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Polaronic and Mott insulating phase of layered magnetic vanadium trihalide VCl3
PublicationTwo-dimensional (2D) van der Waals (vdW) magnetic 3d-transition metal trihalides are a new class of functional materials showing exotic physical properties useful for spintronic and memory storage applications. In this article, we report the synthesis and electromagnetic characterization of single-crystalline vanadium trichloride, VCl 3 , a novel 2D layered vdW Mott insulator, which has a rhombohedral structure (R3, No. 148) at...
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Electronic conductivity in the SiO2-PbO-Fe2O3 glass containing magnetic nanostructures
PublicationThe linear impedance spectra of iron–silicate–lead glass samples were measured in the frequency range from 1 MHz to 1 MHz and in the temperature range from 153 K to 423 K. The structure was investigated by means of XRD and atomic force microscopy. Local electrical and magnetic properties of the samples were tested with the aid of electrostatic force microscopy (EFM) and magnetic force microscopy (MFM). The obtained results show...
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Electrical properties and structure of lead-borate glass containing iron ions.
PublicationThe ac and dc conductivity in iron–lead-borate glass samples was investigated in the frequency range from 1 mHz to 1 MHz and in the temperature range from 153 K to 423 K. The structure was investigated by the means of atomic force microscopy (AFM) and the crystalline phases (if present) were identified by the means of X-ray diffractometry. Two types of ac electrical behaviour were observed. The first group of glass samples which...
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Photochemical and thermal reaction of intermediates in the phenylnitrene rearangment inside a hemicarcerand
PublicationBroadband irradiation (λ > 320 nm) of hemicarceplex H1 between −74 °C and −84 °C, produces encapsulated didehydroazepine (2), triplet phenylnitrene (3PN), 2-azabicyclo[3.2.0]hepta-1,3,6-triene (6), and 4-azaspiro[2.4]hepta-1,4,6-triene (7). The highly strained anti-Bredt imine 6 is formed from 2 via a photochemical four-electron electrocyclization. Under the irradiation conditions, 6 rearranges further to azaspirene 7. In addition,...
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Monitoring of lysozyme thermal denaturation by volumetric measurements and nanoDSF technique in the presence of N-butylurea
PublicationThe results of thermal studies of denaturation of hen egg white lysozyme (HEWL) in water and an aqueous solution of N-butylurea (BU) are presented. High-precision densimetric measurements were used to characterize and analyze the changes of the specific volume, v, during temperature elevation. The temperature of the midpoint of protein denaturation was also determined by nanoDSF technique (differential scanning fluorimetry). The...
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Implementation of Addition and Subtraction Operations in Multiple Precision Arithmetic
PublicationIn this paper, we present a digital circuit of arithmetic unit implementing addition and subtraction operations in multiple-precision arithmetic (MPA). This adder-subtractor unit is a part of MPA coprocessor supporting and offloading the central processing unit (CPU) in computations requiring precision higher than 32/64 bits. Although addition and subtraction operations of two n-digit numbers require O(n) operations, the efficient...
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Superconducting SrSnP with Strong Sn–P Antibonding Interaction: Is the Sn Atom Single or Mixed Valent?
PublicationThe large single crystals of SrSnP were prepared using Sn self-flux method. The superconductivity in the tetragonal SrSnP is observed with the critical temperature of ∼2.3 K. The results of a crystallographic analysis, superconducting characterization, and theoretical assessment of tetragonal SrSnP are presented. The SrSnP crystallizes in the CaGaN structure type with space group P4/nmm (S.G. 129, Pearson symbol tP6) according...
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Soft-mode enhanced type-I superconductivity in LiPd2Ge
PublicationThe synthesis, crystal structure, and physical properties (magnetization, resistivity, heat capacity) in combination with theoretical calculations of the electronic structure and phonon properties are reported for intermetallic compounds LiPd2X (X = Si, Ge, and Sn). LeBail refinement of powder x-ray diffraction data confirms that all compounds belong to the Heusler family (space group Fm-3m, No. 225). The lattice parameter increases...
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Possible quadrupole-order-driven commensurate-incommensurate phase transition in B20 CoGe
PublicationThe B20-type cobalt germanide CoGe was investigated by measuring the specific heat, resistivity, and 59Co nuclear magnetic resonance (NMR).We observed a phase transition at TQ = 13.7 K, evidenced by a very narrow peak of the specific heat and sharp changes of the nuclear spin-spin (T −1 2 ) and spin-lattice (T −1 1 ) relaxation rates. The fact that the entropy release is extremely small and the Knight shift is almost independent...
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Rediscovering Automatic Detection of Stuttering and Its Subclasses through Machine Learning—The Impact of Changing Deep Model Architecture and Amount of Data in the Training Set
PublicationThis work deals with automatically detecting stuttering and its subclasses. An effective classification of stuttering along with its subclasses could find wide application in determining the severity of stuttering by speech therapists, preliminary patient diagnosis, and enabling communication with the previously mentioned voice assistants. The first part of this work provides an overview of examples of classical and deep learning...
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The role of electrolysis and enzymatic hydrolysis treatment in the enhancement of the electrochemical properties of 3D-printed carbon black/poly(lactic acid) structures
PublicationAdditive manufacturing, also known as 3D printing, is beginning to play an unprecedented role in developing many applications for industrial or personalized products. The conductive composite structures require additional treatment to achieve an electroactive surface useful for electrochemical devices. In this paper, the surfaces of carbon black/poly(lactic acid) CB-PLA printouts were activated by electrolysis or enzymatic digestion...
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Mineral Composition of Dietary Supplements-Analytical and Chemometric Approach
PublicationThere is a lack of data on the actual composition and effectiveness of beetroot-based dietary supplements. The research aimed to determine the profile of 22 elements (Na, K, Ca, Mg, P, Fe, As, Se, Zn, Cu, Ag, Co, Ni, Mo, Al, Mn, Sr, Cr, Ba, Li, Pb, Cd) in beetroot and its supplements by the microwave plasma atomic emission spectrometry (MP-AES) method. The analytical procedure was optimised and validated. The composition of both...
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Pi of the Sky – all-sky, real-time search for fast optical transients
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Dariusz Kowalski dr inż.
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Detection of thermal radiation using lanthanum-strontium-iron oxide (LSFO) bolometers
PublicationW artykule przedstawiono bolometr wykonany z tlenków lantanowo-strontowo-żelazowych zastosowany do detekcji promienowania podczerwonego. Parametry bolometru były badane za pomocą wzorcowego źródła poromieniowania o temperaturze 38°C (311 K) oddalonego od bolometru o 500 mm. W trakcie pomiarów uzyskano stosunek sygnał/szum wynoszący ok. 62 (tj. 35.9 dB). Na podstawie wyników pomiarów oszacowano dokładność pomiaru temperatury za...
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Volumetric properties of zinc(II) chloride in N,N-dimethylacetamide and dimethylsulfoxide
PublicationW oparciu o pomiary gęstości szeregu równomolarnych mieszanin soli Zn(ClO4)2 -ZnCl2 wyznaczono pozorne objętości molowe kompleksów powstających podczas kompleksowania jonów cynku jonami chlorkowymi w dimetylosulfotlenku i N,N-dimetyloacetamidzie w 298.15 K. Uzyskane wyniki jednoznacznie wskazują na to, że w N,N-dimetyloacetamidzie wszystkie kompleksy chlorkowe jonów cynku(II) są czterokoordynacyjne. W dimetlosulfotlenku natomiast...
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Wspomaganie decyzji zakupu urządzeń do spawania metodą MIG/MAG z wykorzystaniem analizy skupień
PublicationW pracy podjęto często występujący w praktyce problem doboru właściwego dla danego zastosowania spawalniczego źródła prądu. Jako jedno z potencjalnych rozwiązań zaproponowano zastosowanie metod analizy skupień. Przedstawiono rezultaty klasyfikacji 96 urządzeń do spawania MIG/MAG metodami Warda i k-średnich dla 2 zestawów cech diagnostycznych. Na podstawie wyników uznano, że analiza skupień może być, przy spełnieniu pewnych warunków,...
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Badania możliwości wykorzystania cieczy jonowych w procesach oczyszczania biogazu
PublicationCelem pracy było lepsze zrozumienie mechanizmu przenikania metanu i tlenku węgla(IV) przez imidazoliowe, amoniowe oraz fosfoniowe ciecze jonowe osadzone na nośniku polimerowym, jak również opracowanie nowych procedur badawczych, przygotowania i użycia immobilizowanych membran ciekłych w procesach separacji gazów. Przeprowadzono badania przenikanie CO2 oraz CH4 przez ciecz jonowe unieruchomione w porach porowatego nośnika polimerowego...
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Optical properties of boron-doped nanocrystalline diamond films studied by spectroscopic ellipsometry
PublicationThe optical properties of boron-doped nanocrystalline diamond films, coated using Microwave Plasma Enhanced Chemical Vapour Deposition (μPE CVD) system, were analyzed by spectroscopic ellipsometry. Diamond films were deposited on silicon substrates. The ellipsometry data (refractive index (n(λ)), extinction coefficient (k(λ)) were modeled using dedicated software. Evolution of the optical structure with boron doping was observed...
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Decoherence-free communication over multiaccess quantum channels
PublicationIn this paper we consider decoherence-free communication over multiple access and k-user quantum channels. First, we concentrate on a hermitian unitary noise model U for a two-access bi-unitary channel and show that in this case a decoherence-free code exists if the space of Schmidt matrices of an eigensubspace of U exhibits certain properties of decomposability. Then, we show that our technique is also applicable for generic random unitary...
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Superconductivity in the Endohedral Ga Cluster Compound PdGa5
PublicationSuperconductivity is observed below Tc = 1.6 K in an endohedral Ga cluster compound PdGa5 using magnetization and heat capacity measurements. Electronic structure calculations show that the density of states (DOS) at the Fermi level is dominated by Ga s and p states and that the overall shape of DOS is similar to what was found in other endohedral Ga cluster superconductors, such as MoxGa5x+1, ReGa5, and T2Ga9 (T = Rh and Ir)....
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An Extended Control of the Input Angle for Matrix Converters Connected with the Non-Unity Power Factor Loads.
PublicationThis paper proposes a novel PWM modulation algorithm for Multiphase Conventional Matrix Converters (MCMC), with 3 inputs and k outputs, using the transfer function of the load angle. The proposed approach extends the range of power angle control at the input during the operation with a maximum voltage transfer ratio. The proposed concept is based on the Direct Analytic Voltage PWM (DAV--PWM) modulation with an elliptical trajectory...
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Radiation Therapy-Induced Changes in Serum Lipidome of Head and Neck Cancer Patients
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Conformational studies of [Nphe5]SFTI-1 by means of 2D NMR spectroscopy in conjunction with molecular dynamics calculations
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Estimates for minimal number of periodic points for smooth self-maps of simply-connected manifolds
Open Research DataWe consider a closed smooth connected and simply-connected manifold of dimension at least 4 and its self-map f. The topological invariant Dr[f] is equal to the minimal number of r-periodic points in the smooth homotopy class of f. We assume that r is odd and all coefficients b(k) of so-called periodic expansion of Lefschetz numbers of iterations are...
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Proceduralne modelowanie stworów w Suboceanic
PublicationSuboceanic to niewielki program wykonywalny zajmujący 50 kilobajtów. Został zaprezentowany na party demoscenowym Assembly 2005 w kategorii intro 64k. Efektem działania programu jest multimedialna animacja, w której zarówno obraz jak i dźwięk generowany jest w czasie rzeczywistym. Ta praca opisuje szczegółowo algorytmy opracowane podczas produkcji tego intra do generowania proceduralnych stworów i roślin. Opisana metoda polega na...
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Projekt zespołowy - P, Mechatronika, I st., sem. VI, lato 2021-22 (M:31437W0)
e-Learning CoursesDrodzy Studenci i Drogie Studentki, wraz z dotychczasowymi moimi Studentami i Studentkami opracowaliśmy metodę zdalnego nauczania, która zapewnia możliwie najwyższą jakość tej formy kształcenia. Do prowadzenia zajęć on-line wybraliśmy platformę ZOOM. W tym miejscu czuję się w obowiązku poinformować Państwa, że IOD CUI był bardzo przeciwny użyciu platformy ZOOM do zdalnego kształcenia. Ostatecznie zgodził się, ale pod warunkiem...
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Podstawy konstrukcji maszyn I - W, C, L, IMM, I st., sem. V, lato 2021-22 (M:31639W0)
e-Learning CoursesDrodzy Studenci i Drogie Studentki, wraz z dotychczasowymi moimi Studentami i Studentkami opracowaliśmy metodę zdalnego nauczania, która zapewnia możliwie najwyższą jakość tej formy kształcenia. Do prowadzenia zajęć on-line wybraliśmy platformę ZOOM. W tym miejscu czuję się w obowiązku poinformować Państwa, że IOD CUI był bardzo przeciwny użyciu platformy ZOOM do zdalnego kształcenia. Ostatecznie zgodził się, ale pod warunkiem...
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Podstawy konstrukcji maszyn III - P, IMM, I st., sem. VI, lato 2021-22 (PG_00050262)
e-Learning CoursesDrodzy Studenci i Drogie Studentki, wraz z dotychczasowymi moimi Studentami i Studentkami opracowaliśmy metodę zdalnego nauczania, która zapewnia możliwie najwyższą jakość tej formy kształcenia. Do prowadzenia zajęć on-line wybraliśmy platformę ZOOM. W tym miejscu czuję się w obowiązku poinformować Państwa, że IOD CUI był bardzo przeciwny użyciu platformy ZOOM do zdalnego kształcenia. Ostatecznie zgodził się, ale pod warunkiem...
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Opracowanie kompozytowych przęseł mostów dla pieszych do zastosowania nad drogami GP
ProjectsProject realized in Faculty of Civil and Environmental Engineering according to PBS1/B2/6/2013 agreement from 2013-02-11
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Samotestowanie toru analogowego ze wzmacniaczem w pełni różnicowym w elektronicznych systemach wbudowanych sterowanych mikrokontrole-rami
PublicationPrzedstawiono nową metodę samotestowania toru analogowego opartego na wzmacniaczu w pełni różnicowym w elektronicznych systemach wbu-dowanych sterowanych mikrokontrolerami. Bazuje ona na nowej metodzie diagnostycznej opartej na przekształceniu transformującym próbki odpo-wiedzi czasowej badanej części analogowej na pobudzenie "ujemnym" impulsem prostokątnym na wejściu Vocm na krzywe identyfikacyjne w przestrzeni pomiarowej. Metoda...
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Evaluation of the current output of polymer anodes used in cathodic protection
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Selection of measurement frequency in Mott–Schottky analysis of passive layer on nickel
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Instantaneous impedance spectra of a non-stationary model electrical system
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Electrochemical investigations of conductive coatings applied as anodes in cathodic protection of reinforced concrete
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A correct description of the interaction between a magnetic moment and its image
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Evaluation of cavitation erosion–corrosion degradation of mild steel by means of dynamic impedance spectroscopy in galvanostatic mode
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The time dependence of pit creation impedance spectra
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Evaluation of pitting corrosion by means of dynamic electrochemical impedance spectroscopy
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Fatigue Behaviour of Sintered Duplex Stainless Steel
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Silo music — Mechanism of dynamic flow and structure interaction
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Depression is predictor of SVR to treatment with interferon alfa and ribavirin for HCV
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Pilot plant studies on the removal of trihalomethanes by composite reverse osmosis membranes
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Production of process water using integrated membrane processes
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Purinergic implication in amyotrophic lateral sclerosis—from pathological mechanisms to therapeutic perspectives
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Effect of substrate type on the field performance and chemical composition of highbush blueberry cv.Patriot
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Mechanical and Corrosion Properties of Magnesium-Bioceramic Nanocomposites
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Numerical Simulation of Duplex Steel Multipass Welding
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Degradation of Gel-Coat Layer in Glass/Polyester Laminate in Seawater Environment
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The influence of process parameters on photocatalytic hydrogen production
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