Filtry
wszystkich: 641
-
Katalog
Wyniki wyszukiwania dla: SYNTHETIC APERTURE RADAR
-
A heterotrimetallic synthetic approach in versatile functionalization of nanosized {MxCu13–xW7}3+ and {M1Cu8W6} (M = Co, Ni, Mn, Fe) metal–cyanide magnetic clusters
Publikacja -
4-(Cyclic-amidino)phenols. Preparation and Use in a Diamidine Synthesis
PublikacjaThe Pinner synthesis was applied to the prepn. of phenols 4-substituted with cyclic amidines in high yields from readily available 4-HOC6H4C(OMe):NH.HCl and aliph. diamines. An alternative attempt was made to convert 4-HOC6H4CSNH2 to 4-(1,4,5,6-tetrahydro-5-hydroxy-2-pyrimidinyl)phenol. A procedure for the prepn. of 3,6-bis(4-hydroxyphenyl)-1,2,4,5-tetrazine is reported. The syntheses of 2,4-bis[4-(4,5-dihydro-1H-imidazol-2-yl)phenoxy]pyrimidine...
-
Ewa Hermanowicz prof. dr hab. inż.
Osoby -
The influence of synthesis method on the microstructure and catalytic performance of Y 0.07 Sr 0.93 Ti 0.8 Fe 0.2 O 3-δ in synthetic biogas operated solid oxide fuel cells
PublikacjaThe Y0.07Sr0.93Ti0.8Fe0.2O3-δ (YSTF) material was fabricated using three different synthesis methods: modified polymer precursor method (MPP), Pechini method and a solid state reaction method. It was applied as an anode catalytic material for biogas reforming in solid oxide fuel cells. Clear differences in the microstructure of fabricated catalytic layers were found, mainly with respect to a grain size and distribution of grains....
-
A Conformal Circularly Polarized Series-Fed Microstrip Antenna Array Design
PublikacjaA conformal circularly polarized series-fed microstrip array design for broadside radiation is presented. The array aperture under design is conformal to a cylindrical surface of a given radius. The approach we present primarily addresses focusing of the circularly polarized major lobe of the conformal array by proper dimensioning of the aperture spacings. The proposed analytical models yield the values of the element spacings...
-
Dariusz Witt prof. dr hab. inż.
Osoby -
Chiral [Mn II Mn III 3 M′] (M′=Na I , Ca II , Mn II ) and [Mn II Mn III 6 Na I 2 ] Clusters Built from an Enantiomerically Pure Schiff Base: Synthetic, Chiroptical, and Magnetic Properties
Publikacja -
Zdzisław Kowalczuk prof. dr hab. inż.
OsobyW 1978 ukończył studia w zakresie automatyki i informatyki na Wydziale Elektroniki Politechniki Gdańskiej, następnie rozpoczął pracę na macierzystej uczelni. W 1986 obronił pracę doktorską, w 1993 habilitował się na Politechnice Śląskiej na podstawie pracy Dyskretne modele w projektowaniu układów sterowania. W 1996 mianowany profesorem nadzwyczajnym, w 2003 otrzymał tytuł profesora nauk technicznych. W 2006 założył i od tego czasu...
-
A new synthetic entry to phosphinophosphinidene complexes. Synthesis and structural characterisation of the first side-on bonded and the first terminally bonded phosphinophosphinidene zirconium complexes[mu-(1,2:2-eta-tBu2PLP){Zr(Cl)Cp2}2] and [{Zr(PPhMe2)Cp2}(eta^1^-P-P-tBu2)].
PublikacjaPodano nową metodę syntezy kompleksów fosfinofosfinidenowych polegającą na reakcji dichlorku cyrkonocenu z solą litową difosfanu t-Bu2P-P(SiMe3)Li. Otrzymano pierwsze kompleksy fosfanofosfinidenowe cyrkonu z ligandem związanym w sposób boczny i ligandem związanym terminalnie.
-
Multidisciplinary approach to the assessment of historic structures based on the case of a masonry bridge in Galicia (Spain)
PublikacjaThe paper presents a general method to evaluate a masonry structure with a complex geometry and unknown material properties. This multidisciplinary approach integrates close range digital photogrammetry,ground probing radar (GPR) and finite elements analysis (FEM) to analyse a masonry bridge. The resulting information from photogrammetry and radar is applied to define a 3D model, which is then used to simulate the behaviour of...
-
Do Leonardo da Vinci’s drawings, room acoustics and radio astronomy have anything in common?
PublikacjaAfter introducing Leonardo da Vinci’s (LdV) predecessors in the field of light propagation research, his drawings on the topic of reflecting light by a spherical mirror are analysed. The discovery of LdV is presented, according to which, at an infinitely distant source of rays, a small fragment of the canopy is enough to generate a focus, while the rest of the mirror forms a caustic for which LdV did not indicate an application....
-
Błażej Prusak dr hab.
OsobyBłażej Prusak jest kierownikiem Katedry Finansów na Wydziale Zarządzania i Ekonomii Politechniki Gdańskiej oraz redaktorem naczelnym czasopisma Research on Enterprise in Modern Economy - theory and practice (REME)/Przedsiębiorstwo we współczesnej gospodarce - teoria i praktyka, a także członkiem komitetów redakcyjnych takich czasopism jak: Intellectual Economics; Przestrzeń. Ekonomia. Społeczeństwo; Akademia Zarządzania. Jest autorem...
-
An Optimized Ka-Band Low Profile Dual-Polarized Transmitarray Antenna With 2D Beam Switching
PublikacjaThis article presents an optimized dual-polarized transmitarray antenna (TA) designed for MIMO applications at the Ka-band, capable of switching beams in two directions. The antenna aperture uses a small unit cell with three layers of Taconic RF-35 dielectric substrates, which can be easily fabricated using PCB technology. The unit cell achieved a 360-degree phase shift and a transmission magnitude exceeding –0.4 dB at 28 GHz....
-
Thermal stability of vanadium xerogel powder under different atmpshere
Dane BadawczeThe DataSet contains the results of the thermal behavior of the vanadium xerogel powder. The information about xerogel powder synthesis is described in the Journal of Nanomaterials.
-
Changes in heat of vanadium xerogel powder under different atmosphere
Dane BadawczeThe DataSet contains the DSC curves of the vanadium xerogel powder. The information about xerogel powder synthesis is described in the Journal of Nanomaterials.
-
Rafał Lech dr hab. inż.
OsobyIEEE Senior Member #92122578 Rafał Lech urodził się w Elblągu w 1977 roku. W roku 2001 otrzymał tytuł magistra inżyniera, w roku 2007 stopień doktora nauk technicznych (z wyróżnieniem) a w roku 2018 stopień doktora habilitowanego nauk technicznych w dyscyplinie elektronika w Politechnice Gdańskiej. Obecnie pracuje w Katedrze Inżynierii Mikrofalowej i Antenowej na Wydziale Elektroniki, Telekomunikacji i Informatyki w Politechnike...
-
Wpływ drążenia pionowego w silikatowych elementach murowych na nośność kotew wklejanych
PublikacjaThe article is showing results of measurements of the effectiveness of the assembly anchor of inmates glued in in sunk vertically lime-sandy blocks. Examinations were performed for cases of the assembly anchor in different fragments of blocks: in part fullwall, in an axis of symmetry and on the edge of the aperture vertical. An influence of the location of places of settling was examined anchor to the way of the forming of uniting...
-
Shape Memory Alloy-Based Fluidically Reconfigurable Metasurfaced Beam Steering Antenna
PublikacjaA low-cost actuator-based fluidically programmable metasurface (FPMS) antenna is proposed to solve the slow tuning speed problem of the manually fluidic based reconfigurable antennas. The FPMS-based antenna is probe-fed and comprises a 4 × 4 square ring metasurface as a superstrate. Moreover, two shape memory alloy (SMA)-based electrically-controlled actuators are employed in the design for controlling the position of the 3D-printed...
-
Piotr Figura dr inż.
OsobyPiotr Figura jest pracownikiem Katedry Finansów na Wydziale Zarządzania i Ekonomii Politechniki Gdańskiej, a także członkiem Komisji Wydziałowej ds. Weryfikacji Efektów Uczenia się oraz recenzentem akademickim zadań z zakresu rachunkowości Centralnej Komisji Edukacyjnej. Jest autorem lub współautorem kilku monografii naukowych w tym: Wartości wzorcowe wskaźników finansowych przedsiębiorstw giełdowych; Classical and modern concepts...
-
Improvement of time difference of arrival measurements resolution by using fractional delay filters in a direct sequence-code division multiple access radionavigation system
PublikacjaThis study presents a method of improving time measurements resolution in a direct sequence-code division multiple access receiver by using a fine code tracking loop based on fractional delay filtering of a despreading sequence. It briefly describes the structure of a generic digital code tracking loop and the proposed modification which allows to measure time difference of arrival values with the subsample resolution, together...
-
A Novel Approach of Using Selected Unconventional Geodesic Methods of Estimation on VTS Areas
PublikacjaThe Vessel Traffic Service (VTS) systems belong to the fundamental tools used in ensuring a high level of safety across sea basins with heavy traffic, where the presence of navigational hazards poses a great risk of collision or a ship running aground. In order to determine the mutual location of ships, VTS systems obtain information from different facilities, such as coastal radar stations, AIS, and vision systems. Fixing a ship’s...
-
Compact Electromagnetic Lens Antennas Using Cascaded Metasurfaces for Gain Enhancement and Beam Steering Applications
PublikacjaElectromagnetic (EM) lens antenna designs using cascaded metasurfaces for gain enhancement and beam steering applications are proposed. Two different lens aperture designs are proposed and populated with aperiodic unit cells of size 0.2λo × 0.2λo. In lens Design 1, the unit cells of different phases are distributed in concentric circular zones, whereas in lens Design 2, the unit cells of different phases are distributed in vertical...
-
Automatic sound source localization in disturbing conditions using acoustic vector sensors
PublikacjaA concept, practical realization and applications of a passive acoustic radar to automatic localization and tracking of sound sources in disturbing conditions were presented in the paper. The device consists of the new kind of multichannel miniature sound intensity sensors and a group of digital signal processing algorithms. The sensitivity of the realized acoustic radar was examined in free sound field. Several kinds of sound...
-
Preparation and characterization of Langmuir-Blodgett films of 16-membered azobenzocrown ether with naphthalene residue
PublikacjaOtrzymano i charakteryzowano filmy Langmuira-Blodgett 16-członowej azobenzokorony z resztą naftalenową. Monowarstwy Langmuira były z sukcesem przenoszone na stałe substraty z utworzeniem filmów LB. Filmy osadzone na elektrodach z ITO zostały również użyte jako elektrody w woltametrii cyklicznej i uzyskano rezultaty wskazujące na to, że filmy te wykazują wyraźną odpowiedź na jony metali.
-
Ex situ XANES, XPS and Raman studies of poly(3,4-ethylenedioxythiophene)modified by iron hexacyanoferrate
PublikacjaPraca dotyczy badań XANES, XPS i Ramana polimeru przewodzącego poli(3,4-etylenodioksytiofenu) modyfikowanego heksacyjanożelazianem żelaza. Badania XANES potwierdziły oktaedryczne otoczenie atomu żelaza, którego najbliższymi sąsiadami są atomy węgla oraz atomy azotu. Badania XPS wykazały istnienie wiązań Fe-C, Fe-N oraz chemicznego oddziaływania między atomem siarki polimeru a atomem żelaza błękitu pruskiego. Obecność oddziaływań...
-
Ex situ XANES, XPS and Raman studies of poly(3,4-ethylenedioxythiophene) modified by iron hexacyanoferrate
PublikacjaPraca dotyczy materiału hybrydowego złożonego z polimeru elektroaktywnego poli(3,4-etylenodioksytiofenu) i Błękitu Pruskiego. Wykonano pomiary spektroskopowe z użyciem technik: spektrometrii fotoelektronów wzbudzonych promieniami X (X-ray Photoelectron Spectroscopy (XPS)), spektroskopii absorpcyjnej struktury przykrawędziowej (X-ray Absorption Near Edge Structure (XANES)) oraz spektroskopii mikro-Ramana. Przeprowadzone badania...
-
Tetrapyrazinoporphyrazine with eight peripheral adamantanylsulfanyl units – Synthesis and physicochemical study
Publikacja -
Coherent electron transport in hydrocarbon molecular devices
Publikacja -
Synthesis of Novel Polycationic Quaternary Di- and Trispirocyclic Benzenes
PublikacjaTreatment of hexakis(bromomethyl)benzene with a cyclic amine {morpholine, 1-methylpiperazine, 1-(2-hydroxyethyl)piperazine, isonipecotamide, 4-hydroxypiperidine, 4-[3-(4-piperidyl)propyl]-1-piperidineethanol} gave a range of di- and trispirocyclic ammonium salts in satisfactory yields (22-62%). Presumably, the electrostatic and repulsion forces play an important role in their formation. The structure in soln. and the protonation...
-
Preparation of 1-[Ω-(1,4,5,6-Tetrahydropyrimidin-2-yl)alkyl]thymines
PublikacjaOne-stage prepn. of the hydrochloride salts of 1-[ω-(1,4,5,6-tetrahydropyrimidin-2-yl)alkyl]-thymines, e.g. I, from 1-(ω-cyanoalkyl)thymines and a 1:1-mixt. of 1,3-diaminopropane and ethanol satd. with hydrogen sulfide is described. 1-(2-Cyanoethyl)-thymine gave a facile reversal of the Michael reaction to thymine under the conditions used. The reaction of 1,3-bis(3-cyanobenzyl)thymine with the above reagent produced 1,3-bis[3-(1,4,5,6-tetrahydropyrimidin-2-yl)benzyl]thymine.
-
Heteropolyanions doped polyacetylene—Preparation, spectroscopic and catalytic properties
Publikacja -
A study of optical properties and annealing effect on the absorption edge of pristine- and iodine-doped polyazomethine thin films
Publikacja -
Effect of chemical structure and deposition method on optical properties of polyazomethines with alkyloxy side groups
Publikacja -
TMSCL as a rate accelerating additive in acylations of amines with 5-(α- amino-α'-hydroxy)methylene meldrum's acids
PublikacjaAspects are presented of the acylation of amines, alcohols and thiols with 5-(α-amino- α'-hydroxy)methylene Meldrum's acids. We placed special emphasis on the acylation reaction of secondary amines with 5-(α-amino- α'-hydroxy)methylene Meldrum's acids, which, due to their basicity, caused problems concerning salt formation with a Meldrum acid derivative. We found that secondary amines, which react at the slowest rate and with a...
-
One-step formation of n-alkenyl-malonamides and n-alkenyl-thiomalonamides from carbamoyl meldrum's acids.
PublikacjaA one-pot synthesis for the preparation of N-alkenyl-malonamides and N-alkenyl-thiomalonamides was developed. 5-[Hydroxy/mercapto(aryl/alkylamino)methylene]-2,2-dimethyl-1,3-dioxane-4,6-dione act as a source of ketenes that react with the tautomeric form of alkyl-(2-phenyl-propylidene)-amines. A possible [2+2] or [4+2] cycloaddition product of ketene to imines was not observed.
-
Formation of novel nanostructures using carbon nanotubes as a frame
Publikacja -
Modification of SiC based nanorods via a hydrogenated annealing process
Publikacja -
The influence of the position of a chiral substituent on undecathiophene chain. A DFT study
Publikacja -
Effect of electrode resistance on admittance spectra of planar organic device carrying SCLC and on charge carrier mobility extracted from susceptance
PublikacjaThe work presents small signal admittance spectra of a sandwich system with thin organic layer carrying a space charge limited current. The effect of series resistance of electrodes on the spectra is discussed. Spectra of small signal capacitance are added to get more detailed insight. The analysis performed shows that the series resistance can affect both parts of small signal response within a whole range of frequency. Moreover,...
-
Electroactive polymer/graphene oxide nanostructured composites; evidence for direct chemical interactions between PEDOT and GOx
PublikacjaThis work concerns electrochemical synthesis of nanocomposites consisting of conducting polymer and reduced graphene oxide (rGOx) as electrode materials for supercapacitors. The electrosynthesis was performed in an aqueous solution of the 3,4-ethylenedioxytiophene (EDOT) monomer and graphene oxide (GOx) without supporting electrolyte. The amount of GOx was optimized to obtain the best electrochemical performance of the nanocomposite...
-
Study of the electrochemical stability of polypyrrole coating on iron in sodium salicylate aqueous solution
PublikacjaIn this work electrochemical stability of optimized PPy film on iron in aqueous solution of sodium salicylate is studied. The main drawback of conducting polymers is their possibility to undergo an irreversible degradation (overoxidation). The overoxidized polymers lose their properties, for example, conductivity and redox activity, what excludes them from some practical applications. This study demonstrates that lowering the concentration...
-
Electric transport in organic system with planar DBP/F16ZnPc junction on the basis of direct current and small signal admittance spectra analysis
PublikacjaThe objective of this work was to determine electric transport in the organic device based on a planar junction of electron donor and electron acceptor materials, namely ITO/MoO3/DBP/F16ZnPc/BCP/Ag. The analysis reported herein was based on direct current-voltage measurements and small-signal admittance spectra in the dark and under illumination. Such analysis may provide information on potential barriers, parasitic resistances...
-
Preparation of bicyclic β-lactam and bicyclic 1,3- oxazinone scaffolds using combined cycloaddition and metathesis processes
PublikacjaA simple, efficient two-step method for the preparation of heterobicyclic compounds was developed. Starting from 5-acyl or 5-carbamoyl-2,2- dimethyl-1,3-dioxa-4,5-dione bicyclic scaffolds of 1-azabicyclo[5.2.0]non- 3-en-9-one, 6,9,10,10a-tetrahydro-4H-[1,3]oxazino[3,2-a]azepin-4-one, and 6,9,10,10a-tetrahydro-2H-[1,3]oxazino[3,2-a]azepine-2,4(3H)-dione were prepared using cycloaddition of thermally generated ketenes to aldimines...
-
Electrode materials for electrochemical capacitors based on poly(3,4-ethylenedioxythiophene) and functionalized multi-walled carbon nanotubes characterized in aqueous and aprotic electrolytes
PublikacjaWithin this work, we report a facile one-stage synthesis of nanocomposites based on functionalized carbon nanotubes (CNTs) and electroactive polymer poly(3,4-ethylenedioxythiophene). Three different composites are investigated as potential electrode materials for the electrochemical capacitors. Two of the composites contain carbon nanotubes (ox-CNTs), functionalized by acid oxidation process (65% HNO3, 120 °C). The third composite...
-
New thiourea organocatalysts and their application for the synthesis of 5-(1H-indol-3-yl)methyl-2,2-dimethyl-1,3-dioxane-4,6-diones a source of chiral 3-indoylmethyl ketenes
PublikacjaThe stereoselective properties of modified thiourea organocatalysts were tested in the Friedel–Crafts alkylation of indole with 5-arylidene-2,2-dimethyl-1,3-dioxane-4,6-diones, which produces chiral 5-((1H-indol-3-yl)(aryl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-diones. Based on a tentative reaction mechanism for ((S)-N-benzyl-2-(3-(3,5-bis (trifluoromethyl)phenyl)thioureido)-N,3,3-trimethylbutanamide organocatalysts, modifications...
-
Tmscl as a rate accelerating additive in acylations of amines with 5-(α-amino- α'-hydroxy)methylene meldrum's acids
PublikacjaAspects are presented of the acylation of amines, alcohols and thiols with 5-(α-amino- α'-hydroxy)methylene Meldrum's acids. We placed special emphasis on the acylation reaction of secondary amines with 5-(α-amino- α'-hydroxy)methylene Meldrum's acids, which, due to their basicity, caused problems concerning salt formation with a Meldrum acid derivative. We found that secondary amines, which react at the slowest rate and with a...
-
Novel calix[4]resorcinarenes with side azobenzo-15-crown-5 residues
PublikacjaZsyntezowano nowe kaliks[4]rezorcareny z dwoma lub czteroma resztami azobenzo-15-korony-5 w dowolnym pierścieniu. Związki te otrzymano w reakcji kondensacji rezorcynolu z odpowiednimi aldehydami (acetalami).
-
Electrostatic interface recombination in the system of disordered materials characterized by different permittivities
PublikacjaWe report on the analysis of an electrostatic interface recombination in a system consisting of disordered organic materials. This process is a consequence of the polarization effect which takes place at the interface of two phases characterized by different permittivities. In this paper, the impact of tail and deep localized states on the recombination order is demonstrated. We also discuss the influence of temperature on this...
-
Electrochemical characterization of a composite comprising PEDOT/PSS and N doped TiO2 performed in aqueous and non-aqueous electrolytes
PublikacjaNitrogen doped titania (N-TiO2) was used as an inorganic component of composite electrodes containing poly(3,4-ethylenedioxythiophene) with poly(4-styrenesulphonate) PEDOT/PSS/N-TiO2. The composite materials were obtained by direct electrodeposition from an N-TiO2 suspension containing polyelectrolyte (NaPSS) and monomer EDOT. The electrodes were electrochemically tested in aqueous and non-aqueous electrolytes using cyclic voltammetry...
-
Electrochemical synthesis and characterization of nanocomposites based on poly(3,4-ethylenedioxythiophene) and functionalized carbon nanotubes
PublikacjaThis work is focused on new composite materials consisting of poly(3,4-ethylenedioxythiophene) (pEDOT) and functionalized multi-walled carbon nanotubes synthesized electrochemically. Three types of composites were synthesized: the first one containing carbon nanotubes with carboxyl groups (covalent functionalization), the second one containing oxidized carbon nanotubes ox-MWCNTs (with different oxygen-rich polar groups) (covalent...