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Wyniki wyszukiwania dla: fischer reaction
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Distortional buckling of composite thin-walled columns of a box-type cross section with diaphragms
PublikacjaDistortional buckling of axially compressed columns of box-like composite cross sections with andwithout internal diaphragms is investigated in the framework of one-dimensional theory. The channel membersare composed of unidirectional fibre-reinforced laminate. Two approaches to the member orthotropic materialare applied: homogenization based on the theory of mixture and periodicity cells, and homogenization basedon the Voigt–Reuss...
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Propagation in the Open Cylindrical Guide of Arbitrary Cross Section With the Use of Field Matching Method
PublikacjaA simple solution to propagation problem in open waveguides and dielectric fibers of arbitrary convex cross section is presented. The idea of the analysis is based on the direct field matching technique involving the usage of the field projection at the boundary on a fixed set of orthogonal basis functions. A complex root tracing algorithm is utilized to find the propagation coefficients of the investigated guides. Different convex...
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Moment resistance of I-section end-plate roof girder splices; a case study
PublikacjaThis article deals with the problem of determining the resistance of end-plate connections. A nonlinear FEM model of the joint was constructed in order to predict its carrying capacity. A standard code procedure was done as well. The analyses have been done to assess atypical end-plate joints designed and constructed as a part of roof structures.
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Scattering From a Cylindrical Object of Arbitrary Cross Section With the Use of Field Matching Method
PublikacjaA simple and intuitive solution to scattering problems in shielded and open structures is presented. The main idea of the analysis is based on the direct field matching technique involving the usage of projection of the fields at the boundary on a fixed set of orthogonal basis functions. Different convex shapes and various obstacle materials are considered to verify the validity of the method in open and closed structures. The...
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Microwave radiation in the synthesis of urethane prepolymers
PublikacjaThis paper describes the use of microwave radiation in the synthesis of urethane prepolymers in bulk (without solvent). The prepolymers were synthesized using 1,6-hexamethylene diisocyanate (HDI) and poly (ε-caprolactone) diol (PCL) at a molar ratio of 4:1. The reaction was carried out without a catalyst in the reactor with a conventional heating system (oil bath) or in the microwave reactor (MW Reactor NOVA 09) at temperatures...
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Natalia Anna Wójcik dr hab. inż.
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Application of Monoferrocenylsumanenes Derived from Sonogashira Cross-Coupling or Click Chemistry Reactions in Highly Sensitive and Selective Cesium Cation Electrochemical Sensors
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Quantitative structure activity relationships for the electron transfer reactions ofAnabaenaPCC 7119 ferredoxin-NADP+oxidoreductase with nitrobenzene and nitrobenzimidazolone derivatives: mechanistic implications
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TMSCl Promoted Acylation of Amines with 5-(α-amino- α'-hydroxy)methylene Meldrum's Acids - Elucidation of Mechanism.
PublikacjaRecently we have observed accelerating influence of trimethyl silyl chloride addition on the rate of the reactions of 5-(α-amino- α'-hydroxy)methylene Meldrum's Acids with amines, particularly in the case of highly basic amines. However the nature of the aforementioned process remain unexplained. In proposed communication we wish to report insightful elucidation of this mechanism. The reaction under investigation involves simply...
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Exemplary SEM images of polished cross sections of symmetrical cell with SrTi0.50Fe0.50O3-d electrodes and CGO-20 substrate sintered at 800 °C
Dane BadawczeThis dataset contains images of polished cross section of symmetrical cell with SrTi0.50Fe0.50O3-d electrodes and CGO-20 substrate sintered at 800 °C. Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope (SEM) with an accelerating voltage of 12 kV in a high vacuum mode.
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Synteza i analiza wieloetapowego klasyfikatora Fishera.**2002 s. 108, rys.,tab. w rozdz. bibliogr. 92 poz. maszyn. Rozprawa doktorska (08.07.2002) Promotor: doc. dr hab. inż. Witold Malina
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NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION B-BEAM INTERACTIONS WITH MATERIALS AND ATOMS
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Improved Efficacy Behavioral Modeling of Microwave Circuits through Dimensionality Reduction and Fast Global Sensitivity Analysis
PublikacjaBehavioral models have garnered significant interest in the realm of high-frequency electronics. Their primary function is to substitute costly computational tools, notably electromagnetic (EM) analysis, for repetitive evaluations of the structure under consideration. These evaluations are often necessary for tasks like parameter tuning, statistical analysis, or multi-criterial design. However, constructing reliable surrogate models...
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Experimental and theoretical studies on the photodegradation of 2-ethylhexyl 4-methoxycinnamate in the presence of reactive oxygen and chlorine species
Publikacja2-Ethylhexyl 4-methoxycinnamate (EHMC) is one of the most commonly used sunscreen ingredient. In this study we investigated photodegradation of EHMC in the presence of such common oxidizing and chlorinating systems as H2O2, H2O2/HCl, H2O2/UV, and H2O2/HCl/UV. Reaction products were detected by gas chromatography with a mass spectrometric detector (GC-MS). As a result of experimental studies chloro-substituted 4-methoxycinnamic...
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Three-dimensional structure of wave-induced momentum flux in irrotational waves in combined shoaling-refraction conditions
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The Landscape of the Spa Parks Creation through Components Influencing Environmental Perception Using Multi-Criteria Analysis
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Occlusion phenomenon of redox probe by protein as a way of voltammetric detection of non-electroactive C-reactive protein
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Sustained Sympathetic and Blood Pressure Reduction 1 Year After Renal Denervation in Patients With Resistant Hypertension
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The PARAGON-Heart failure trial – another disappointment for heart failure patients with hypertension and preserved ejection fraction
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Left ventricular ejection fraction and aortic stiffness are independent predictors of neurological outcome in acute ischemic stroke
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Microbiological, biochemical and ecotoxicological evaluation of soils in the area of biochar production in relation to polycyclic aromatic hydrocarbon content
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INDICES OF VASCULAR STIFFNESS AND WAVE REFLECTION IN RELATION TO BODY MASS INDEX OR BODY FAT IN HEALTHY SUBJECTS
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Selection of Methods of Surface Texture Characterisation for Reduction of the Frequency-Based Errors in the Measurement and Data Analysis Processes
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Interactions of Nitroaromatic Compounds with the Mammalian Selenoprotein Thioredoxin Reductase and the Relation to Induction of Apoptosis in Human Cancer Cells
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Two-electron reduction of quinones by Enterobacter cloacae NAD(P)H:nitroreductase: quantitative structure-activity relationships
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Endogenous Polyamines and Ethylene Biosynthesis in Relation to Germination of Osmoprimed Brassica napus Seeds under Salt Stress
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Photodynamic Inactivation of Candida albicans with Imidazoacridinones: Influence of Irradiance, Photosensitizer Uptake and Reactive Oxygen Species Generation
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Antitumor Effects of Vitamin D Analogs on Hamster and Mouse Melanoma Cell Lines in Relation to Melanin Pigmentation
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Relation between polyphenols, malondialdehyde, antioxidant capacity, lactate dehydrogenase and toxic elements in human colostrum milk
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Spin probe dynamics in relation to free volume in crystalline organics from ESR and PALS: N-tridecane
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Globalized Knowledge-Based Simulation-Driven Antenna Miniaturization Using Domain-Confined Surrogates and Dimensionality Reduction
PublikacjaDesign of contemporary antenna systems encounters multifold challenges, one of which is a limited size. Compact antennas are indispensable for the new fields of application such as inter-net of things or 5G/6G mobile communication. Still, miniaturization generally undermines elec-trical and field performance. When attempted through numerical optimization, it turns into a constrained problem with costly constraints requiring electromagnetic...
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Mutual Coupling Reduction in Antenna Arrays Using Artificial Intelligence Approach and Inverse Neural Network Surrogates
PublikacjaThis paper presents a novel approach to reduce undesirable coupling in antenna arrays using custom-designed resonators and inverse surrogate modeling. To illustrate the concept, two stand-ard patch antenna cells with 0.07λ edge-to-edge distance are designed and fabricated to operate at 2.45 GHz. A stepped-impedance resonator is applied between the antennas to suppress their mutual coupling. For the first time, the optimum values...
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Serum Cholesteryl Ester Transfer Protein (CETP) and Sortilin (SORT) in Patients with Psoriasis with Relation to Systemic Treatment
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A Text as a Set of Research Data. A Number of Aspects of Data Acquisition and Creation of Datasets in Neo-Latin Studies
PublikacjaIn this paper, the authors, who specialise in part in neo-Latin studies and the his-tory of early modern education, share their experiences of collecting sources for Open Research Data sets under the Bridge of Data project. On the basis of inscription texts from St. Mary’s Church in Gdańsk, they created 29 Open Research Data sets. In turn, the text of the lectures of the Gdańsk scholar Michael Christoph Hanow, Praecepta de arte...
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Dietary Hemp Seeds More Effectively Attenuate Disorders in Genetically Obese Rats than Their Lipid Fraction
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Low-Cost Method for Internal Surface Roughness Reduction of Additively Manufactured All-Metal Waveguide Components
PublikacjaIn this study, a novel low-cost polishing method for internal surface roughness reduction of additively manufactured components, developed for waveguide (WG) circuits operating in the millimeter frequency range is proposed. WG components fabricated using powder bed fusion (PBF) generally feature roughness of ten to fifty microns, which influences the increase of roughness-related conductor power losses having a major effect on...
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Effect of nitrogen doping on TiOxNy thin film formation at reactive high-power pulsed magnetron sputtering
PublikacjaThe paper is focused on a study of formation of TiOxNy thin films prepared by pulsed magnetron sputtering of metallic Ti target. Oxygen and nitrogen were delivered into the discharge in the form of reactive gases O2 and N2. The films were deposited by high-power impulse magnetron sputtering working with discharge repetition frequency f = 250 Hz at low (p = 0.75 Pa) and high (p = 10 Pa) pressure. The substrates were on floating...
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Evaluation of electrical parameters of traction supply system for complex railway traffic conditions, using simulation methods
PublikacjaDevelopment of electrified transport systems, railways modernization, expansion of urban transport networks, purchases of modern rolling stock causes that updating of electric traction supply system is necessary. This chapter presents an effective method for electrical parameters of traction supply system evaluation, using simulation methods.
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Fast Multi-Objective Optimization of Narrow-Band Antennas Using RSA Models and Design Space Reduction
PublikacjaComputationally efficient technique for multi-objective design optimization of narrow-band antennas is presented. In our approach, the corrected low-fidelity antenna model (obtained through coarse-discretization EM simulations) is enhanced using frequency scaling and response correction, sampled, and utilized to obtain a fast response surface approximation (RSA) antenna surrogate. The RSA model is constructed in the reduced design space....
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Generation of vorticity motion by sound in a chemically reacting gas and inversion of acoustic streaming in the non-equilibrium regime
PublikacjaBadanie dotyczy nieliniowych pobudzeń modu wirowego wywoływanych przez straty momentu pędu w gazie, w którym zachodzą reakcje chemiczne. Zostało wyprowadzone chwilowe dynamiczne równanie dla modu wirowego. Zawiera ono nieliniową siłę akustyczną co pokazuje, że powodem interakcji między modami akustycznym i wirowym jest nieliniowość. Równanie pozwala jako przyczynę ruchu wirowego rozważać zarówno dźwięk okresowy, jak i aperiodyczny....
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Instrumented end notched flexure - Crack propagation and process zonemonitoring Part II: Data reduction and experimental
PublikacjaA mode II instrumented end notched flexure three point bending (ENF) adhesion test is described. The adhesive joint consists of two aluminium alloy (AW7075-T6) plates bonded with a structural epoxy adhesive (Hysol EA 9395™). Strain gauges are attached to the outer surface (backface) of the substrates in the lengthwise direction to measure local surface strain during crack propagation. Simultaneously, load/displacement measurements...
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Study of the Operation of Synchronous Generator Voltage Regulator During the Creation of Post Blackout Start-up Path
PublikacjaThis paper presents the influence of automatic voltage regulator (AVR) of synchronous generator on the process of creation of post black-out start-up path. Two elements of AVR have a significant impact on this process: underexcitation limiter (UEL) and load compensation (LC). The authors present a theoretical investigation and simulation results that illustrate how the mentioned elements of AVR affect voltage levels in a power...
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A Fail-Safe NVRAM Based Mechanism for Efficient Creation and Recovery of Data Copies in Parallel MPI Applications
PublikacjaThe paper presents a fail-safe NVRAM based mechanism for creation and recovery of data copies during parallel MPI application runtime. Specifically, we target a cluster environment in which each node has an NVRAM installed in it. Our previously developed extension to the MPI I/O API can take advantage of NVRAM regions in order to provide an NVRAM based cache like mechanism to significantly speed up I/O operations and allow to preload...
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Modeling of a Quasi-Resonant DC Link Inverter Dedicated to Common-Mode Voltage and Ground Current Reduction
PublikacjaIn this paper, the modeling methodology of the AC drive system with a Parallel Quasi-Resonant DC Link Inverter (PQRDCLI) is described. A presented modeling approach is an attractive tool used for the effective evaluation of a common-mode (CM) voltage and grounds current reduction methods. Designed models of inverter, induction machine (IM), and cable are simple, thus the methods for parameter extraction are not complicated. Verification...
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A reactive algorithm for deducing nodal forwarding behavior in a multihop ad-hoc wireless network in the presence of errors
PublikacjaA novel algorithm is presented to deduce individual nodal forwarding behavior from standard end-to-end acknowledgments. The algorithm is based on a well-established mathematical method and is robust to network related errors and nodal behavior changes. The proposed solution was verified in a network simulation, during which it achieved sound results in a challenging multihop ad-hoc network environment.
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Influence of vision measurement system spatial configuration on measurement uncertainty, based on the example of electric traction application
PublikacjaTechnical diagnostics plays a significant role in ensuring operational reliability of electrified rail transport. The most critical point in the transmission of electric energy to vehicles is the sliding contact of the current collector with the traction network. For this reason, work is currently being carried on new measuring methods, whose appliance allows for more complete diagnostics of the contact line and current collectors,...
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Structure and thermoelectric properties of Cs-Bi-Te alloys fabricated by different routes of reduction of oxide reagents
PublikacjaCesium-bismuth-telluride polycrystalline materials were fabricated using a cost-effective method based on a reduction of oxide reagents, leading to a production of a material with good thermoelectric properties. Several samples with various initial stoichiometry were prepared by melting of oxide powders at 1050 °C, quenching, milling to powders and then reducing in pure hydrogen at 400 °C. Another concept was to obtain the CsBi4Te6...
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Assessing ecotoxicity and the endocrine potential of selected phthalates, BADGE and BFDGE derivatives in relation to environmentally detectable levels
PublikacjaThere is no doubt that the subject area of plasticmaterials (e.g., production of epoxy resins or polyesters) is inherently connected to issues concerning bisphenol A (BPA) and its analogues. Unfortunately, much less attention has been given to other compounds, which are also used for the production of these materials. Bisphenol A diglycidyl ether (BADGE) is a synthetic industrial compound obtained by a condensation reaction between...
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Cast polyurethanes obtained from reactive recovered polyol intermediates via crude glycerine decomposition process
PublikacjaIn this work, the possibility of applying intermediates from polyurethane waste recycling in polyurethane synthesis was presented. Polyurethanes were synthesised in a two-step method using a mixture of petrochemical polyol and glycerolysate, used as a reactive component, 4,4-diphenylmethane diisocyanate (MDI) and 1,4-buthanediol (BD). Glycerolysates were produced during decomposition of polyurethane elastomer by crude glycerine...
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Influence of reduction process on the structural and mechanical properties of (Pb,Bi)-(Si,Ge)-O oxide glasses
PublikacjaThe effect of the reduction process in H2 at 380 °C on the microstructure and elemental composition of a glass Bi0.4Pb0.2Si0.4Ox has been investigated. It has been shown that after reduction a clearly separated top layer with a thickness of approx. 50 µm was formed on the surface of the sample. This layer is depleted of oxygen and has higher electrical conductivity than the interior of the glass. It has also been found that some...