Filtry
wszystkich: 2146
wybranych: 1792
-
Katalog
- Publikacje 1792 wyników po odfiltrowaniu
- Czasopisma 74 wyników po odfiltrowaniu
- Konferencje 1 wyników po odfiltrowaniu
- Osoby 59 wyników po odfiltrowaniu
- Projekty 4 wyników po odfiltrowaniu
- Kursy Online 46 wyników po odfiltrowaniu
- Wydarzenia 1 wyników po odfiltrowaniu
- Dane Badawcze 169 wyników po odfiltrowaniu
Filtry wybranego katalogu
wyświetlamy 1000 najlepszych wyników Pomoc
Wyniki wyszukiwania dla: GREEN ANALYTICAL SORBENTS
-
EvOLAP Graph – Evolution and OLAP-Aware Graph Data Model
PublikacjaThe objective of this paper is to propose a graph model that would be suitable for providing OLAP features on graph databases. The included features allow for a multidimensional and multilevel view on data and support analytical queries on operational and historical graph data. In contrast to many existing approaches tailored for static graphs, the paper addresses the issue for the changing graph schema. The model, named Evolution...
-
Non-proportional full-order Luenberger observers of induction motors
PublikacjaThe paper recapitulates recently conducted investigations of non-proportional Luenberger observers, applied to reconstruction of state variables of induction motors. Three structures of non-proportional observers are analyzed, a proportional-integral observer, modified integral observer and observer with integrators. Criteria for gain selection of the observer are described, classical ones based on poles, as well as additional,...
-
Molecular detection of Candida krusei
PublikacjaThe species identification of fungi belonging to genus Candida is an important issue as this genus becomes the emerging problem of nosocomial infections. As Candida krusei presents intrinsicresistance to the fluconazole that is the drug of the first choice in case of invasive candidiasis the PCR identifying the DNA of C. krusei was elaborated. The analytical sensitivity of the assay on spiked blood samples was estimated at 3-5...
-
The Use of Electronic Nose for Sunflower and Rapeseed Oil Classification
PublikacjaThe electronic nose is an analytical device often used in food industries to examine the authenticity of their products. The use of the electronic nose allows for a rapid assessment of the quality of food. The oil samples from sunflower and rapeseed were used in this study. Both oil samples were kept inside the thermostat incubator at different ranging from 20oC to 180oC with increment of 40oC. Principal Component Analysis (PCA)...
-
The Use of Electronic Nose for Sunflower and Rapeseed Oil Classification
PublikacjaThe electronic nose is an analytical device often used in food industries to examine the authenticity of their products. The use of the electronic nose allows for a rapid assessment of the quality of food. The oil samples from sunflower and rapeseed were used in this study. Both oil samples were kept inside the thermostat incubator at different ranging from 20oC to 180oC with increment of 40oC. Principal Component Analysis (PCA)...
-
Influence of stirrups in a concrete shell on strengthening reinforced concrete column
PublikacjaTwelve concrete columns, with a 150x150mm square section and three columns with a circular section (d=200mm), are tested to investigate the effect of strengthening by RC jacket. Based on a confined concrete model for axial static loading, an analytical methods, reported in the literature are proposed to predict the behavior of columns with RC jacket. The results support the conception that the effect of strengthening depends...
-
Scattering and Propagation Analysis for the Multilayered Structures Based on Field Matching Technique
PublikacjaA semi-analytical method is employed to the analysis of scattering and guiding problems in multilayer dielectric structures. The approach allows to investigate objects with arbitrary convex cross section and is based on the direct field matching technique involving the usage of the field projection at the boundary on a fixed set of orthogonal basis functions. For the scattering problems the scattered field in the far zone is calculated...
-
SYNTHETIZED MEMBRANES FOR ULTRASOUND-ASSISTED SOLVENT EXTRACTION OF POROUS MEMBRANE PACKED SOLID SAMPLES.
PublikacjaMembranes are becoming more and more popular in analytical chemistry, which is why they are used, among others, in extraction processes. Therefore, this work focuses on the process of synthesis PVDF membranes and its optimization. The obtained membranes were used as bags for the phthalate extraction in disposable diapers for babies. Extraction was accomplished by method ultrasound-assisted solvent extraction of porous PVDF membrane...
-
Application of chromogenic dye in biogenic amines determination using spectrophotometry
PublikacjaBiogenic amines content can be the source of information in the field of freshness and suitability of certain foods for consumption. However, most analytical methods for their determination require complicated sample preparation and expert knowledge. Because of that, a novel approach based on chromogenic dye application was proposed. After the SN1 reaction of an amine with S 0378 dye, the absorbance of the solution was measured...
-
Passive sampling and/or extraction techniques in environmental analysis: a review
PublikacjaThe current state-of-the-art of passive sampling and/or extraction methods for long-term monitoring of pollutants in different environmental compartments is discussed in this review. Passive dosimeters that have been successfully used to monitor organic and inorganic contaminants in air, water, sediments, and soil are presented. The application of new approaches to the determination of pollutants at the sampling stage is discussed....
-
An evaluation of sucrose as a possible contaminant in e-liquids for electronic cigarettes by hydrophilic interaction liquid chromatography–tandem mass spectrometry
Publikacja -
New approach based on solid-phase extraction for the assessment of organic compound pollutions in so-called pharmaceutically pure water
PublikacjaOpisano mozliwość zastosowania nowej procedury analitycznej opartej na wykorzystaniu techniki ekstrakcji do fazy stałej (na etapie izolacji i wzbogacania analitów) do oznaczania śladowych ilości zanieczyszczeń organicznych w wodzie specjalnej czystości używanej do celów farmaceutycznych.Próbka badanej wody jest przepuszczana przez złoże sorbenta, które jest osuszane za pomocą strumienia oczyszczonego powietrza, przed etapem termicznej...
-
Determination (monitoring) of PAHs in surface waters: why operationally defined procedure is needed
PublikacjaW pracy przedstawiono i skomentowano rezultaty badań międzylaboratoryjnych oznaczania wielopierścieniowych węglowodorów aromatycznych w wodzie czystej i wodzie zawierającej zawiesinę. Badania wskazują, ze wyniki oznaczania zależa od zastosowanej techniki izolacji analitów z próbki i końcowej procedury ich rozdzielania i oznaczania. Przeprowadzone badania wskazują, że nowoczesna analityka nie dysponuje technikami izolacji, które...
-
Passive sampling as a tool for obtaining reliable analyticalinformation in environmental quality monitoring
PublikacjaSpośród technik pobierania próbek analitów technika dozymetrii pasywnej wydaje się być interesującą alternatywą w stosunku do powszechnie stosowanych technik dynamicznych. Dozymetria pasywna łączy w sobie etap pobierania próbki z etapem izolacji i wzbogacania analitów, które są zatrzymywane w odpowiednim medium zatrzymującym. Prowadzi to do znacznego uproszczenia operacji analitycznych wykonywanych in situ. W odróżnieniu od aktywnych...
-
A comparison of three solvent-free techniques coupled with gas chromatography for determining trihalomethanes in urine samples
PublikacjaDążenie do oznaczania lotnych analitów organicznych w próbkach płynów biologicznych charakteryzujących się złożonym, a często zmiennym składem matrycy, stanowi siłę napędową do działań analityków w zakresie poszukiwania nowych rozwiązań metodycznych i aparaturowych. Publikacja ta przedstawia porównanie trzech technik zastosowanych do tych celów: technikę analizy fazy nadpowierzchniowej z generacją strumienia ciekłego sorbentu...
-
Determination of tributylotin (TBT) in marine sediment using pressurised liquid extraction-gas chromatography-isotope dilution mass spectrometry (PLE-GC-IDMS) with a hexane-tropolone mixture
PublikacjaOpracowano metodę oznaczania zawartości tributylocyny w próbkach osadu morskiego. Na etapie izolacji zastosowano technikę przyspieszonej ekstrakcji za pomocą roztworu tropolonu w heksanie.Na etapie oznaczeń końcowych wykorzystano technikę chromatografii gazowej, stosując metodę spektrometrii mas rozcieńczenia izotopowego. Wyznaczono parametry walidacyjne opracowanej metody: granicę wykrywalności, precyzję, poprawność i niepewność.
-
Metal-coated fused silica fibres as a support for immobilized compounds yielding a volatile analyte (C2H4)
PublikacjaPrzedstawiono wyniki badań dotyczących wykorzystania chemicznie modyfikowanych włókien szklanych pokrytych warstwą metalu (aluminium), jako nośników związków powierzchniowych. W trakcie procesu termicznego rozkładu z tak zmodyfikowanych włókien uwalnia się eten, który stanowi składnik mierzony uzyskiwanej gazowej mieszaniny wzorcowej. Ilość uwalnianego etenu zależy jedynie od długości danego rodzaju i typu modyfikowanego włókna...
-
Electroanalytical and spectroscopic procedures for examination of interactions between double stranded DNA and intercalating drugs
PublikacjaPrzedstawiono metodę elektrochemicznego opisu oddziaływań dsDNA ze związkiem biologicznie czynnym w warunkach, w których zarówno badany związek jak i cząsteczka DNA są w roztworze elektrolitu. Opracowano warunki pomiaru, gdzie ani związek, ani DNA nie adsorbuje na elektrodzie. Wykazano, podobnie jak podczas badania innymi metodami, że oddziaływania są dwojakiego rodzaju: elektrostatyczne i poporzez interkalację.
-
Reporter Fluorescent Molecules in Biological Systems: The Current Overview
Publikacja -
Fabrication of a Molecularly Imprinted Polymer Adsorbent for Pipette Tip Micro Solid-phase Extraction of Levofloxacin from Aqueous Samples Prior to its Spectrophotometric Determination
Publikacja -
A new approach for the extraction of tetracyclines from soil matrices: application of the microwave-extraction technique
Publikacja -
Ionic liquids for the passive sampling of sulfonamides from water—applicability and selectivity study
Publikacja -
Preliminary study on suitability of ionic liquids as potential passive-sampling media of polyaromatic-hydrocarbon (PAH) analyses in water
Publikacja -
Current Issues in Pharmaceutical Residues in Drinking Water
Publikacja -
Metal-coated fused silica fibers as a support for immobilized compounds yielding a volatile analyte (C2H4)
Publikacja -
Determination of tributyltin in marine sediment: Comit� Consultatif pour la Quantit� de Mati�re (CCQM) pilot study P-18 international intercomparison
Publikacja -
Determination of tributyltin (TBT) in marine sediment using pressurised liquid extraction–gas chromatography–isotope dilution mass spectrometry (PLE–GC–IDMS) with a hexane–tropolone mixture
Publikacja -
Theoretical opportunities and actual limitations of pH gradient HPLC
Publikacja -
Transformations of Tetrahydrocannabinol, tetrahydrocannabinolic acid and cannabinol during their extraction from Cannabis sativa L.
Publikacja -
Hydrolytical instability of hydroxyanthraquinone glycosides in pressurized liquid extraction
Publikacja -
Nanosized zinc, epigenetic changes and its relationship with DMBA induced breast cancer in rats
Publikacja -
The state-of-the-art determination of urinary nucleosides using chromatographic techniques “hyphenated” with advanced bioinformatic methods
Publikacja -
New approaches to chromatographic determination of lipophilicity of xenobiotics
Publikacja -
Micro-cloud point extraction for preconcentration of Aspirin in commercial tablets prior to spectrophotometric determination
Publikacja -
Magnetic molecularly imprinted polymer nanoparticles for selective extraction of copper from aqueous solutions prior to its flame atomic absorption determination
Publikacja -
A simple graphene-based pipette tip solid-phase extraction of malondialdehyde from human plasma and its determination by spectrofluorometry
Publikacja -
The Mesoporous Porphyrinic Zirconium Metal-Organic Framework for Pipette-Tip Solid-Phase Extraction of Mercury from Fish Samples Followed by Cold Vapor Atomic Absorption Spectrometric Determination
Publikacja -
Carbon Paste Electrode Modified with ZrO2 Nanoparticles and Ionic Liquid for Sensing of Dopamine in the Presence of Uric Acid
Publikacja -
Different Aspects of the Elemental Analysis of Honey by Flame Atomic Absorption and Emission Spectrometry: A Review
Publikacja -
Hanging drop cathode-atmospheric pressure glow discharge as a new method of sample introduction for inductively coupled plasma-optical emission spectrometry
Publikacja -
HPLC–DAD Analysis, Antimicrobial and Antioxidant Properties of Aromatic Herb Melissa officinalis L., Aerial Parts Extracts
Publikacja -
Rapid Evaluation of Poultry Meat Shelf Life Using PTR-MS
PublikacjaThe use of proton transfer reaction mass spectrometry (PTR-MS) for freshness classification of chicken and turkey meat samples was investigated. A number of volatile organic compounds (VOCs) were selected based on the correlation (> 95%) of their concentration during storage at 4 °C over a period of 5 days with the results of the microbial analysis. In order to verify if the selected compounds are not sample-specific, a number...
-
Complementary Use of Multi-dimensional Gas Chromatography and Proton Transfer Reaction Mass Spectrometry for Identification of Rapeseed Oil Quality Indicators
PublikacjaThe change of concentration of various volatiles generated during frying may be an indicator of oil quality. Chemical compounds such as aldehydes, ketones, alcohols and carboxyl acids are the products of oxidation during thermal degradation of edible oils. Shown in this work is a complementary use of GC×GC-TOFMS and PTR-MS for the detection and determination of quality indicators of rapeseed oil. The former technique was used for...
-
Fatal N-Ethylhexedrone Intoxication
PublikacjaN-Ethylhexedrone [2-(ethyloamino)-1-phenylhexan-1-one; α-ethylaminohexanophenone; NEH] is one of the most recent synthetic cathinones that appeared on the illegal market in late 2015. The majority of information concerning the model of consumption of NEH and its impact on the body originates only from self-reports from grey literature websites and drug forums. There are only limited data associated with the concentrations of NEH...
-
A nontargeted approach to determine the authenticity of Ginkgo biloba L. plant materials and dried leaf extracts by liquid chromatography-high-resolution mass spectrometry (LC-HRMS) and chemometrics
PublikacjaThe lack of stringent regulations regarding raw materials for herbal supplements used for medicinal purposes has been a constant challenge in the industry. Ginkgo biloba L. leaf extracts attract consumers because of the supposed positive effect on mental performance and memory. Supplements are produced using dried leaf materials and standardized leaf extracts such as EGb 761. Adulteration of Ginkgo biloba L. plants and extracts...
-
The Toolbox of Methods for Multidirectional Characterization of Dietary Nucleic Acids; Verification for Raw and Processed Food Products
PublikacjaCurrently, the nutritional value of food is associated mainly with components such as proteins, carbohydrates, and lipids. However, another important macromolecules present in many foods are dietary nucleic acids (dietNA), i.e., DNA as well as both coding and non-coding RNAs. In the context of food chemistry and nutrition, dietNA are nowadays vastly neglected. In consequence, there are no dedicated methodologies to characterize...
-
Application of normal-phase high-performance liquid chromatography followed by gas chromatography for analytics of diesel fuel additives
Publikacja -
Measurement of benzene concentration in urban air using passive sampling
PublikacjaAbstract The concentration of benzene in urban air in theTri-City area of Poland (Gdańsk-Sopot-Gdynia, andTczew) was assessed using diffusive passive samplers (Rad-iello). Samples were collected during a four-year monitoringcampaign (2007-2010) at selected monitoring stations man-aged by the Agency of Regional Air Quality Monitoring inthe Gdańsk Metropolitan Area (ARMAAG) Foundation.The performance of the passive samplers was investigatedin...
-
A new procedure for the determination of distillation temperature distribution of high-boiling petroleum products and fractions
PublikacjaThe distribution of distillation temperatures of liquid and semi-fluid products, including petroleum fractions and products, is an important process and practical parameter. It provides information on properties of crude oil and content of particular fractions, classified on the basis of their boiling points, as well as the optimum conditions of atmospheric or vacuum distillation. At present, the distribution of distillation temperatures...
-
Oil refinery dusts: morphological and size analysis by TEM
PublikacjaThe objectives of this work were to develop a means of sampling atmospheric dusts on the premises of an oil refinery for electron microscopic study to carry out preliminary morphological analyses and to compare these dusts with those collected at sites beyond the refinery limits. Carbon and collodion membranes were used as asupport for collection of dust particles straight on transmission electron microscopy (TEM) grids. Micrographs...