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Wyniki wyszukiwania dla: SPEKTROMERIA MAS
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Determination of tributyltin (TBT) in marine sediment using pressurised liquid extraction–gas chromatography–isotope dilution mass spectrometry (PLE–GC–IDMS) with a hexane–tropolone mixture
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Green, simple analytical method for biogenic amines determination in fruit juice samples using salting-out assisted liquid-liquid microextraction and gas chromatography-mass spectrometry
PublikacjaSalting-out assisted liquid-liquid microextraction (SALLME) was integrated with the derivatization procedure to establish a one-step sample pre-treatment approach for rapid analysis of 14 biogenic amines (BAs) in fruit juices. The methodology consists of salting-out of analytes, derivatization with ethyl chloroformate (ECF), extraction with ethyl acetate (EtAc), and the analysis of the derivatized BAs using gas chromatography-mass...
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A New Approach to Generation of Standard Gas Mixtures used in the Calibration of Gas Analysers
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Nieukierunkowana analiza fosfolipidów w próbkach biologicznych i żywności Część II. Zaawansowane techniki analityczne w analizie fosfolipidów
PublikacjaRozwój zaawansowanych technik analitycznych, który miał miejsce na przestrzeni ostatnich lat, w znaczący sposób przyczynił się do rozwoju lipidomiki – nauki mającej na celu określenie roli związków lipidowych w funkcjonowaniu systemów biologicznym, w tym ludzkiego organizmu. Nieukierunkowana analiza dostarczanych do organizmu i występujących w nim lipidów wymaga zastosowania wysokorozdzielczych technik analitycznych. Wprowadzenie...
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The presence of polycyclic aromatic hydrocarbons in disposable baby diapers: A facile determination method via salting-out assisted liquid-liquid extraction coupled with gas chromatography-mass spectrometry
PublikacjaIn this paper we demonstrate the development of the extraction procedure of polycyclic aromatic hy- drocarbons from baby diapers along with their quantification by gas chromatography-mass spectrometry. Apart from covering plastic foil, disposable baby diapers contain sorbents intended to absorb urine and feces. A hygroscopic, adsorptive, and tough-to-homogenize fibrous sorbent, represents an analytical chal- lenge to analytical...
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Efficiency of linear and non-linear classifiers for gas identification from electrocatalytic gas sensor
PublikacjaElectrocatalytic gas sensors belong to the family of electrochemical solid state sensors. Their responses are acquired in the form of I-V plots as a result of application of cyclic voltammetry technique. In order to obtain information about the type of measured gas the multivariate data analysis and pattern classification techniques can be employed. However, there is a lack of information in literature about application of such...
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Gas Detection Using Resistive Gas Sensors And Radial Basis Function Neural Networks
PublikacjaWe present a use of Radial Basis Function (RBF) neural networks and Fluctuation Enhanced Sensing (FES) method in gas detection system utilizing a prototype resistive WO3 gas sensing layer with gold nanoparticles. We investigated accuracy of gas detection for three different preprocessing methods: no preprocessing, Principal Component Analysis (PCA) and wavelet transformation. Low frequency noise voltage observed in resistive gas...
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Flicker Noise in Resistive Gas Sensors—Measurement Setups and Applications for Enhanced Gas Sensing
PublikacjaWe discuss the implementation challenges of gas sensing systems based on low-frequency noise measurements on chemoresistive sensors. Resistance fluctuations in various gas sensing materials, in a frequency range typically up to a few kHz, can enhance gas sensing by considering its intensity and the slope of power spectral density. The issues of low-frequency noise measurements in resistive gas sensors, specifically in two-dimensional...
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Gas mixtures recognition using an array of amperometric gas sensors with drifting or faulty sensors
PublikacjaIn this study, the possibility of using selected methods for diagnostics of performance of matrix composed with six amperometric electrochemical gas sensors is investigated. Measurements of sensor responses in selected concentrations of single toxic gases or gas mixtures were performed and were repeated over time to show sensor drift. Additionally, the studies on the sensors’ drift were performed. The drift has been recognized...
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Multidimensional attitudes scale toward persons with disabilities: factor and exploratory analysis for a Ukrainian version (MAS-UA)
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Sztuczna słodzycz wokół nas
PublikacjaSyntetyczne słodziki o dużej mocy słodzącej stanowią ważną klasę dodatków do żywności, które są szeroko stosowane w przemyśle spożywczym. Główną cechą tych zwykle niskokalorycznych środków jest bardzo intensywny słodki smak. Producenci żywności, mając na uwadze osiągnięcie lepszych doznań smakowych, stosują coraz to nowe typy słodzików bądź ich różne mieszaniny. Zapotrzebowanie na żywność z substancjami słodzącymi nieustannie rośnie....
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Otopy classes of equivariant maps
PublikacjaW artykule definiuje się stopień topologiczny niezmienniczych odwzorowań lokalnych w przypadku gradientowym i niegradientowym. Wyniki dotyczą relacji pomiędzy tymi dwoma niezmiennikami topologicznymi.
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An experimental study on polymer mass
PublikacjaA new method of repairing damaged structures by filling the cracks with specially prepared polymer mass has been recently proposed. The technique is mainly dedicated to historical objects where minimum intervention is permitted. The flexible joint bonds the disrupted elements and ensures further safe exploitation of a damaged structure. The aim of the present paper is to show the results of an experimental study on polymer mass...
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Sulfur compounds: Gas chromatography
PublikacjaSulfur compounds, due to their properties, are responsible for the damage of our environment. For this reason sulfur containing compounds are of constant concern in many fields. Gas chromatography (GC), due to combination of separation capability and sensitive detection is a prime technique for the analysis of thes compounds in various matrices. The chapter rewies general problems of the determination of these compounds by GC and...
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On the space of equivariant local maps
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Mechanism of the phase transitions in MnAs
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Indices of iterations of planar maps
PublikacjaArtykuł omawia najnowsze rezultaty badań dotyczące postaci indeksów punktu stałego iteracji odwzorowań planarnych.
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AI in the creation of the satellite maps
PublikacjaSatellite and aerial imagery acquisition is a very useful source of information for remote monitoring of the Earth’s surface. Modern satellite and aerial systems provide data about the details of the site topography, its characteristics due to different criteria (type of terrain, vegetation cover, soil type and moisture content), or even information about emergency situations or disasters. The paper proposes and discusses the process...
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An absorbing set for the Chialvo map
PublikacjaThe classical Chialvo model, introduced in 1995, is one of the most important models that describe single neuron dynamics. In order to conduct effective numerical analysis of this model, it is necessary to obtain a rigorous estimate for the maximal bounded invariant set. We discuss this problem, and we correct and improve the results obtained by Courbage and Nekorkin (2010). In particular, we provide an explicit formula for an...
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Developments in Miniaturization of Gas Chromatography
Publikacja.
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Palao de las Artes.
PublikacjaOmówiono najnowszą realizację S. Calatravy Paleo de las Artes", stanowiącą wraz z trzema innymi obiektami przykład rewitalizacji terenów dawnego koryta rzeki Turia w centrum Walencji w Hiszpanii.
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Comparison of effectiveness of gas sensing by low frequency fluctuations in resistance and microbalance quartz gas sensors
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Extraction and evaluation of gas-flow-dependent features from dynamic measurements of gas sensors array
PublikacjaGas analyzers based on gas sensors are the devices which enable recognition of various kinds of volatile compounds. They have continuously been developed and investigated for over three decades, however there are still limitations which slow down the implementation of those devices in many applications. For example, the main drawbacks are the lack of selectivity, sensitivity...
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Investigation of the Combustion Processes in the Gas Turbine Module of an FPSO Operating on Associated Gas Conversion Products
PublikacjaIn this paper, we consider the issue of thermo-chemical heat recovery of waste heat from gas turbine engines for the steam conversion of associated gas for offshore vessels. Current trends in the development of offshore infrastructure are identified, and the composition of power plants for mobile offshore drilling units and FPSO vessels is analyzed. We present the results of a comparison of power-to-volume ratio, power-to-weight...
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Limited selectivity of amperometric gas sensors operating in multicomponent gas mixtures and methods of selectivity improvement
PublikacjaIn recent years, smog and poor air quality have became a growing environmental problem. There is a need to continuously monitor the quality of the air. The lack of selectivity is one of the most important problems limiting the use of gas sensors for this purpose. In this study, the selectivity of six amperometric gas sensors is investigated. First, the sensors were calibrated in order to find a correlation between the concentration...
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INVESTIGATION OF THE CHARACTERISTICS OF A LOWEMISSION GAS TURBINE COMBUSTION CHAMBER OPERATING ON A MIXTURE OF NATURAL GAS AND HYDROGEN
PublikacjaT his article is devoted to the investigation of the characteristics of a low-emission gas turbine combustion chamber, which can be used in Floating Production, Storage and Offloading (FPSO) vessels and operates on a mixture of natural gas and hydrogen. A new approach is proposed for modelling the processes of burning out a mixture of natural gas with hydrogen under preliminary mixing conditions in gaseous fuel with an oxidizer...
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Influence of gas parameters alteration on the form of gas-flow-impact appearing in long transportation pipelines
PublikacjaPrzy szybkich zamknięciach przepływu w długich liniach transportowych gazu, obserwuje się znaczne przesterowania ciśnienia, towarzyszące zjawiskom udarowym, wywołane zarówno falą uderzeniową jak i odbitą. Głównym czynnikiem wpływającym na postać fali uderzeniowej i jej amplitudy, jest szybkość zamykania zaworu odcinającego określona stałą czasową serwomotoru sterującego zaworem. Ponieważ obserwuje się zmiany właściwości chemicznych...
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An algorithm for preliminary estimating hull structure mass and mass centre height of inland navigation ships
PublikacjaPrzedstawiono algorytm obliczeniowy służący do wstępnego wyznaczania masy i wysokości środka ciężkości konstrukcji kadłuba statków śródlądowych. Algorytm opracowano opierając się na zaleceniach zawartych w Przepisach Klasyfikacji i Budowy Statków Śródlądowych PRS oraz zastosowano uproszczoną metodę wyznaczania mas usztywnień poszycia kadłuba. Algorytm dotyczy wymiarowania konstrukcji klasycznych statków służących do przewozu drobnicy,...
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Energy requirements for methods improving gas detection by modulating physical properties of resistive gas sensors
PublikacjaAbstract. One of the most important disadvantage of resistive gas sensors is their limited gas selectivity. Therefore, various methods modulating their physical properties are used to improve gas detection. These methods are usually limited to temperature modulation or UV light irradiation for the layers exhibiting photocatalytic effect. These methods cause increased energy consumption. In our study we consider how much energy...
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[Rozdział] 3. Jakość wyników analitycznych
PublikacjaPrzedstawiono charakterystykę systemu zapewnienia jakości pomiaru analitycznego. Podano klasyfikację współczesnych metod analitycznych. Opisano i scharakteryzowano technikę spektrometrii mas rozcieńczenia izotopowego jako przykład metody pierwotnej.
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Potential for Prebiotic Stabilized Cornus mas L. Lyophilized Extract in the Prophylaxis of Diabetes Mellitus in Streptozotocin Diabetic Rats
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Characteristics of Cucumis metuliferus, Actinidia deliciosa and Musa paradisica fragrance profiles using a comprehensive two-dimensional gas chromatography with time-of-flight mass spectrometric detection (GC×GC-TOF MS)
PublikacjaComprehensive two-dimensional gas chromatography with time-of-flight mass spectrometric detection (GC×GC-TOF-MS) is a modern analytical technique used in many fields. This technique enables an effective separation of volatile chemical compounds [1]. In recent years, the topic of healthy food and healthy living has become very popular. For this reason, more and more scientific publications related to the analysis of food products...
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Portable exhaled breath analyzer employing fluctuation-enhanced gas sensing method in resistive gas sensors
PublikacjaThis paper presents a portable exhaled breath analyser, developed to detect selected diseases. The set-up employs resistive gas sensors: commercial MEMS sensors and prototype gas sensors made of WO3 gas sensing layers doped with various metal ingredients. The set-up can modulate the gas sensors by applying UV light to induce physical changes of the gas sensing layers. The sensors are placed in a tiny gas chamber of a volume...
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Materials for potentiometric electrochemical gas sensors
PublikacjaPublikacja przeglądowa na temat zasady działania oraz rodzajów czujników elektrochemicznych gazów.
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Fluctuation-enhanced gas sensing in practice
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Fluctuation phenomena in semiconductor gas sensors
PublikacjaCzujniki gazu mogą być wytwarzane z cienkiej warstwy półprzewodnika, która po podgrzaniu do odpowiedniej temperatury staje się czuła na gaz. Zjawisko to jest dobrze znane i szeroko opisane w literaturze. Jako wskaźnik detekcji gazu wykorzystuje się zmianę rezystancji stałoprądowej czujnika. Zwiększenie czułości i, co najważniejsze z praktycznego punktu widzenia, selektywności dyskryminacji można uzyskać jeśli warstwa półprzewodnika...
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Tools for signal analysis of gas sensors
PublikacjaStatystyki drugiego rzedu oraz jklasyczna analiza widmowa są zwykle stosowane do badania sygnałów losowych o rozkładzie gaussowskim. Są one jednak często nieodpowiednie w przypadku analizy niestacjonarnych sygnałów niegaussowskich. Pewne narzędzia do analizy takich sygnałów sa dostępne w bibliotekach środowiska MATLAB. Zostały one wykorzystane do do analizy fluktuacji sygnałów czujników gazów. W artykule przedstawiono system do...
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On the selectivity of nanostructured semiconductor gas sensors
Publikacja.
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Gas-steam mixture wood drying
PublikacjaBadania skuteczności suszenia wysokotemperaturowego suszenia drewna w komorze suszarniczej - wstępne wyniki.
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Geodesic monitoring of tower and mast structures
PublikacjaW artykule przedstawiono obciążenia jakim są poddawane konstrukcje wieżowe i masztowe. Opisano zakres oraz wymagania dotyczące pomiarów geodezyjnych przeprowadzanych w czasie eksploatacji konstrukcji smukłych. Wskazano metody pomiaru oraz zaprezentowano niektóre sposoby pomiaru w praktyce. Zamieszczono wyniki pomiarów przemieszczeń elektrowni wiatrowej o mocy 2 MW i wysokości elementu wsporczego 80 m oraz zaprezentowano pomiary...
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Quantum dots in gas sensing a review
PublikacjaAir pollution becomes an increasing problem in the recent years. There is a need to develop more sensitive gas sensors. Much effort has been performed to develop different types of gas sensors, such as electrochemical sensors or polymer sensors. One of the most promising approaches to improve sensors performance is the application of the nanostructures as sensing materials. State of the art of quantum...
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Hydrogen sulphide electrocatalytic gas sensor
PublikacjaIn this article measurement results of the electrocatalytic gas sensor in different concentrations of hydrogen sulphide are presented. Working principle of such sensor is based on electric current acquisition, while voltage ramp is applied to the sensor. During voltage sweep oxidation and reduction reactions occurs on the sensor electrodes. Obtained current-voltage plot has unique shape connected...
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Gas sensors based on superionic conductors
PublikacjaW pracy przedstawiono przegląd rozwiązań elektrochemicznych czujników gazów na bazie elektrolitów stałych.
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GAS SENSORS WITH TEMPERATURE MODULATION – AN OVERVIEW
PublikacjaAlthough different methods of improving semiconductor gas sensor properties have been proposed, a technique involving temperature modulation seems to be the most promising. Semiconductor gas sensors working with modulated temperature can be more stable and are more selective comparing with sensor working at one temperature. In this paper, various approaches to temperature modulation are reviewed.
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Perforating systems in shale gas recovery
PublikacjaHydraulic fracturing is common method of shale gas recovery. Due to environmental, economical and technological problems many alternative technologies have been developed. One of the most promising group of technologies is based on perforating systems. This paper describes theoretical and practical aspects of best known technologies used to create perforations. New perforating/fracturing technologies which can replace hydraulic fracturing...
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Self Organizing Maps for Visualization of Categories
PublikacjaVisualization of Wikipedia categories using Self Organizing Mapsshows an overview of categories and their relations, helping to narrow down search domains. Selecting particular neurons this approach enables retrieval of conceptually similar categories. Evaluation of neural activations indicates that they form coherent patterns that may be useful for building user interfaces for navigation over category structures.
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Electrocatalytic gas sensor with reference layer
PublikacjaIn recent years electrochemical gas sensors based on solid state electrolytes have been intensively developed. They are easy to obtain, use and relative durable. Nasicon is one of the most promising materials, which have been used in construction of gas sensors. Most of these devices work in potentiometric or amperometric mode. However, some works are dedicated to sensors working in electrocatalytic mode. Principle of operation...
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Electrocatalytic Gas Sensor with Reference Layer
PublikacjaThis paper presents studies of gas sensors prepared in ceramic technology with Nasicon as a solid electrolyte. Sensors work in the voltammetric mode thus based on the excitation of a sensor with a periodic potential signal while current response is recorded. The main aim is to investigate a Bi8Nb2O17 reference layer influence on sensor properties. Sensors I-V characteristics in different concentration of nitrogen dioxide have been...
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Noise related to gas bottles explosions
PublikacjaModern industrialized world is in a never ending danger of accidents and catastrophes of technical nature. Some of them may involve fires and explosions of gas storage bottles or containers. Technical University of Gdansk, Poland performed numerous tests where bottles containing acetylene, oxygen, hydrogen, CO2, LPG, LNG or CNG were blown due to excessive temperature caused by fire. Although those experiments were not focused on...
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Transportable, Portable and Micro Gas Chromatographs
PublikacjaSignificant benefits can be obtained by miniaturization of conventional benchtop gas chromatographs. The attractive features arising from miniaturization include low-power requirements, low heat capacity of separation columns, low consumption of mobile phase, enhanced performance, higher portability, and easily coupling to detectors and secondary chromatographic systems. In separation sciences, including gas phase separations,...