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Search results for: GREEN ANALYTICAL CHEMISTRY
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The Role of and the Place of Method Validation in the Quality Assurance and Quality Control (QA/QC) System
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Quality problems in determination of organic compounds in environmental samples, such as PAHs and PCBs
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Standard gas mixtures – indispensable reference materials in the analysis of gaseous media
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Gaseous standard mixtures – the challenge of obtaining small amounts of measurands
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Prospects for the Production, Research and Utilization of Reference Materials
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Validation of a sampling procedure
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Gradient reversed-phase high-performance chromatography of ionogenic analytes
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Critical approach to PLE technique application in the analysis of secondary metabolites in plants
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Statistical evaluation of the effectiveness of different extraction techniques for determining robenidyne levels in poultry feed.
PublicationPoprzez zastosowanie testu Kruskala-Wallisa i chemometrycznej techniki analizy podobieństwa porównano efektywność sześciu różnych technik ekstrakcji (wytrząsanie, ekstrakcja w aparacie Soxhleta, w aparacie Soxteca, wspomaganej ultradźwiękami, wspomaganej promieniowaniem mikrofalowym oraz przyspieszonej ekstrakcji rozpuszczalnikiem) na podstawie wyników odzysku robenidyny z próbek paszy dla ptaków. W zależności od zastosowanej techniki...
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Challenges in preparing honey samples for chromatographic determination of contaminants and trace residues
PublicationThe determination of contaminations and residues in honey is of growing concern over past few years, especially that these compounds can not only diminish beneficial properties of honey but more importantly, if present in significant amounts, can pose serious threat to human health. Since honey is characterized by complex composition of the matrix sample, it is often necessary to apply clean-up step, in order to eliminate interfering...
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The state of the art in the field of non-stationary instruments for the determination and monitoring of atmospheric pollutants
PublicationW artykule przedstawiono informacje oparte zarówno na danych literaturowych jak i własnych doświadczeniach dotyczące:-podstawowych tendencji rozwojowych w zakresie analityki i monitoringu zaneczyszczeń powietrza atmosferycznego-wymogów metrologicznych stawianych różnych typom urządzeń kontrolno-pomiarowych;-klasyfikacji analizatorów i monitorów wykorzystywanych w monitoringu powietrza.
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Miniaturized Passive Emission Chambers for In Situ Measurement of Emissions of Volatile Organic Compounds
PublicationThe results of many different studies have demonstrated unequivocally that the quality of indoor air is often much worse than that of atmospheric air. The presence of dangerous chemical compounds in indoor air can have an adverse impact on human health and cause numerous diseases of the respiratory and circulatory systems. Such harmful chemicals get into indoor air as a result of their emission from building and indoor materials....
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LC-MS and LC-NMR as Complementary Techniques for the Determination of Pharmaceuticals in Dosage Formulations
PublicationPharmaceuticals contain not only pharmacologically active compounds but also a range of excipients. The danger exists that impurities may also be present in such drugs, which may adversely affect their efficacy and even endanger patient health and life. Monitoring the composition of pharmaceutical products is therefore essential. The trace amounts of such impurities in pharmaceuticals are often identified and determined with liquid...
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The Use of Vegetables in the Biomonitoring of Cadmium and Lead Pollution in the Environment
PublicationLead and cadmium emitted from various anthropogenic sources have the ability to accumulate in tissues of living organisms. The phenomenon of accumulation of metals in the body is harmful and undesirable. On the other hand, the ability of plants to accumulate heavy metals from the individual elements of the environment has been used in biomonitoring of pollution. Leaf and root of vegetables have particular predisposition for accumulating...
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Developments in ultrasound-assisted microextraction techniques for isolation and preconcentration of organic analytes from aqueous samples
PublicationThe great potential of ultrasonic assistance in sample preparation, especially extraction, is being recognized. In this review, we discuss the applications of ultrasonic radiation in assisting microextraction. Topics covered include ultrasound-assisted emulsification microextraction, ultrasound-assisted-emulsification-dispersive liquid-liquid microextraction, and ultrasound-assisted hollow-fiber liquid-phase microextraction with...
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Recent achievements in element analysis of bee honeys by atomic and mass spectrometry methods
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Advances in assessing the elemental composition of distilled spirits using atomic spectrometry
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Critical evaluation of recent achievements in low power glow discharge generated at atmospheric pressure between a flowing liquid cathode and a metallic anode for element analysis by optical emission spectrometry
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Development of direct-current, atmospheric-pressure, glow discharges generated in contact with flowing electrolyte solutions for elemental analysis by optical emission spectrometry
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Impact and practicability of recently introduced requirements on elemental impurities
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Cold atmospheric plasma-induced chemical vapor generation in trace element analysis by spectrometric methods
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Determination of aminoglycoside antibiotics: Current status and future trends
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Element analysis of bee-collected pollen and bee bread by atomic and mass spectrometry – Methodological development in addition to environmental and nutritional aspects
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Application of gas chromatography to the analysis of spirit-based alcoholic beverages
PublicationSpirit-based beverages are alcoholic drinks, which production processes are dependent on the type and origin of raw materials. The composition of this complex matrix is difficult to analyze and scientists commonly choose a gas chromatography techniques for this reason. With a wide selection of extraction methods and detectors it is possible to provide qualitative and quantitative analysis for many chemical compounds with a various...
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Devices for the production of reference gas mixtures
PublicationFor many years there has been growing demand for gaseous reference materials, which is connected with development in many fields of science and technology. As a result, new methodological and instrumental solutions appear that can be used for this purpose. Appropriate quality assurance/quality control (QA/QC) must be used to make sure that measurement data are a reliable source of information. Reference materials are a significant...
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Perspectives and challenges in extracellular vesicles untargeted metabolomics analysis
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Determination of Zinc, Copper, and Mercury in Water Samples by Using Novel Micro Cloud Point Extraction and UV-Vis Spectrophotometry
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Recent Developments in Methods of Analysis for Fluoride Determination
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Developments in Methods of Analysis for Naphthalene Sulfonates
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Application of Microextraction Techniques Including SPME and MESI to the Thermal Degradation of Polymers: A Review
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Application of Dispersive Liquid-Liquid Microextraction in Narrow-Bore Tube for Preconcentration and Spectrophotometric Determination of Cadmium in Aqueous Samples
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Prospects of ionic liquids application in electronic and bioelectronic nose instruments
PublicationThis paper addresses the problem of application of ionic liquids to chemical sensors and biosensors being an integral part of the electronic and bioelectronic-type instruments. The design and principle of operation of the electronic and bioelectronic noses are compared. Both the benefits and shortcomings of the application of ionic liquids in these type of instruments are described. The prospects of the development and application...
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Determination of Selected Metals in Fruit Wines by Spectroscopic Techniques
PublicationThe determination of metals in different types of food and beverages samples has drawn significant attention due to several reasons with the most important one being the nutritional and toxic effects of these elements or their compounds. The knowledge of certain elements content in wines/fruit wines is of special interest due to their toxicity in case of excessive intake and also the effect they seem to have on the organoleptic...
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Solid Phase Microextraction: Apparatus, Sorbent Materials, and Application.
Publicationhe primary objective of this review article is to strategically screen and highlight the advancements in the area of solid phase microextraction (SPME). The plenty of review articles have been written on different aspects of SPME, this review is dedicated to provide the brief but clear overview of the research footprints so produced from SPME. Some of the key advancements in types and designs, coating materials, coating strategies,...
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The Use of Sensory Analysis Techniques to Assess the Quality of Indoor Air
PublicationThe quality of indoor air is one of the significant elements that influences people's well-being and health inside buildings. Emissions of pollutants, which may cause odor nuisance, are the main reason for people's complaints regarding the quality of indoor air. As a result, it is necessary to perform tests aimed at identifying the sources of odors inside buildings. The article contains basic information on the characteristics...
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Complementarity of electronic and vibrational circular dichroism based on stereochemical studies of vic-diols
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Application of electrochemical sensors and sensor matrixes for measurement of odorous chemical compounds
PublicationIn this paper describes the principle of operation of the electrochemical sensors and the sensor matrixes comprised of electrochemical sensors intended for measurement of odorous compounds. Critical comparison of these sensors’ advantages and disadvantages has been made. The fields of economy contributing to release of odours and the potential sources of their emission have been identified. Commercially available electrochemical...
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Application of Ionic Liquids in Amperometric Gas Sensors
PublicationThis article presents an analysis of available literature data on metrological parameters of the amperometric gas sensors containing ionic liquids as an electrolyte. Four mechanism types of signal generation in amperometric sensors with ionic liquid are described. Moreover, this article describes the influence of selected physico-chemical properties of the ionic liquids on the metrological parameters of these sensors. Some metrological...
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The Verification of the Usefulness of Electronic Nose Based on Ultra-Fast Gas Chromatography and Four Different Chemometric Methods for Rapid Analysis of Spirit Beverages
PublicationSpirit beverages are a diverse group of foodstuffs. They are very often counterfeited which cause the appearance of low quality products or wrongly labelled products on the market. It is important to find a proper quality control and botanical origin method enabling the same time preliminary check of the composition of investigated samples, which was the main goal of this work. For this purpose, the usefulness of electronic nose...
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Ionic liquids in the microextraction techniques: the influence of ILs structure and properties
PublicationIonic liquids (ILs) are composed entirely of ions thus they possess unique properties, including negligible volatility, a liquid state in a broad range of temperatures and ability to change them depending on the chosen type of anion and cation, which make ILs unique and useful for many applications in sample preparation techniques. A deeper understanding of the nature of ILs and the impact of their structure on their parameters...
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Advances in mass spectrometry for iron speciation in plants
PublicationIron is an important nutrient essential for plants and critical for human health. The state-of-the art of methods for iron speciation in cereal grains and plant fluids is critically reviewed. Particular attention is given to the latest developments in the coupling of HPLC with the parallel ICP MS and electrospray ionization (ESI) MS/MS detection, usually QTOF MS or Q-Orbitrap MS, for the identification and quantification of iron...
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Trace analysis - challenges and problems
PublicationW pracy przedstawiono podstawowe problemy związane z oznaczaniem składników śladowych i ultraśladowych w próbkach o złożonym składzie matrycy. W oparciu o dane literaturowe omówiono sposoby zapobiegania błędom jakimi mogą być obarczone wyniki oznaczeń końcowych.
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Denudation - a convenient method of isolation and enrichment of analytes
PublicationW pracy przedstawiono: podstawy teoretyczne techniki denudacyjnej; rozwiązania konstrukcyjne podstawowych typów urządzeń denudacyjnych; obszar praktycznego wykorzystania technik denudacyjnych.
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Sample preparation and chromatographic analysis of acidic herbicides in soils and sediments
PublicationW pracy przedstawiono różne techniki przygotowania próbek i oznaczania herbicydów z grupy pochodnych fenoli i pochodnych kwasów karboksylowych w próbkach gleby. Opisano wybrane metody wzbogacania i izolacji analitów, m. in.: ekstrakcję za pomocą wodnych roztworów zasad i rozpuszczalników organicznych płynem w stanie nadkrytycznym, wodą w stanie podkrytycznym, cieczą pod zwiększonym ciśnieniem, cieczą wspomaganą mikrofalami. Niski...
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Modern techniques of extraction of organic analytes from environmental matrices.
PublicationW pracy przedstawiono usystematyzowane informacje dotyczące dostępnych jak i nowych technik izolacji i wzbogacania analitów organicznych przed etapem oznaczeń końcowych.
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Preparation of gaseous standard mixtures: methods for controlling the amount of components generated in the process of thermal decomposition of immobilized compounds.
PublicationGazowe mieszaniny wzorcowe odgrywają ważną rolę w ocenie metod analitycznych i urządzeń pomiarowych. W tym przypadku gazowe mieszaniny wzorcowe mogą być traktowane jako specjalny rodzaj materiału odniesienia.Proces walidacji wymaga użycia tzw. matrycowych materiałów odniesienia. Wybór techniki umożliwiającej uzyskanie gazowej mieszaniny wzorcowej o żądanych parametrach użytkowych zależy od natury składników mierzonych i gazu...
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State of the art in sample preparation for human breast milk metabolomics—merits and limitations
PublicationHuman breast milk (HBM) contains metabolites that are diverse in chemical structure and concentration. These metabolites range from high-abundance to low-abundance compounds and from polar to nonpolar. This complex nature of HBM makes HBM samples difficult to analyze, especially in global metabolomic studies for the determination and characterization of complete sets of metabolites. In this review, the state of the art in sample...
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Multi-objective optimization of microextraction procedures
PublicationOptimization of extraction process requiresfinding acceptable conditions for many analytes and goodperformance in terms of process time or solvent consumption. These optimization criteria are oftencontradictory to each other, the performance of the system in given conditions is good for some criteriabut poor for others. Therefore, such problems require special assessment tools that allow to combinethese contradictory criteria into...
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Olfactory receptor-based biosensors as potential future tools in medical diagnosis
PublicationThe detection of biomarkers is the future of non-invasive medical diagnosis and screening. Discovery and identification of reliable disease specific volatile organic compounds is dependent on repeatable, accurate analysis of trace level gaseous analytes mainly in breath samples. Natural variety of the olfactory systems and the compounds capable of gas molecules binding creates wide possibilities of acquisition and implementation...
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Evaluation of Langmuir and Freundlich Isotherms for Removal of Cephalexin and Tetracycline Antibiotics By Sistan Sand from Water and Wastewater Samples
PublicationIn this research, Sistan sand was used as a natural and inexpensive sorbent for removal of cephalexin and tetracycline antibiotics from water and wastewater samples. For a concentration 60.0 mg L-1 of cephalexin, optimum removal conditions were: pH of the sample 3.0, adsorbent amount 1.0 g, contact time 20.0 min, added amount of sodium chloride to adjust the ionic strength of the solution 7.0 g L-1. Langmuir isotherm was the best...