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Search results for: NMR PROTONOWY
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Structural and luminescence investigation of GeO2-PbO-Bi2O3-SrF2 glasses doped with Eu3+, Tb3+ and Tm3+ ions
PublicationThe GeO2-PbO-Bi2O3-SrF2 (GePbBiSr) glass systems doped with Eu3 +, Tb3 +, Tm3 + and triply-doped with Eu3 +/Tb3 +/Tm3 + ions were successfully synthesized. Their structural and luminescent properties have been investigated with various techniques. Obtained results indicate that these glass systems are suitable materials for the RE3 + ions hosts. RE3 + ions can be excited by single UV light wavelength (355/378/395 nm) and simultaneously...
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Novel Approaches of Using of Spirulina Platensis in Natural Rubber Based Composites
PublicationThe aim of this work was to investigate the influence of Spirulina (Spirulina platensis) as a natural filler on the curing characterization, morphology and mechanical, thermomechanical and thermal properties of natural rubber (NR) based composites. Spirulina was introduced into NR mixture in amount of 0 phr, 10 phr and 30 phr. The vulcanization process was carried out at the determined process condition by using hydraulic press...
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Dylematy polskiej polityki kursowej w dobie globalizacji. W: Wewnętrzne i zewnętrzne determinanty procesów decyzyjnych w zarządzaniu finansami przed-siębiorstw. Monografia Katedry Finansów nr 1. Gdańsk: Kated. Finan. Wydz.Zarz. i Ekon. P. Gdań.**2003 s. 107-118, 1 rys. 3 tab. bibliogr. 21 poz.
PublicationArtykuł prezentuje kwestię doboru odpowiedniej polityki kursowej w dobie globalizacji. Jest w nim również dokonana analiza możliwych rozwiazań kur- sowych w Polsce na drodze do Unii Gospodarczej i Walutowej.
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Planowanie finansowe a strategia przedsiębiorstwa. W: Wewnętrzne i zewnę-trzne determinanty procesów decyzyjnych w zarządzaniu finansami przed-siębiorstw. Monografia Katedry Finansów nr 1. Gdańsk: Kated. Finan. Wydz.Zarz. i Ekon. P. Gdań.**2003 s. 5-17, 1 rys. 1 tab. 1 bibliogr. 8 poz.
PublicationArtykuł obejmuje studium problematyki planowania finansowego wzbogaconego teoriami zarządzania strategicznego. Autor identyfikuje kategorie planowania w świetle koncepcji rozumienia strategii przedsiębiorstwa. Na tej podstawie określa nowe związki i definicje.
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Doskonalenie informacji o kosztach jednostek służby zdrowia w celu tworze- nia podstaw decyzyjnych. W: Wewnętrzne i zewnętrzne determinanty procesówdecyzyjnych w zarządzaniu finansami przedsiębiorstw. Monografia KatedryFinansów nr 1. Gdańsk: Kated. Finan. Wydz.Zarz. i Ekon. P. Gdań.**2003 s.31-38 bibliogr. 11 poz.
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EKSPERTYZA W ZAKRESIE POPRAWY DOSTĘPNOŚCI ZGODNIE Z ZARZĄDZENIEM PREZYDENTA MIASTA GDYNI NR 10740/13/VI/U Z DN. 17 MAJA 2013 W SPRAWIE PRZYJĘCIA STANDARDÓW DOSTĘPNOŚCI DLA MIASTA GDYNI. Dotyczy: projektu węzła integracyjnego i publicznego parkingu związanego z obsługą drogową w Gdyni Chyloni.
PublicationOcena dostępności do potrzeb osób z niepełnosprawnościami projektu integracyjnego węzła komunikacyjnego w Gdyni Chyloni. Sprawdzenie zgodności z wytycznymi Standardów Dostępności.
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OPINIA TECHNICZNA nr 1/PG Sprawowanie nadzoru naukowo-technicznego podczas opracowywania projektów obiektów hydrotechnicznych, mostowych i drogowych w ramach realizacji przedsięwzięcia pn. „Budowa drogi wodnej łączącej Zalew Wiślany z Zatoka Gdańską” Opinia nt. rozwiązań technicznych przedstawionych w koncepcji przekopu w lokalizacji Nowy Świat
PublicationOpinię przygotowano w ramach prowadzonego nadzoru naukowo-technicznego podczas opracowywania projektów obiektów hydrotechnicznych, mostowych i drogowych w ramach realizacji przedsięwzięcia pn. „Budowa drogi wodnej łączącej Zalew Wiślany z Zatoka Gdańską”.
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The influence of the type of halogen substituent and its position on the molecular conformation, intermolecular interactions and crystal packing for a series of 1-benzoyl-3-(halogenophenyl)thioureas
PublicationBy the reaction of benzoyl chloride, potassium isothiocyanate and the appropriate halogenoaniline, i.e. 2/3/4-(bromo/iodo)aniline, we have obtained five new 1-benzoyl-3-(halogenophenyl)thioureas, namely, 1-benzoyl-3-(2-bromophenyl)- thiourea and 1-benzoyl-3-(3-bromophenyl)thiourea, C14H11BrN2OS, and 1-benzoyl-3-(2-iodophenyl)thiourea, 1-benzoyl-3-(3-iodophenyl)thiourea and 1-benzoyl-3-(4-iodophenyl)thiourea, C14H11IN2OS. Structural...
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Unexpected Z/E isomerism of N-methyl-O-phosphothioyl benzohydroxamic acids, their oxyphilic reactivity and inertness to amines
PublicationThiophosphinoylation of N-methyl p-substituted benzohydroxamic acids using disulfanes (method A) or diphenylphosphinothioyl chloride (method B) provides only one conformer of the respective O-phosphothioyl derivative (Xray and NMR analysis). Undergoing the P-transamidoxylation reaction is an evidence of the reversibility of thiophosphinoylation. Only those products containing strong EWG substituents in the aroyl residue or bulky...
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Ipertrofan Revisited—The Proposal of the Complete Stereochemistry of Mepartricin A and B
PublicationBeing a methyl ester of partricin, the mepartricin complex is the active substance of a drug called Ipertrofan (Tricandil), which was proven to be useful in treatment of benign prostatic hyperplasia and chronic nonbacterial prostatitis/chronic pelvic pain syndrome. Nevertheless, no direct structural evidence on the stereochemistry of its components has been presented to date. In this contribution, we have conducted detailed, NMR-driven...
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Technology of an adhesive silicone film as drug carrier in transdermal therapy I. Analytical methods used for characterization and design of the universal elastomer layers
PublicationSilicone polymers possess unique properties, which make them suitable for many different applications, for example in the pharmaceutical and medical industry. To create an adhesive silicone film, the appropriate silicone components have to be chosen first. From these components two layers were made: an adhesive elastomer applied on the skin, and a non-adhesive elastomer on the other side of the film. The aim of this study was...
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Charakterystyka frakcji oleju palmowego otrzymanych na drodze wielostopniowej krystalizacji
PublicationPrzeprowadzono wielostopniową frakcjonowaną krystalizację oleju palmowego z acetonu. Stosując temperatury krystalizacji od 25 do 0C, otrzymano siedem frakcji znacznie różniących się budową chemiczną i właściwościami fizycznymi. We frakcjach oznaczono skład kwasów tłuszczowych metodą GLC oraz zawartość triacylogliceroli metodą HPLC. Zbadano też właściwości fizyczne otrzymanych frakcji. Oznaczono zawartości fazy stałej metodą pulsacyjnego...
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Unsaturated, biobased polyesters and their cross-linking via radical copolymerization
PublicationBiobased, unsaturated polyesters derived from isosorbide, maleic anhydride and succinic acid were synthesized and characterized. The presence of maleic anhydride units in the structure of the polyesters allowed converting them into cured coatings by radical copolymerization with cross-linking agents such as 2-hydroxyethyl methacrylate, N-vinyl-2-pyrrolidinone, acrylic acid or methacrylamide. The investigated polyesters were obtained...
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Reactivity of Phosphanylphosphinidene Complex of Tungsten(VI) toward Phosphines: A New Method of Synthesis of catena-Polyphosphorus Ligands
PublicationThe reactivity of an anionic phosphanylphosphinidene complex of tungsten(VI), [(2,6-i-Pr2C6H3N)2(Cl)- W(η2-t-Bu2P=P)]Li·3DME toward PMe3, halogenophosphines, and iodine was investigated. Reaction of the starting complex with Me3P led to formation of a new neutral phosphanylphosphinidene complex, [( 2,6-i-Pr2C6H3N)2(Me3P)W(η2-t-Bu2P=P)]. Reactions with halogenophosphines yielded new catena-phosphorus complexes. From reaction with...
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The influence of different glycerine purities on chemical recycling process of polyurethane waste and resulting semi‐products
PublicationChemical recycling is the most favourable recycling method due to the possibility of polyol recovery. This work is dedicatedto the utilisation of crude glycerine and polyurethane waste. It aims at determining the impact of the use of glycerine fromthe production of biodiesel with various degrees of purity as a cleavage agent on the decomposition process of polyurethanefoam. The influence of glycerine purit y on the chemical structure...
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Thermo-Chemical Decomposition Study of Polyurethane Elastomer Through Glycerolysis Route with Using Crude and Refined Glycerine as a Transesterification Agent
PublicationDue to the increasing amount of polyurethane waste, chemical recycling of these materials is a topic of growing interest for many researchers. The primary pur- pose of polyurethane feedstock recycling is to recover the starting polyol. In this study glycerolysis using glycerine from two sources and two purity grades is proposed as a method of chemical recycling. The main effort of this paper focuses on the employment of commercial...
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Preparation and characterization of natural rubber composites highly filled with brewers' spent grain/ground tire rubber hybrid reinforcement
PublicationBrewers' spent grain (BSG) and ground tire rubber (GTR) were applied as low-cost hybrid reinforcement natural rubber (NR). The impact of BSG/GTR ratio (in range: 100/0, 75/25, 50/50, 25/75 and 0/100 phr) on processing and performance properties of highly filled natural rubber composites was evaluated by oscillating disc rheometer, Fourier-transform infrared spectroscopy, thermogravimetric analysis, scanning electron microscopy,...
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Oxidation kinetics of Zircaloy-4 alloy at 673 K determined by GDOES technique
PublicationOxidation of zirconium alloys is a process that takes place during the operation of nuclear reactors and is essential for assessing the durability of fuel claddings. The present study was aimed to determine the oxidation kinetics of the Zircaloy-4 alloy using GDOES (glow discharge optical emission spectroscopy) at temperature 673 K corresponding to the conditions of use of fuel pellets. The tests were performed on non-oxidized...
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UZUPEŁNIENIE TEKSTU ZALECEŃ DLA OPRACOWANIA: Ekspertyza techniczna dotycząca przestrojenia konstrukcji stadionu żużlowego w Zielonej Górze z analizą numeryczną w formalizmie metody elementów skończonych
PublicationPrzedmiotem orzeczenia jest wskazanie metody (lub metod) przestrojenia konstrukcji stadionu żużlowego w celu poprawy jego dynamiki przy obciążeniu synchronicznym skokiem grupy ludzi. Zakres prac badawczych obejmował:określenie częstości i postaci drgań stadionu ze wzmocnieniem słupkami (stan aktualny stadionu żużlowego) oraz wykonanie symulacji obciążenia synchronicznym skokiem grupy ludzi (wzmocnienie nr 1); określenie częstości...
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Ekspertyza techniczna dotycząca przestrojenia konstrukcji stadionu żużlowego w Zielonej Górze z analizą numeryczną w formalizmie metody elementów skończonych
PublicationPrzedmiotem orzeczenia jest wskazanie metody (lub metod) przestrojenia konstrukcji stadionu żużlowego w celu poprawy jego dynamiki przy obciążeniu synchronicznym skokiem grupy ludzi. Zakres prac badawczych obejmował: określenie częstości i postaci drgań stadionu ze wzmocnieniem słupkami (stan aktualny stadionu żużlowego) oraz wykonanie symulacji obciążenia synchronicznym skokiem grupy ludzi (wzmocnienie nr 1); określenie częstości...
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Unifying classical and quantum key distillation
PublicationPrzypuśćmy, że dwie oddalone od siebie osoby, Alicja i Bob, oraz osoba z nimi niewspółpracująca, Ewa, mają dostęp do systemów kwantowych przygotowanych w stanie rho_ABE. Ponadto Alicja i Bob mogą używać lokalnych operacji i uwiarygodnionej komunikacji publicznej. Celem Alicji i Boba jest ustanowienie klucza, który nie będzie znany Ewie. Nasze badania inicjują podejście do wspomnianego zagadnienia oparte na unifikacji dwóch standardowych...
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Fluorescence emission of carbon disulfide in low energy electron collision.
PublicationZbadano widma emisyjne dwusiarczku węgla w zakresie widmowym od 235 nm do575 nm wzbudzane zderzeniami elektronów o energii 9.7eV I 15eV. W otrzymanych widmach największe natężenie miały pasma pochodzące z dysocjacji cząsteczek dwusiarczku węgla.
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Man in Early Islamic Philosophy: Al-Kindi and Al-Farabi
PublicationMan was, neither for Al-Kindi, nor for Al-Farabi, a clearly isolated object of philosophical reflection. This does not mean, however, that both Islamic philosophers were not at all concerned with the uniqueness of man, his nature or the purpose of his existence. In order to understand and analyze in depth the philosophies of man voiced by Al-Kindi and Al-Farabi, one must focus primarily on their epistemologies, on their philosophical...
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Empirical investigation on labour market interactions in an enlarged Europe
PublicationThis paper proposes an empirical assessment of economic interactions between the labour markets ofthe integrating EU over the period of time 1995-2005. Drawing on recently made available industrystatistics, we provide a sector level study (13 tradable sectors, including manufacturing and services),analysing the contemporary evolution of domestic and trade partners' employment levels. Given theintensification of trade relations...
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Economic growth, structural change and quality upgrading in New Member States
PublicationThe purpose of this research is to present the recent developments concerning structural change and productivity growth in New Member States and the role played in such process by country specific factors. We focus on ten countries (NMS-10) which joined the EU in 2004 and analyze productivity dynamics of their labor structures between the years 1995 and 2005 in a comparative setting versus EU-15 economies. NMS-10 have gone through...
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Towards spectral sensitivity curve for two-photon vision mechanism
PublicationAbstract Purpose: The perceived brightness of different visible light sources can be compared with photometric units based on the standardized luminosity curves (300-780nm range). As reported previously (PNAS 111(50), pp. E5445-E5454 (2014)), near-infrared (NIR) radiation can cause isomerization of visual pigments by one- or two-photon absorption. The perceived color of the stimulus is red in the case of one-photon vision (1PV)...
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Trunked Radio Solutions for Special Application
PublicationIn the paper modern concepts of radio communication trunking-dispatch systems for special applications are presented. Basic standards of TETRA, DMR, and cdma2000 are mentioned. The aim of the paper is to present innovative trunking solutions based on the LTE system working both in FDD and TDD mode. The architecture of LTE trunked radio is shown as well as new services possible to implementation are described. The way of TETRA and...
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Systemy dyspozytorskie nowej generacji - system trankingowy LTE
PublicationReferat dotyczy rozwiązań systemów trankingowych-dyspozytorskich opartych na infrastrukturze LTE. W pierwszej części omówiono rozwiązanie w postaci odrębnego systemu trankingowego LTE, natomiast w drugiej opisano propozycję rozwiązania systemu trankingowego w ramach ogólnie dostępnej sieci LTE. Scharakteryzowano również problem integracji takiego systemu z systemem TETRA lub DMR.
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Optical properties of thin TiO2 film deposited on the fiber optic sensor head
PublicationThe presented study was focused on investigation of the titanium dioxide (TiO2) thin film deposited on the fiber tip. The intention of this investigation was using TiO2 film in the construction of the optical fiber sensor head. In the demonstrated construction TiO2 thin layer was deposited on the tip of a commonly used telecommunication single mode optical fiber (SMF-28) by means of the Atomic Layer Deposition (ALD). Thickness...
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Strefa podmiejska w warunkach zrównoważonego rozwoju.
PublicationNR DOKUM: D 73137
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Investigation on polypropylene friction stir joint: effects of tool tilt angle on heat flux, material flow and defect formation
PublicationTool tilt angle (TTA) is a critical factor that can control material flow in polymeric materials' friction stir joining (FSJ). This study selected a TTA range between 0° to 4° for FSJ of polypropylene (PP) polymer sheet. A modified computational fluid dynamic (CFD) technique was implemented to gain a deep understanding of the effects of TTA during FSJ of PP. The PP joint's internal flow, defect formation, heat generation, and tensile...
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Novel design of sodium alginate based absorbable stent for the use in urethral stricture disease
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Synthesis and characterization of mechanically alloyed nanostructured ternary titanium based alloy for bio-medical applications
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Estimation, optimization and analysis based investigation of the energy consumption in machinability of ceramic-based metal matrix composite materials
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Effect of ball-milling process parameters on mechanical properties of Al/Al2O3/collagen powder composite using statistical approach
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Tool wear, surface roughness, cutting temperature and chips morphology evaluation of Al/TiN coated carbide cutting tools in milling of Cu–B–CrC based ceramic matrix composites
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Effect of mixing method and particle size on hardness and compressive strength of aluminium based metal matrix composite prepared through powder metallurgy route
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Experimental investigation of selective laser melting parameters for higher surface quality and microhardness properties: taguchi and super ranking concept approaches
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Experimental investigation and optimization of compression moulding parameters for MWCNT/glass/kevlar/epoxy composites on mechanical and tribological properties
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Improvement of machinability of Ti and its alloys using cooling-lubrication techniques: a review and future prospect
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Experimental investigations and prediction of WEDMed surface of nitinol SMA using SinGAN and DenseNet deep learning model
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Effect of alumina oxide nano-powder on the wear behaviour of CrN coating against cylinder liner using response surface methodology: processing and characterizations
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Material independent effectiveness of workpiece vibration in μ-EDM drilling
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Investigation of machinability of Ti–B-SiCp reinforced Cu hybrid composites in dry turning
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Experimental investigations and optimization of MWCNTs-mixed WEDM process parameters of nitinol shape memory alloy
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Experimental investigation on welding of 2.25 Cr-1.0 Mo steel with regulated metal deposition and GMAW technique incorporating metal-cored wires
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Experimental investigation on the effect of dry and multi-jet cryogenic cooling on the machinability and hole accuracy of CFRP composites
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Investigation on microstructure, mechanical, and tribological performance of Cu base hybrid composite materials
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Investigations on surface induced tribological characteristics in MQCL assisted machining of duplex stainless steel
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On the effectiveness of Ni alloy-bronze composite lattice structures used in slide bearings operated under heavy loads
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