coloring consisting in partitioning the vertex set of a graph such that each of the resulting sets induces a graph in a given additive, hereditary class of graphs P. We focus on partitions generated by the greedy algorithm. In particular, we show that given a graph G and an integer k deciding if the greedy algorithm outputs a P-coloring with a least k colors is NP-complete for an infinite...
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Wczesny Mickiewicz jako zapowiadający się historiozof
PublikacjaThe paper shows young Mickiewicz’s family and historical experiences. It discussesthe knightly premises for his historiosophy and explains its radicalism and structureon the grounds of the knightly tradition. The study reveals the pre-Slavic deposits ofspiritual archeology in the Romantic poet. It proves that the activation of these depositsshaped Mickiewicz’s view on the collision between Poland and...
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Optimal Placement of Phasor Measurement Unit in Power System using Meta-Heuristic Algorithms
PublikacjaThe phasor measurement units (PMUs) play an important and vital role in power system monitoring and controlling, since they provide the power system phasors stamped with a common real time reference through a global positioning system (GPS). Indeed, from economical point of view it is not possible to set PMUs in all system buses due to the high cost and the requirement of more complex communication...