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Realization of multi-operand modular adders in the FPGA technology
PublikacjaW pracy opisano projektowanie i realizację struktur wielooperandowych sumatorów modularnych (MOMA) w środowisku Xilinx FPGA z użyciem technologii Virtex-6. Projekt oparty jest na pamięciach LUT (26x1), które symulują małe pamięci RAM służące jako podstawowy komponent do realizacji sumatorów. W pracy pokazano MOMA dla dodawania modularnego operandów 5-bitowych. Najpierw rozważono ogólne struktury MOMA i następnie dwa podstawowe...
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New Tetragonal ReGa5(M) (M = Sn, Pb, Bi) Single Crystals Grown from Delicate Electrons Changing
PublikacjaSingle crystals of the new Ga-rich phases ReGa~5(Sn), ReGa~5(Pb) and ReGa~5(Bi) were successfully obtained from the flux method. The new tetragonal phases crystallize in the space group P4/mnc (No. 128) with vertex-sharing capped Re2@Ga14 oblong chains. Vacancies were discovered on the Ga4 and Ga5 sites, which can be understood as the direct inclusion of elemental Sn, Pb and Bi into the structure. Heat capacity measurements were...
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Sterowanie czujnikami pracującymi w sieci zigbee przy pomocy komend glosowych
PublikacjaPrzedstawiono bezprzewodową sieć sensorową, pobierającą i przekazującą informacje z czujników temperatury i oświetlenia sterowanych głosem. Funkcjonalność systemu może zostać wykorzystana do sterowania urządzeniami automatyki domowej. System składa się z trzech zasadniczych elementów: koordynatora sieci ZigBee, urządzenia końcowego (pomiarowego) wyposażonego w czujniki światła i temperatury oraz komputera PC. Użytkownik może zarządzać...
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Optimal state feedback controller for balancing cube
PublikacjaIn this paper, a nonlinear balancing cube system is considered, the concept for which is based on an inverted pendulum. The main purpose of this work was the modelling and construction of a balancing cube with the synthesis of the control system. The control objectives included swing-up and stabilization of the cube on its vertex at an unstable equilibrium. Execution of the intended purpose required, first, deriving a cognitive...
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As causas do trincamento a frio de um ação submetido a soldagem subaquática
PublikacjaA soldagem subaquàtica usada na confeccao de juntas de acos de alta resistencia aumenta a sua susceptibilidade ao trincamento a frio, um efeito decorrente da transferencia de calor muito mais rapida a partir da area de soldagem e da presenca de hidrogenio difusivel, o que causa aumento da fragilidade do metal. Este trabalho avalia esta propensao ao trincamento a frio do aco S355G10+N usado na construcao de estrururas hidrotecnicas...
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Uwagi o usuwaniu ze ścieków piasku.
PublikacjaPrzeanalizowano stosowane metody usuwania ze ścieków piasku pod kątem ich efektywności oraz złozoności stosowanych urządzeń. Odnotowano występujące problemy z właściwym funkcjonowaniem piaskowników, istotne wobec wzrostu kosztu składowania odpadów. Przedyskutowano możliwość stosowania separatorów płuczących.
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All-gather Algorithms Resilient to Imbalanced Process Arrival Patterns
PublikacjaTwo novel algorithms for the all-gather operation resilient to imbalanced process arrival patterns (PATs) are presented. The first one, Background Disseminated Ring (BDR), is based on the regular parallel ring algorithm often supplied in MPI implementations and exploits an auxiliary background thread for early data exchange from faster processes to accelerate the performed all-gather operation. The other algorithm, Background Sorted...
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Micro-Raman spectroscopy in the studies of multiphase separated polyurethanes. [online] W: [Proc.] UTECH Europe 2003 . The International Polyurethane Industry Conference and Exhibition. 25/26/27 March 2003, The Hague, Netherlands. London: Crain Communications Ltd. Dostępny w World Wide Web: http://UTECH-2003.com + wydruk.**2003 [s. 123-130 bibliogr. 41 poz.]Mikro-Ramanowska spektroskopia w badaniach poliuretanów wykazujących separację wielofazową.
PublikacjaPrzedmiotem badań były trzy próbki poliuretanowe o zawartości 30% segmentówsztywnych otrzymanych z politlenku propylenu, diizocyjanianu difenylometanui butanodiolu. Próbki te wykazują morfologię wielofazową, w której można wy-różnić globule i sferolity rozproszone w matrycy polimerowej.Za pomocą spek-troskopii mikro-Ramana przeprowadzono mikroanalizę chemiczną wszystkich ele-mentów morfologicznych. Stwierdzono odmienny skład...
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Analytical procedures for quality control of pharmaceuticals in terms of residual solvents content: Challenges and recent developments
PublikacjaResidual solvents play an important role in the synthesis of drugs and in product formulations. In addition, they pose a serious problem, that is toxicity, as many of them exhibit toxic or environmentally hazardous properties. Therefore, constant monitoring of quality control is needed. In this study, we present an overview of regulatory and general methods described by various pharmacopoeias. Then, the most commonly used methodologies...
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Searching for Solvents with an Increased Carbon Dioxide Solubility Using Multivariate Statistics
PublikacjaIonic liquids (ILs) are used in various fields of chemistry. One of them is CO2 capture, a process that is quite well described. The solubility of CO2 in ILs can be used as a model to investigate gas absorption processes. The aim is to find the relationships between the solubility of CO2 and other variables—physicochemical properties and parameters related to greenness. In this study, 12 variables are used to describe a dataset...
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Pharmaceutical and forensic drug applications of chiral supercritical fluid chromatography
PublikacjaTHE SUPERCRITICAL FLUID IS AN EXCELLENT CHOICE AS THE CHROMATOGRAPHIC MOBILE PHASE BECAUSE IT ALLOWS RAPID SEPARATION WITH HIGH EFFICIENCY AND APPLICATIONS INVOLVING ENANTIORESOLUTION ARE COMMON. SUPERCRITICAL FLUID CHROMATOGRAPHY (SFC) IS INCREASINGLY USED FOR ANALYTICAL, SEMI-PREPARATIVE AND PREPARATIVE PURIFICATION OF CHIRAL COMPOUNDS, INCLUDING PRODUCTION OF ENANTIOMERS THAT ARE MAINLY ENCOUNTERED DURING DRUG DEVELOPMENT. SFC...
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Experimental investigation of heat transfer enhancement in straight and U-bend double-pipe heat exchanger with wire insert
PublikacjaIn this paper, the possibility of heat transfer enhancement in the U-bend exchanger was presented. Experimental research has been carried out for four individual heat exchanger constructions i.e. plain tube in tube, turbulized tube in tube, plain U-bend and U-bend with turbulator. Also, heat transfer experiments for various boundary conditions were performed to obtain reference values. In case of U-bend exchanger with and without...
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LTE as a Trunking - Dispatch System
PublikacjaIn the paper solutions of trunking-dispatch systems based on the LTE system are presented. The solution in the form of separate LTE/TDD trunking system is discussed, and the concept of the LTE/FDD trunking system operating in the infrastructure of public, mobile networks is characterised.
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The Effect of Temperature on Wear Mechanism of the AlCrN Coated Components
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Hyperbranched polyethylenimine functionalized silica/polysulfone nanocomposite membranes for water purification
PublikacjaHyperbranched polyethyleneimine functionalized silica (PEI-SiO2) nanoparticles with considerable hydrophilicity were synthesized and incorporated into a polysulfone (PSF)/dimethylacetamide (DMA)/polyvinylpyrrolidone (PVP) membrane casting solution in five different ratios to fabricate PEI-SiO2/PSF nanocomposite membranes using nonsolvent-induced phase separation. The hydrophilic PEI-SiO2 nanoparticles were characterized by TEM,...
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Measurements of Activity Coefficients at Infinite Dilution for Organic Solutes in the Ionic Liquids N-Ethyl- and N-Octyl-N-methylmorpholinium Bis(trifluoromethanesulfonyl)imide. A Useful Tool for Solvent Selection
PublikacjaIn recent years, many papers describing ionic liquids (IL) as promising solvents in separation techniques have been published. The conscious choice of appropriate ionic liquid as absorption media in effective extraction of selected types of analytes requires deeper understanding of the analyte−IL interactions. Therefore, intensive research is conducted to determine the values of activity coefficient at infinite dilution, which...
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Steady magnetohydrodynamic flow in a diverging channel with suction or blowing
PublikacjaAn analysis is made of steady two-dimensional divergent flow of an electrically conducting incompressible viscous fluid in a channel formed by two non-parallel walls, the flow being caused by a source of fluid volume at the intersection of the walls. The fluid is permeated by a magnetic field produced by an electric current along the line of intersection of the channel walls. The walls are porous and subjected to either suction...
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The influence of storage time on the performance of polypropylene membranes applied for membrane distillation
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Water Purification by Membrane Distillation Process
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Removal of metal particles from carbon nanotubes using conventional and microwave methods
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Recovery of hydrochloric acid from metal pickling solutions by membrane distillation
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The fermentation process integrated with membrane distillation
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The influence of salt in solutions on hydrochloric acid recovery by membrane distillation
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CONCENTRATION OF NaCl SOLUTION BY MEMBRANE DISTILLATION INTEGRATED WITH CRYSTALLIZATION
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The influence of magnetic water treatment on CaCO3 scale formation in membrane distillation process
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Membrane distillation with laminar flow
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How to model temporal changes in nontargeted metabolomics study? A Bayesian multilevel perspective
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Evaluation of sample injection precision in respect to sensitivity in capillary electrophoresis using various injection modes
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Disposable pipette tips extraction: Fundamentals, applications and state of the art
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Application of ionic liquid-based microwave-assisted extraction of malachite green and crystal violet from water samples
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Enantioselective comprehensive two-dimensional gas chromatography of lavender essential oil
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Headspace liquid phase microextraction for quantitation of hexanal in potato crisps by gas chromatography
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Enantioselective comprehensive two-dimensional gas chromatography. A route to elucidate the authenticity and origin ofRosa damascena Milleressential oils
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Determination of fluoride as fluorosilane derivative using reversed-phase HPLC with UV detection for determination of total organic fluorine
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Micellar liquid chromatography for lipophilicity determination of new biologically active 1,3‐purinodiones
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Magnetic composite adsorbents of phenolic compounds with superior corrosion resistance
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Synthesis and adsorptive properties of sulfonated nanocomposites based on carbon-encapsulated iron nanoparticles and styrene-p-divinylbenzene copolymer
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Effect of process parameters on fouling and stability of MF/UF TiO2 membranes in a photocatalytic membrane reactor
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Selective transport of zinc ions through novel polymer inclusion membranes (PIMS) containing β-diketone derivatives as carrier reagents
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The Influence of Alkyl Chain Length and Steric Effect on the Stability Constants and Extractability of Co(II) Complexes with 1-Alkyl-2-Methylimidazoles
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Solvent extraction of copper ions by 3-substituted derivatives of β-diketones
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Thermodynamic study of new antiepileptic compounds by combining chromatography on the phosphatidylcholine biomimetic stationary phase and differential scanning calorimetry
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Comparison of mouse plasma and brain tissue homogenate sample pretreatment methods prior to high-performance liquid chromatography for a new 1,2,4-triazole derivative with anticonvulsant activity
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High-performance liquid chromatography thermodynamic study of new potential antiepileptic compounds on a cholesterol column using isocratic elution with methanol/water and acetonitrile/water eluent systems
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Solid-phase extraction using octadecyl-bonded silica modified with photosynthetic pigments from Spinacia oleracea L. for the preconcentration of lead(II) ions from aqueous samples
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Salinity and pH as factors affecting the passive sampling and extraction of pharmaceuticals from water
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Complexing and Chelating Agents Immobilized on Silica Gel and Related Materials and Their Application for Sorption of Inorganic Species
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Static and dynamic superheated water extraction of essential oil components fromThymus vulgarisL.
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In-tube extraction for the determination of the main volatile compounds in Physalis peruviana L
PublikacjaAn analytical procedure based on in-tube extraction followed by gas chromatography with mass spectrometry has been developed for the analysis of 24 main volatile components in cape gooseberry (Physalis peruviana L.) samples. According to their chemical structure, the compounds were organized into different groups: one hydrocarbon, one aldehyde, four alcohols, four esters, and 14 monoterpenes. By single-factor experiments, incubation...
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Reliability and efficiency of pollution removal during long-term operation of a one-stage constructed wetland system with horizontal flow
PublikacjaThe paper presents the results of a study of the reliability and efficiency of pollutant removal during long term operation of a one-stage constructed wetland system with horizontal flow. The flow rate of the wastewater treatment plant was 1.2 m3·d-1 during the research period. Physical and chemical analyses of raw wastewater and treated effluent were carried out in the years 1997–2010 (14 years). During this study period, 56 series...