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Simone de Beauvoir Studies
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Vingtième Siècle. Revue d'histoire
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Sample preparation procedure using extraction and derivatization of carboxylic acids from aqueous samples by means of deep eutectic solvents for gas chromatographic-mass spectrometric analysis
PublikacjaThe paper presents a new procedure for the determination of organic acids in a complex aqueous matrixusing ultrasound-assisted dispersive liquid–liquid microextraction followed by injection port derivati-zation and GC–MS analysis. A deep eutectic solvent (choline chloride: 4-methylphenol in a 1:2 mol ratio)was used both as an extracting solvent and as a derivatizing agent to yield ion pairs which were next con-verted to methyl...
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Current trends in analytical strategies for determination of polybrominated diphenyl ethers (PBDEs) in samples with different matrix compositions – Part 1.: Screening of new developments in sample preparation
PublikacjaPolybrominated diphenyl ethers (PBDEs) are ubiquitous compounds in the environment. Restrictions on the use of PBDEs introduced at the beginning of the 21st century have not eliminated these highly persistent and bioaccumulative compounds from the environment. Despite many existing regulations to control and phase out, extensive research on PBDEs is still necessary to fully evaluate the hazard their create to the environment. In...
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Validation and Regulatory Issues for Sample Preparation
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Introductory Chapter: Evolution of Sample Preparation
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Introductory Chapter: Evolution of Sample Preparation
Publikacja.
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A simple way of increasing estimation accuracy of generalized adaptive notch filters
PublikacjaGeneralized adaptive notch filters are used for identification/tracking of quasi-periodically varying dynamic systems and can be considered an extension, to the system case, of classical adaptive notch filters. It is shown that frequency biases, which arisein generalized adaptive notch filtering algorithms, can be significantly reduced by incorporating in the adaptive loop an appropriately chosen decision delay. The resulting performance...
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Structural properties of hydration shell around various conformations of simple polypeptides
PublikacjaIn this paper we investigate structural properties of water within the solvation shell around the peptide core created by a well-defined conformation of polypeptide chain. The following secondary structures are investigated: linear (straight chain), and three helices PII (polyproline-like), 310, and α. We propose using the two-particle contribution to entropy as a rational measure of the water structural ordering within the solvation...
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A note on simple bifurcation of equilibrium forms of an elastic rod on a deformable foundation
PublikacjaWe study bifurcation of equilibrium states of an elastic rod on a two-parameter Winkler foundation. In the article "Bifurcation of equilibrium forms of an elastic rod on a two-parameter Winkler foundation" [Nonlinear Anal., Real World Appl. 39 (2018) 451-463] the existence of simple bifurcation points was proved by the use of the Crandall-Rabinowitz theorem. In this paper we want to present an alternative proof of this fact based...
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Verification of ESPAR Antennas Performance in the Simple and Calibration Free Localization System
PublikacjaThis paper presents the results of simulations and measurements of an indoor localization system that uses Electronically Steerable Parasitic Array Radiator (ESPAR) antennas with switched directional beam. Proposed antennas are dedicated for 2.4GHz ISM low-cost applications where determination of the incoming signal is required. The antennas performance is analyzed and verified with relation to positioning methods based on the...
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Simple colorimetric copper(II) sensor – spectral characterization and possible applications
PublikacjaNew o-hydroxyazocompound L bearing pyrrole residue was obtained in the simple synthetic protocol. The structure of L was confirmed and analyzed by X-ray diffraction. It was found that new chemosensor can be successfully used as copper(II) selective spectrophotometric regent in solution and can be also applied for the preparation of sensing materials generating selective color signal upon interaction with copper(II). Selective colorimetric...
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Two-Row ESPAR Antenna with Simple Elevation and Azimuth Beam Switching
PublikacjaIn this letter, we propose a two-row electronically steerable parasitic array radiator (ESPAR) antenna designed for direction of arrival (DoA) estimation in Internet of Things (IoT) applications relying on simple microcontrollers. The antenna is capable of elevation and azimuth beam switching using a simple microcontroller-oriented steering circuit and provides 18 directional radiation patterns, which can be grouped in 3 distinctive...
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Vapor correction of FTIR spectra – A simple automatic least squares approach
PublikacjaFTIR spectroscopy is one of the best techniques to study intermolecular interactions. However, such an application requires high quality spectra with as little noise as possible, which are often difficult to obtain. One of the main sources of unwanted interference is water vapor. Here a robust method is proposed for automatic, fast and reliable vapor correction of FTIR spectra. The presented least squares approach of vapor subtraction...
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A simple modification of PCR thermal profile applied to evade persisting contamination
PublikacjaThe polymerase chain reaction (PCR), one of the most commonly applied methods of diagnostics and molecular biology has a frustrating downside known as the false positive signal or contamination. Several solutions to avoid and to eliminate PCR contaminations have been worked out to date but the implementation of these solutions to laboratory practice may be laborious and time consuming. A simple approach to circumvent the problem...
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Simple 2-D Direction-of-Arrival Estimation Using an ESPAR Antenna
PublikacjaIn this letter, it has been shown how an electronically steerable parasitic array radiator (ESPAR) antenna can be used for 2-D direction-of-arrival (DoA) estimation employing received signal strength (RSS) values only. The proposed approach relies on changes in RSS values recorded at the antenna output port observed for different vertical and horizontal directions, while antenna’s main beam sweeps 360° area around the ESPAR antenna. Based...
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Seizième siècle (Formerly : Nouvelle revue du XVIe siècle) (Formerly : La Nouvelle revue du seizième siècle see Nouvelle revue du seizième siècle )
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Diagnostic model of compression-ignition engine slide bearings for controlling the changes of their state
PublikacjaW artykule przedstawiono koncepcję umożliwiającą sterowanie procesami zmian stanów eksploatacyjnych silnika na podstawie modelu diagnostycznego łożysk ślizgowych. Jako model łożyska ślizgowego przyjęty został topologiczny model diagnostyczny, pozwalający na pełne i dokładne wykorzystanie oleju smarowego jako jednego z nośników informacji o stanie technicznym łożyska. Przedstawiona została przykładowa interpretacja stanów eksploatacyjnych...
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Internal heat recuperation in vapor compression and hybrid desiccant air conditioning systems
PublikacjaPraca przedstawia badania prowadzone w Katedrze Techniki Cieplnej Politechniki Gdańskiej nad wewnętrznym odzyskiem ciepła w parowo-spreżarkowych oraz adsorpcyjnych hybrydowych urządzeniach klimatyzacyjnych. Zaprezentowano wyniki analizy psychrometrycznej procesów realizowanych w urządzeniach, stanowiska badawcze urządzeń oraz uzyskane wyniki eksperymentalne.
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Strain-dependent behaviour of cold recycled material mixtures in cyclic compression tests
PublikacjaThe purpose of the study is to evaluate strain-dependent behaviour of Cold Recycled Material (CRM) mixtures using three frameworks typically applied for Hot Mix Asphalt (HMA): linear viscoelastic (LVE) limits; non-linearity directions; changes in rheological model parameters. To this aim, the complex modulus of three CRM mixtures with different bitumen-to-cement ratio (0.2, 0.6 and 1.8) was measured in cyclic compression mode,...
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ECU calibration for gaseous dual fuel supply system in compression ignition engines
PublikacjaThe dual fuel (DF) combustion mode is proven solution that allows to improve or get at the same level engine performance and reduce toxic compounds in exhaust gases which is confirmed by researchers and end-users. DF combustion mode uses two fuels gaseous fuel as a primary energy source and a pilot quantity of diesel fuel as ignition source. However, in order, to fully take advantage of the potential of the dual fuel mode, DF system...
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Possibility to use engine compression ignition engines in floating power plants marine
PublikacjaCompression-ignition engines used in ship technology as main propulsion engines are large units reaching even to 50-60 MW. The engines can be used in power industry for electricity generation in a simple or combined steam turbine system in combined heat and power plants. The leading engine in such an arrangement is an internal-combustion piston engine. The main propulsion engines are used in large piston internal-combustion engines...
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Effect of fabric anisotropy on shear localization in sand during plane strain compression
PublikacjaW artykule przedstawiono wyniki numerycznej wpływu anizotropii strukturalnej w materiałach granulowanych na powstawanie lokalizacji odkształceń. Obliczenia wykonano dla ściskania w płaskim stanie odkształcenia stosując metodę elementów skończonych na bazie mikropolarnego modelu hipoplastycznego.
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FE-analysis of failure behaviour of reinforced concrete columns under eccentric compression
PublikacjaArtykuł omawia obliczanie słupów żelbetowych poddanych ściskaniu mimośrodowemu z uwzględnieniem lokalizacji odkształceń. Obliczenia wykonano przy zastosowaniu MES i sprężysto-plastycznego prawa konstytutywnego rozszerzonego o długość charakterystyczną mikrostruktury za pomocą teorii nielokalnej.
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Application of Box–Behnken design in the optimization of a simple graphene oxide/zinc oxide nanocomposite-based pipette tip micro-solid phase extraction for the determination of Rhodamine B and Malachite green in seawater samples by spectrophotometry
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Experimental and theoretical studies of the spectroscopic properties of simple symmetrically substituted diphenylacetylene derivatives
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Simple 60 GHz Switched Beam Antenna for 5G Millimeter-Wave Applications
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Hydration of Simple Carboxylic Acids from Infrared Spectra of HDOand Theoretical Calculations
PublikacjaBadanie hydratacji kwasów karboksylowych w rozcieńczonych roztworach wodnych ma duże znaczenie dla zrozumienia ich funkcji biologicznych. Metodą stosowaną w badaniach była spektroskopia oscylacyjna FTIR z zastosowaniem techniki rozcieńczenia izotopowego wody półciężkiej HDO w roztworze wody zwykłej. Do analizy danych widmowych wykorzystano ''metodę widm różnicowych''. Widma HDO zaburzonej przez kwasy: mrówkowy, octowy i propionowy...
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Simple multi-laminate model for soft soils incorporating structural anisotropy and destructuration
PublikacjaZaproponowano nowy model konstytutywny należący do rodziny tzw. modeli wielopłaszczyznowych (multi-laminate) dla gruntów słabonośnych. Oryginalnymi rozwiązaniami w modelu są: wprowadzenie kierunkowo zależnej prekonsolidacji oraz uwzględnienie zmian anizotropii wytrzymałości na ściskanie podczas destrukturyzacji naturalnych gruntów słabonośnych. Model zweryfikowano dla podstawowych badań elementowych.
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A simple method for selection of trypsin chromogenic substrates using combinatorial chemistry approach
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Towards the autonomy of urban management: simple system as a solution for complex urban environment
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Simple and novel synthesis of 3-(thio)phosphoryl-β-lactams by radical cyclization
PublikacjaRadical cyclization of phosphono-acetenamides promoted by manganese(III) acetate leads exclusively to the formation of 3-phosphoryl-β-lactams. The thiophosphoryl analogues were also prepared using this method. In particular, the presented protocol does not require the use of noble metals, while comparable methods do.
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Simple 60 GHz Switched Beam Antenna for 5G Millimeter-Wave Applications
PublikacjaA new 60 GHz band single-input switched beam antenna is proposed for the fifth-generation (5G) millimeter-wave network applications. The presented design is capable of electronically switching the main beam in two different directions via a proposed microstrip-line-to-slotline single-pole dual-throw (SPDT) switch based on commercially available p-i-n diodes. The antenna is fabricated in a low-cost printed circuit board process...
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Design of a Patch Power Divider with Simple Structure and Ultra-Broadband Harmonics Suppression
PublikacjaThis paper introduces a simple H-shaped patch Wilkinson power divider (WPD), which provides ultra wide harmonics suppression band. The presented WPD designed at 1.8 GHz, and exhibits good performance at the operating bandwidth. In the proposed divider structure, two simple patch low-pass filters (LPFs) are employed at each branch, and three open ended stubs are added at each port. The proposed divider, implemented using the aforementioned...
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A Simple-Topology Compact Broadband Circularly Polarized Antenna With Unidirectional Radiation Pattern
PublikacjaIn this letter, a geometrically simple, reflector-backed single-point-fed circularly polarized (CP) antenna with unidirectional radiation pattern is presented. The structure comprises a simple coplanar waveguide (CPW) feeding circuit with an open slot etched on one side of the coplanar ground. The enhanced CP bandwidth is obtained by combining the loop mode, the slot mode, and the asymmetrical configuration of the coplanar ground...
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A simple approach to heat exchanger sizing optimisation by means of entrophy generation minimisation
PublikacjaIn the paper an attempt is presented to find the method of optimization of microtube diameter with respect to optimal thermal-hydraulic conditions in the single-phase shell-and-tube heat exchangers. The approach is based on consideration of pumping power at the condition of maximum heat transfer by the heat exchanger tube system. In the optimization method the tube diameter is first specified and then appropriate calculations are...
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UHF ESPAR antenna for simple Angle of Arrival estimation in UHF RFID applications
PublikacjaAn electronically switched beam antenna for localization of passive UHF RFID tags based on a simple Angle of Arrival (AoA) technique is proposed‥ Detailed antenna design and realization are presented together with corresponding simulations and measurement results. Experimental tests with passive UHF RFID tag show the validity of theoretical assumptions for application of the antenna in UHF RFID based localization systems.
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Annihilation rates of low-energy positron scattering from simple diatomic molecules
PublikacjaWe discuss the calculations of Zeff coefficients for a series of diatomic molecules over the range of energies below the positronium formation. During the development of a general code for polyatomic, nonlinear molecules colliding with positrons, it was discovered that the earlier one, employed only for diatomic molecules, had an error. The error is corrected and the corrected results are presented here. We also discuss a way of...
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Experimental economics in business education: Using simple games to achieve multifaceted effects
PublikacjaEconomics differs from other sciences not only because of its normative part, but also because of very limited use of experiments. In this way, economics is often perceived as being methodologically more similar to astronomy or meteorology rather than physics or chemistry. Over last decades, however, experimental economics has been significantly developed. This chapter presents some of the possibilities for academic teachers to...
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The conception of energetic investigations of the multisymptom fatigue of the simple mechanical systems' constructional materials
PublikacjaThe article presents the basic assumptions of the research project aimed, as the main scientific purpose, an identification of the slow-changeable energy processes surrounding the high-cycle fatigue of constructional materials within the plain mechanical system, especially the marine one, for diagnostic purposes. There is foreseen an application of alternative diagnostic methods based on energetic observations of the multi-symptom,...
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FE-simulations of a direct and a true simple shear test within a polar hypoplasticity
PublikacjaW artykule przedstawiono wyniki numerycznej analizy testu bezpośredniego ścinania i testu prostego ścinania w materiałach granulowanych. Obliczenia wykonano stosując metodę elementów skończonych i mikropolarne hipoplastyczne prawo konstytutywne. W analizie uwzględniono lokalizację odkształceń stycznych.
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The Effect of Dimple Distortions on Surface Topography Analysis
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Modern Sample Preparation Techniques: A Brief Introduction
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AGREEprep – Analytical greenness metric for sample preparation
PublikacjaThis work proposes for the first time, a metric tool that gives prominence to sample preparation. The developed metric (termed AGREEprep) was based on 10 categories of impact that were recalculated to 0 e1 scale sub-scores, and then used to calculate the final assessment score. The criteria of assessment evaluated, among others, the choice and use of solvents, materials and reagents, waste generation, energy consumption, sample...
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SIMPLY AND LOW COAST ELECTROMYOGRAPHY SIGNAL AMPLIFIER
PublikacjaRecently, there has been a noticeable increase in interest in solu tions utilizing electrical signals accompanying muscle activity. Electromyography (EMG) is a technique for recording, analysis and evaluating the electrical activity produced by striated muscle. Its great popularity is due, among other, to the ability to measure with non-invasive electrodes (calle d as sEMG surface electromyography)....
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Green Analytical Chemistry Approaches in Sample Preparation
PublikacjaThis chapter presents environmentally friendly solutions for sample preparation. Attention is focused on extraction techniques and the minimization of organic solvent consumption, as the large quantitiesused in analytical laboratories are a pressing environmental problem. Solventless sample preparation techniques, alternative solvents, mediated extractions are discussed. The principle of each technique isbriefly described, together...
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Sample Rate Conversion with Fluctuating Resampling Ratio
PublikacjaIn this paper a sample rate conversion with continuouslychanging resampling ratio has been presented. The proposed implementation is based on variable fractional delay filter implemented using a Farrow structure. It have been demonstrated that using the proposed approach instantaneous resampling ratio can be freely changed. This allows for simulation of audio recored on magnetic tape with nonuniform velocity as well as removal...
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Green Aspects of Miniaturized Sample Preparation Techniques
PublikacjaCorrect monitoring and control of the state of the environment and scientific research on the subject of environmental protection often require that determinations of compounds present at very low concentrations be made in samples characterized by a matrix of complex composition (e.g., biological samples, water and soil samples). Moreover, due to the limited number of analytical techniques which are sufficiently sensitive to conduct...
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Sample Rate Conversion with Fluctuating Resampling Ratio
PublikacjaIn this paper a sample rate conversion with continuously changing resampling ratio has been presented. The proposed implementation is based on variable fractional delay filter implemented using a Farrow structure. It have been demonstrated that using the proposed approach instantaneous resampling ratio can be freely changed. This allows for simulation of audio recored on magnetic tape with nonuniform velocity as well as removal...
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Behaviour of asphalt concrete in cyclic and static compression creep test with and without lateral confinement
PublikacjaArtykuł przedstawia wpływ metodyki badań na określanie parametrów betonu asfaltowego. Wykazano, że badania pełzania bez skrępowania bocznego w większym stopniu uwypuklają wpływ asfaltu na parametry badanego betonu asfaltowego natomiast w badaniach ze skrępowaniem bocznym, zarówno rola asfaltu jak i szkieletu mineralnego jest uwzględniana przy ocenie parametrów betonu asfaltowego. Ponadto wykazano, że lepszymi miarami do oceny betonu...