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Search results for: thin layer chromatography
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Preparation and Characterization of Microsphere ZnO ALD Coating Dedicated for the Fiber-Optic Refractive Index Sensor
PublicationWe report the fabrication of a novel fiber-optic sensor device, based on the use of a microsphere conformally coated with a thin layer of zinc oxide (ZnO) by atomic layer deposition (ALD), and its use as a refractive index sensor. The microsphere was prepared on the tip of a single-mode optical fiber, on which a conformal ZnO thin film of 200 nm was deposited using an ALD process based on diethyl zinc (DEZ) and water at 100 °C....
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In-situ monitoring of electropolymerization processes at boron-doped diamond electrodes by Mach-Zehnder interferometer
PublicationIn this work, the Mach-Zehnder interferometer was designed to monitor the electrochemical processes conducted at boron-doped diamond electrode surface. The diamond electrodes were synthesized via Microwave Plasma-Assisted Chemical Vapor Deposition on optical grade quartz glass. The achieved transmittance in working are of diamond electrodes reached 55 %. A cage system-based Mach-Zehnder interferometer was used which allowed the...
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Area-Averaged Surface Moisture Flux over Fragmented Sea Ice: Floe Size Distribution Effects and the Associated Convection Structure within the Atmospheric Boundary Layer
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Expanded graphite assistant construction of gradient-structured char layer in PBS/Mg(OH)2 composites for improving flame retardancy, thermal stability and mechanical properties
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Properties comparison of rubber and three layer PTFE-NBR-bronze water lubricated bearings with lubricating grooves along full bush circumference based on experimental tests
PublicationWater lubricated bearings have been in industrial use for well over a century. During the last decade their traditional range has been expanded with new, modern products. Despite that fact, certain solutions continue to employ the standard rubber bearing with lubricating grooves located along entire bush circumference. The work presents experimental research conducted on comparable sliding bearings with lubrication grooves along...
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Wpływ stanu warstwy wierzchniej na mikrostrukturę i właściwości korozyjne stopu SUPERSTON = Influence of the state of surface layer on microstructure and corrosion properties of SUPERSTON alloy
PublicationW artykule przedstawiono rezultaty nadtapiania laserowego w warunkach kriogenicznych stopu SUPERSTON. Dokonano oceny mikrostruktury powierzchni i przekroju stopu SUPERSTON po obróbce laserowej. Określono właściwości stopu, które porównano ze stanem powierzchni po nadtapianiu oraz nadtapianiu i szlifowaniu.
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Comparison of mouse plasma and brain tissue homogenate sample pretreatment methods prior to high-performance liquid chromatography for a new 1,2,4-triazole derivative with anticonvulsant activity
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Dispersive solid-phase extraction using multi-walled carbon nanotubes combined with liquid chromatography–mass spectrometry for the analysis of β-blockers: Experimental and theoretical studies
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Photocatalytic degradation of acetaldehyde in high temperature reaction chamber
Open Research DataThis dataset contains chromatograms recorded during the decomposition of acetaldehyde in a high-temperature reaction chamber under UV irradiation using TiO2 (titanium dioxide) as photocatalysts. It includes data on the influence of flow rate, TiO2 (titanium dioxide) filling the entire reactor, a thin layer of TiO2 (titanium dioxide) supported on KBr...
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Determination of the content of saccharides and ethanol in samples of fermented beverages
Open Research DataThe data set presents the results of measurements of the content of mono- and disaccharides: glucose, maltose, fructose and ethanol in samples of beverages fermented by high performance liquid chromatography (HPLC-RID).
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Hemocompatibility of nanocrystalline diamond layers
Open Research DataThe biocompatibility of the diamond films were investigated with whole human blood samples. Blood used in this study was drawn from 10 healthy human patients of different age, sex, and blood group. A 2 ml samples were collected into standard tubes with EDTA anticoagulation agent. Blood was used within 6 hours from the collection time. A reference blood...
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SEM images of dewetted gold films
Open Research DataGold nanostructures were prepared on silicon - Si(111) as a substrate. as a result of dewetting process. Thin golds films were deposited using a table-top dc magnetron sputtering coater under pure Ar plasma conditions . The Au target had 99.99% purity, the rate of Au layer deposition was about 0.4 nm·s−1 and the incident power was 32 W. The thickness...
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Oxidation of silver nanostructures
Open Research DataSilver nanostructures were prepared on Si substrate. Thin Ag films (2 and 6 nm thickness) were deposited using a tabletop dc magnetron sputtering coater (EM SCD 500, Leica) in pure Ar plasma. The Ag target was of 99.99% purity, the rate of layer deposition was about 0.4 nm·s−1 , and the incident power was in the range of 30–40 W. The layer thickness...
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On local buckling of cold-formed channel members
PublicationThe paper deals with local buckling of the compressed flanges of cold-formed thin-walled channel beams subjected to pure bending or axially compressed columns. Arbitrarily shaped flanges of open cross-sections and the web-flange interactions are taken into account. Buckling deformation of a beam flange is described by displacement related to torsion of the flange about the line of its connection with the web. Total potential energy...
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<title>Software layer for SIMCON ver. 2.1. FPGA based LLRF control system for TESLA FEL part I: system overview, software layers definition</title>
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Surface characteristics of glass fibres covered with an aluminum layer after a chemical modification process using secondary ion mass spectrometry (SIMS) and atomic force microscopy (AFM)
PublicationPrzedstawiono wyniki z badań powierzchni modyfikowanych włókien szklanych (przed i po procesie chemicznej modyfikacji ich powierzchni), które są kandydatem na przyszły oryginalny bezmatrycowy materiał odniesienia lotnych analitów etenu (C2H4) metodami spektrometrii mas jonów wtórnych oraz mikroskopii sił atomowych. Badania miały na celu obserwację zmian oraz procesów, jakie zaszły na powierzchni włókien szklanych pokrytych...
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Analiza budowy i własności napoiny wykonanej z proszku 1606 ze stopu kobaltu = Morphology and property analyze of the layer made of 1606 powder of cobalt alloy
PublicationW pracy analizowano budowę i zmiany zachodzące w strukturze napawanej laserowo warstwy wykonanej ze stopu kobaltu pod wpływem korozyjnego środowiska gazów spalinowych. Warstwa wykazywała się znaczną niejednorodnością chemiczną i składem różnym od założonego jednakże te nieprawidłowości nie wpłynęły znacząco na jej odporność korozyjną w gorących gazach spalinowych.
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Anti-plane shear waves in an elastic strip rigidly attached to an elastic half-space
PublicationWe consider the anti-plane shear waves in a domain consisting of an infinite layer with a thin coating lying on an elastic half-space. The elastic properties of the coating, layer, and half-space are assumed to be different. On the free upper surface we assume the compatibility condition within the Gurtin–Murdoch surface elasticity, whereas at the plane interface we consider perfect contact. For this problem there exist two possible...
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Hydrophobic deep eutectic solvents as “green” extraction media for polycyclic aromatic hydrocarbons in aqueous samples
PublicationThe paper presents novel nonionic and hydrophobic deep eutectic solvents which were synthesized from natural compounds, i.e., thymol, ±camphor, decanoic and 10-undecylenic acids. Fundamental physicochemical properties of the synthesized deep eutectic solvents were determined, followed by their application as extractants in ultrasound-assisted dispersive liquid-liquid microextraction to isolate and enrich polycyclic aromatic hydrocarbons...
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Determination of tributylotin (TBT) in marine sediment using pressurised liquid extraction-gas chromatography-isotope dilution mass spectrometry (PLE-GC-IDMS) with a hexane-tropolone mixture
PublicationOpracowano metodę oznaczania zawartości tributylocyny w próbkach osadu morskiego. Na etapie izolacji zastosowano technikę przyspieszonej ekstrakcji za pomocą roztworu tropolonu w heksanie.Na etapie oznaczeń końcowych wykorzystano technikę chromatografii gazowej, stosując metodę spektrometrii mas rozcieńczenia izotopowego. Wyznaczono parametry walidacyjne opracowanej metody: granicę wykrywalności, precyzję, poprawność i niepewność.
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Application of headspace-solid phase microextraction followed by gas chromatography-mass spectrometry to determine short-chain monocarboxylic acids in cattle farm wastewater and waste landfill leachates
PublicationZaproponowano metodykę oznaczania krótkołańcuchowych kwasów monokarboksylowych w ściekach z hodowli bydła i odciekach ze składowisk zawierających organiczne odpady, oparta na technice mikroekstrakcji do fazy stacjonarnej z fazy nadpowierzchniowej próbek ciekłych, w połączeniu ze sprzężonym układem GC-MS.
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High-performance liquid chromatography thermodynamic study of new potential antiepileptic compounds on a cholesterol column using isocratic elution with methanol/water and acetonitrile/water eluent systems
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Quantification of key red blood cell folates from subjects with defined MTHFR 677C>T genotypes using stable isotope dilution liquid chromatography/mass spectrometry
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Determination of tributyltin (TBT) in marine sediment using pressurised liquid extraction–gas chromatography–isotope dilution mass spectrometry (PLE–GC–IDMS) with a hexane–tropolone mixture
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A nontargeted approach to determine the authenticity of Ginkgo biloba L. plant materials and dried leaf extracts by liquid chromatography-high-resolution mass spectrometry (LC-HRMS) and chemometrics
PublicationThe lack of stringent regulations regarding raw materials for herbal supplements used for medicinal purposes has been a constant challenge in the industry. Ginkgo biloba L. leaf extracts attract consumers because of the supposed positive effect on mental performance and memory. Supplements are produced using dried leaf materials and standardized leaf extracts such as EGb 761. Adulteration of Ginkgo biloba L. plants and extracts...
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ODOUR IMPACT OF MUNICIPAL LANDFILL MONITORED WITH ULTRA-FAST GAS CHROMATOGRAPHY = ODDZIAŁYWANIE ZAPACHOWE SKŁADOWISKA ODPADÓW KOMUNALNYCH MONITOROWANE ZA POMOCĄ ULTRA SZYBKIEJ CHROMATOGRAFII GAZOWEJ
PublicationPrzedstawiono wyniki badań klasyfikacji próbek powietrza atmosferycznego pobranych wokół miejskiego składowiska odpadów komunalnych w okresie zimowym i letnim pod kątem uciążliwości zapachowej. Badania przeprowadzono przy pomocy komercyjnego elektronicznego nosa typu Fast/Flash GC - HERACLES II. Klasyfikację próbek powietrza atmosferycznego pobranych z różnych kierunków względem wysypiska śmieci przeprowadzano przy użyciu dyskryminacyjnej...
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Preparation and evaluation of 1,3-alternate 25,27-dibenzyloxy-26,28-bis-[3-propyloxy]-calix[4]arene - bonded silica stationary phase for high performance liquid chromatography
PublicationOtrzymano nową fazę stacjonarną na bazie dibenzyloksy pochodnej kaliks[4]arenu w konformacji 1,3-naprzemianległej, chemicznie związaną z żelem krzemionkowym. Przeprowadzano badania selektywności i sprawności tej fazy w rozdzielaniu izomerów konstytucyjnych benzenu i pochodnych fenoli. Zaprezentowano wyniki badania wpływu pH fazy ruchomej oraz stężenia metanolu na zdolność rozdzielczą nowej fazy stacjonarnej.
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Comparison of XPS spectra of Ag3d for silver nanostructures and bulk material
Open Research DataAg nanostructures were prepared on borosilicate glass (Corning 1737F) and Si substrates. In both cases, the substrateswere cleaned with acetylacetone and then rinsed in ethanol. Thin Ag films (2 and 6 nm thickness) were deposited using a tabletop dc magnetron sputtering coater (EM SCD 500, Leica) in pure Ar plasma (argon, Air Products 99.999%). The...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,1 V at 420 mA. Sample 103.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,1 V and discharged to 10 mV by constant current 420 mA. Sample 103. Voltage was increased to accelerate the ageing process.The images were taken with thermographic camera VigoCAM V50. The sample...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 732 mA. Sample J51.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 732 mA. Sample J51.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 366 mA. Sample J51.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 366 mA. Sample J51.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,2 V at 420 mA. Sample 103.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,2 V and discharged to 10 mV by constant current 420 mA. Sample 103. Voltage was increased to accelerate the ageing process.The images were taken with thermographic camera VigoCAM V50. The sample...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,8 V at 420 mA. Sample 103.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,8 V and discharged to 10 mV by constant current 420 mA. Sample 103. Voltage was increased to accelerate the ageing process.The images were taken with thermographic camera VigoCAM V50. The sample...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 1098 mA. Sample J51.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 1098 mA. Sample J51.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 480 mA. Sample 103.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 480 mA. Sample 103. The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 915 mA. Sample J51.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 915 mA. Sample J51.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 108 mA. Sample J51.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 108 mA. Sample J51.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 549 mA. Sample J51.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 549 mA. Sample J51.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,5 V at 420 mA. Sample 103.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,5 V and discharged to 10 mV by constant current 420 mA. Sample 103. Voltage was increased to accelerate the ageing process.The images were taken with thermographic camera VigoCAM V50. The sample...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,0 V at 250 mA. Sample 24.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,0 V and discharged to 10 mV by constant current 250 mA. Last experiment with sample 24The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,5 V at 180 mA. Sample 24
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,5 V and discharged to 10 mV by constant current 180 mA. The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface emission....
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 80 mA. Sample 41.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 80 mA. Sample 41.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,5 V at 241 mA. Sample 24
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,5 V and discharged to 10 mV by constant current 241 mA. The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface emission....
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,5 V at 80 mA. Sample 24
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,5 V and discharged to 10 mV by constant current 80 mA. The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface emission....
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,5 V at 301 mA. Sample 24
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,5 V and discharged to 10 mV by constant current 301 mA. The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface emission....
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 160 mA. Sample 41.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 160 mA. Sample 41.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,5 V at 120 mA. Sample 24
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,5 V and discharged to 10 mV by constant current 120 mA. The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface emission....
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 112 mA. Sample 71.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 112 mA. Sample 71.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 108 mA. Sample 61.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 108 mA. Sample 61.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 2,7 V at 135 mA. Sample 61.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 2,7 V and discharged to 10 mV by constant current 135 mA. Sample 61.The images were taken with thermographic camera VigoCAM V50. The sample was covered by black graphite paint to ensure uniform surface...