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Application of headspace-solid phase microextraction followed by gas chromatography-mass spectrometry to determine short-chain monocarboxylic acids in cattle farm wastewater and waste landfill leachates
PublikacjaZaproponowano metodykę oznaczania krótkołańcuchowych kwasów monokarboksylowych w ściekach z hodowli bydła i odciekach ze składowisk zawierających organiczne odpady, oparta na technice mikroekstrakcji do fazy stacjonarnej z fazy nadpowierzchniowej próbek ciekłych, w połączeniu ze sprzężonym układem GC-MS.
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Determination of tributylotin (TBT) in marine sediment using pressurised liquid extraction-gas chromatography-isotope dilution mass spectrometry (PLE-GC-IDMS) with a hexane-tropolone mixture
PublikacjaOpracowano metodę oznaczania zawartości tributylocyny w próbkach osadu morskiego. Na etapie izolacji zastosowano technikę przyspieszonej ekstrakcji za pomocą roztworu tropolonu w heksanie.Na etapie oznaczeń końcowych wykorzystano technikę chromatografii gazowej, stosując metodę spektrometrii mas rozcieńczenia izotopowego. Wyznaczono parametry walidacyjne opracowanej metody: granicę wykrywalności, precyzję, poprawność i niepewność.
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Surface characteristics of glass fibres covered with an aluminum layer after a chemical modification process using secondary ion mass spectrometry (SIMS) and atomic force microscopy (AFM)
PublikacjaPrzedstawiono wyniki z badań powierzchni modyfikowanych włókien szklanych (przed i po procesie chemicznej modyfikacji ich powierzchni), które są kandydatem na przyszły oryginalny bezmatrycowy materiał odniesienia lotnych analitów etenu (C2H4) metodami spektrometrii mas jonów wtórnych oraz mikroskopii sił atomowych. Badania miały na celu obserwację zmian oraz procesów, jakie zaszły na powierzchni włókien szklanych pokrytych...
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Characterization of GM3 Gangliosides in Human Milk throughout Lactation: Insights from the Analysis with the Use of Reversed-Phase Liquid Chromatography Coupled to Quadrupole Time-Of-Flight Mass Spectrometry
PublikacjaGangliosides are complex lipids found in human milk that play important structural and biological functions. In this study, we utilized reversed-phase liquid chromatography coupled to quadrupole time-of-flight mass spectrometry to evaluate the molecular distribution of GM3 in human milk samples collected at distinct lactation stages, ranging from colostrum to advanced lactation samples. Throughout lactation, GM3 d40:1 emerged as...
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Green, simple analytical method for biogenic amines determination in fruit juice samples using salting-out assisted liquid-liquid microextraction and gas chromatography-mass spectrometry
PublikacjaSalting-out assisted liquid-liquid microextraction (SALLME) was integrated with the derivatization procedure to establish a one-step sample pre-treatment approach for rapid analysis of 14 biogenic amines (BAs) in fruit juices. The methodology consists of salting-out of analytes, derivatization with ethyl chloroformate (ECF), extraction with ethyl acetate (EtAc), and the analysis of the derivatized BAs using gas chromatography-mass...
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An algorithm for preliminary estimating hull structure mass and mass centre height of inland navigation ships
PublikacjaPrzedstawiono algorytm obliczeniowy służący do wstępnego wyznaczania masy i wysokości środka ciężkości konstrukcji kadłuba statków śródlądowych. Algorytm opracowano opierając się na zaleceniach zawartych w Przepisach Klasyfikacji i Budowy Statków Śródlądowych PRS oraz zastosowano uproszczoną metodę wyznaczania mas usztywnień poszycia kadłuba. Algorytm dotyczy wymiarowania konstrukcji klasycznych statków służących do przewozu drobnicy,...
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Simultaneous analysis of non-steroidal anti-inflammatory drugs and estrogenic hormones in water and wastewater samples using gas chromatography–mass spectrometry and gas chromatography with electron capture detection
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Application of gas flow headspace liquid phase micro extraction coupled with gas chromatography-mass spectrometry for determination of 4-methylimidazole in food samples employing experimental design optimization
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The presence of polycyclic aromatic hydrocarbons in disposable baby diapers: A facile determination method via salting-out assisted liquid-liquid extraction coupled with gas chromatography-mass spectrometry
PublikacjaIn this paper we demonstrate the development of the extraction procedure of polycyclic aromatic hy- drocarbons from baby diapers along with their quantification by gas chromatography-mass spectrometry. Apart from covering plastic foil, disposable baby diapers contain sorbents intended to absorb urine and feces. A hygroscopic, adsorptive, and tough-to-homogenize fibrous sorbent, represents an analytical chal- lenge to analytical...
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Customers Perspective on Mass-customization of Houses
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The control software of the portable raman spectrometer
PublikacjaThe paper contains a description of the control software of a portable Raman spectrometer which was built in the Department of Optoelectronics and Electronic Systems Faculty of Electronics, Telecommunications and Informatics Gdansk University of Technology. The software has modular structure, which includes the laser control module and the spectrum acquisition module (laser power selection, working mode and data acquisition time)...
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Association between plasma proteome profiles analysed by mass spectrometry, a lymphocyte-based DNA-break repair assay and radiotherapy-induced acute mucosal reaction in head and neck cancer patients
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Novel analytical approach for real-time monitoring of volatile Maillard reaction products emitted from the sugar-amino acid model system using proton transfer reaction mass spectrometry
PublikacjaIn the presented research, volatile Maillard reaction products formation in the two sugar-amino acid model systems, namely glucoselysine and ribose-lysine model systems were investigated using proton transfer reaction mass spectrometry. Obtained data were supported by the reference method, i.e., UV/Vis spectrometry. A number of volatile organic compounds were selected based on the correlation of the effect of Maillard reaction...
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Determination of metals in water samples by atomic absorption spectrometry and flame emission spectrometry
PublikacjaMetal species in environmental waters are relevant to characterize the metal toxicity, the mobility between different environmental compartments, and for remediation purposes in case of contamination. The concentration of many trace metals in natural water samples are generally at µg/l level. The paper describes determination of metals in water samples based on flame atomic emission and flame atomic absorption spectrometry.
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Mobile chromatographs and spectrometers for the analysis of chemical warfare agents
PublikacjaThis article describes the technological state of readiness regarding mobile chromatographs and spectrometers and their appiicability for the analysis of chemical warfare agents (CWAs), degradation products, simulants, and precursors.
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Loads on walls and inserts in a mass-flow silos
PublikacjaArtykuł przedstawia numeryczną symulację przepływu materiału sypkiego w silosach z uwzględnieniem wkładki silosowej o kształcie podwójnego stożka. Pokazany został wpływ zamontowanej wkładki na rodzaj przepływu oraz na wartość i kształt naporu na ścianę silosu.
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Improvement of radiotracers experiments in mass transfer processes
PublikacjaThe greatest part of industrial mass transfer is based on continuous transportation of different substances throughout especially constructed installations. In that kind of practice, a flow of such mass in each part determines the process unit and can be described by the residence time distribution (RTD) of the substance inside this unit. This parameter may be evaluated by the properly arranged tracer experiment. It is worthwhile...
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Portable raman spectrometer with two excitation wavelengths
PublikacjaSelected problems of development of a portable Raman spectrometer having small size, reduced power consumption and robust construction are shown. The device dedicated for semiskilled personnel uses two lasers: 785nm and 355nm. Results of preliminary tests are presented. Also data processing procedures as well as problems referred to Raman signals acquisition through packages and influence of interfering signals are discussed.
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Portable Raman spectrometer - design rules and applications
PublikacjaRaman spectroscopy has become more popular due to its new prospective field applications in forensic sciences, war against terrorism, environment protection and other field chemical analysis. Raman spectrometers can be miniaturised to portable devices and their price is decreasing due to development of optoelectronics components. Unfortunately, this technology has still numerous limitations that influence their design and limit...
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Portable raman spectrometer for maritime security applications
PublikacjaThe fast identification of explosives, narcotics and other chemicals carried on board of ships or transported in containers to the harbors is an important problem of maritime security. Raman spectroscopy is widely used for fast identification of various chemicals. Continuous progress in the field of photonics has resulted in commercial availability of low-power compact Raman spectrometers which can be integrated into portable systems....
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Detection of illicit chemicals by portable Raman spectrometer
PublikacjaThe Raman spectrometers can be built as the portable devices and can be used in various places to detect illicit chemicals. This method has become popular due to deficiency of other fast methods that could be applied against terrorist attacks or could help police at their work. The conception of a portable Raman spectrometer has been presented. The description enclosures presentation of the prepared device and its possible applications...
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Accurate, Direct, and High-Throughput Analyses of a Broad Spectrum of Endogenously Generated DNA Base Modifications with Isotope-Dilution Two-Dimensional Ultraperformance Liquid Chromatography with Tandem Mass Spectrometry: Possible Clinical Implication
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“Dilute & Shoot” approach for rapid determination of trace amounts of nicotine in zero-level e-liquids by reversed phase liquid chromatography and hydrophilic interactions liquid chromatography coupled with tandem mass spectrometry-electrospray ionization
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Fast, sensitive and reliable multi-residue method for routine determination of 34 pesticides from various chemical groups in water samples by using dispersive liquid – liquid microextraction coupled with gas chromatography – mass spectrometry
PublikacjaA simple and efficient dispersive liquid-liquid microextraction technique (DLLME) was developed by using a mixture of two solvents: 40 μL of tetrachlorethylene (extraction solvent) and 1.0 mL of methanol (disperser solvent), which was rapidly injected with a syringe into 10mL ofwater sample. Some important parameters affecting the extraction efficiency, such as type and volume of solvents, water sample volume, extraction time,...
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“Dilute & Shoot” approach for rapid determination of trace amounts of nicotine in zero-level e-liquids by reversed phase liquid chromatography and hydrophilic interactions liquid chromatography coupled with tandem mass spectrometry-electrospray ionization
PublikacjaTwo analytical procedures are proposed where HILIC and RPLC techniques are coupled with tandem mass spectrometry detection for rapid determination of trace amounts of nicotine in zero-level liquids for electronic cigarettes. Samples are prepared on the basis of the approach “dilute & shoot” which makes this important step quick and not complicated. The chromatographic separation was carried out on a Zorbax XDB column (RPLC method)...
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Heat and mass exchange in the process of condensation on critical droplets.
PublikacjaSformułowano model wzrostu kropli krytycznej podając równania zmiany masy i temperatury kropli. Pokazano formę zlinearyzowaną tych równań dobrze aproksymującą wzrost kropli w poblizu wymiaru krytycznego. Podano rozwiązanie układu zlinearyzowanego uzależniając zmianę temperatury od zmiany masy kropli i czasu charakterystycznego.
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Detection of additional mass in rods: Experimental and numerical investigation
PublikacjaW pracy przedstawiono wyniki badań eksperymentalnych i numerycznych nad wykorzystaniem zmian w propagacji fal sprężystych do detekcji masy skupionej znajdujacej się w konstrukcji prętowej.
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Modelling of heat and mass transfer through wooden buildings
PublikacjaThe aim of this review paper is to examine the most recent available studies dealing with theoretical, numerical and experimental aspects related to modelling of heat and mass transfer through wooden buildings. The main thermophysical, mechanical and hygrometric properties of wood are firstly discussed. Then, the basic governing equations of heat and mass transfer phenomena are presented. A detailed description of the physical...
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Experimental study on static and dynamic properties of polymer mass
PublikacjaA new method of repairing damaged structures by filling the cracks with a specially prepared polymer mass has been recently proposed. This new and innovative technique, known as the Flexible Joint Method (FJM), is mainly dedicated to masonries and historical objects, where minimum intervention is permitted. The flexible joint bonds the disrupted elements and ensures further safe exploitation of a damaged structure. The aim of the...
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Heat and mass transfer in air-fed pressurised suits
PublikacjaOpisano konieczność modelowania transportu masy i ciepła w kombinezonach ochronnych. Omówiono różne sposoby modelowania wymiany ciepła, łącznie ze sprzężoną wymianą ciepła. Uwzględniono również ludzki metabolizm i turbulentne mechanizmy wymiany masy i ciepła. Publikacja opisuje również sposób modelowanie turbulentnych przepływów wieloskładnikowych. Pokazano również porównanie obliczeń z eksperymentem.
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Mass Customization jako alternatywa dla produkcji masowej
PublikacjaW publikacji zaprezentowano kluczowe zagadnienia charakteryzujące koncepcję Mass Customization w porównaniu z klasyczną koncepcją produkcji masowej. Przedstawiono definicje i cechy charakteryzujące obie koncepcje produkcji, podjęto próbę porównania obu koncepcji. Skupiając się na koncepcji Mass Customization zestawiono wymagania do projek-towania procesu produkcyjnego wg koncepcji. Skrótowo przedstawiono również wyniki analiz wybranego...
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Mass and momentum conservation in the simplified flood routing models
PublikacjaW pracy wykazano, że uproszczone modele fal wezbraniowych w postaci fali kinematycznej reprezentują w przypadku liniowych zarówno zasadę zachowania masy jaki i pędu, natomiast w przypadku nieliniowym, reprezentują albo zasadę zachowania masy albo pędu, zależnie od postaci zachowawczej równania. Ponadto wykazano, iż nieliniowa fala dyfuzyjna nie spełnia ani całkowowej zasady zachowania masy ani pędu.
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Hydrodynamics and Mass Transfer Analysis in BioFlow® Bioreactor Systems
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Heat and mass transfer in air-fed pressurised suits
PublikacjaOpisano konieczność modelowania transportu masy i ciepła w kombinezonach ochronnych. Omówiono różne sposoby modelowania wymiany ciepła, łącznie ze sprzężoną wymianą ciepła. Uwzględniono również ludzki metabolizm i turbulentne mechanizmy wymiany masy i ciepła. Publikacja opisuje również sposób modelowanie turbulentnych przepływów wieloskładnikowych. Pokazano również porównanie obliczeń z eksperymentem.
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Mass transfer in Spinning Fluids Reactor — Measurement and prediction
PublikacjaSpecific mass transfer area (a) and overall volumetric mass transfer coefficient (kLa) are mass transfer parameters commonly used in the description and comparison of various chemical reactors’ constructions. Determination of these was performed for Spinning Fluids Reactor (SFR). Sodium sulfite oxidation in the presence of cobalt ion catalyst was used for the determination of a and kLa. The a and kLa were successful predicted....
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Low energy electron mass stopping power in H2
PublikacjaWe present experimental mass stopping powers of electrons in gaseous H2 obtained with a newly developed electron time-of-flight spectrometer, for the incident electron energy range of 10eV to 25eV. In our procedure the average energy loss is derived from our conversion of measured electron time-of-flight spectra into equivalent electron energy loss spectra so as to obtain the values of mass stopping power for electron scattering...
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“In situ” observations of carbon nanotube generation in CVD cell coupled to spectrometers
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A framework for risk matrix design: A case of MASS navigation risk
PublikacjaRisk matrix, a tool for visualizing risk assessment results, is essential to facilitate the risk communication and risk management in risk-based decision-making processes related to new and unexplored socio-technical systems. The use of an appropriate risk matrix is discussed in the literature, but it is overlooked for emerging technologies such as Maritime Autonomous Surface Ships (MASS). In this study, a comprehensive framework...
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Experimental Study on Polymer Mass Used to Repair Damaged Structures
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Serum mass profile signature as a biomarker of early lung cancer
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Uncertainty of the liquid mass flow measurement using the orifice plate
PublikacjaThe article presents an estimation of measurement uncertainty of a liquid mass flow using the orifice plate. This subject is essential because of the widespread use of this type of flow meters. Not only the quantitative estimation but also the qualitative results of those measurements are important. To achieve these results the authors of the paper propose to use the theory of uncertainty. The article shows the analysis of the...
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Left Ventricular Mass: Correlation with Fatness, Hemodynamics and Renal Morphology
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Capillary Electrophoresis in Determination of Low Molecular Mass Organic Acids
PublikacjaThis paper presents overviews the capabilities of capillary electrophoretic techniques to determine low molecular mass organic acids in a variety of aqueous, gas and solid samples. It mainly focuses on short - chain carboxylic acids containing one or more carboxylic groups and possibly some other functional groups (hydroxyl, keto-, amino- etc.). Finally the procedures applied to the determine the acids in different matrices are...
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Estimating the uncertainty of the liquid mass flow using the orifice plate
PublikacjaThe article presents estimation of measurement uncertainty of a liquid mass flow using the orifice plate. This subject is essential because of the widespread use of this type of flow meters, which renders not only the quantitative estimation but also qualitative results of this type so those measurements are important. To achieve this goal, the authors of the paper propose to use the theory of uncertainty. The article shows the...
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Experimental study on polymer mass used to repair damaged structures
PublikacjaA new method of repairing damaged structures by injecting the cracks with specially designed polymer mass (flexible two-component grout based on polyurethane resin) has been recently proposed. The technique is mainly dedicated to damaged masonries, especially historical structures where minimum intervention is permitted. The cracks are filled with the special injection, forming the flexible joints bonding the disrupted structural...
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Heritability of Plasma Adiponectin Levels and Body Mass Index in Twins
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Monitoring of volatile organic compounds (VOCs) in atmospheric air. Part I. On-line gas analyzers
PublikacjaThe paper reviews the subject literature concerning the analytical instruments routinely used for monitoring volatile organic compounds in atmospheric air. The analyzers are classified as stationary or mobile according to their ease of transport. Stationary DOAS (Differential Optical Absorption Spectroscopy) analyzer is characterized, as are MIMS (Membrane Introduction Mass Spectrometry), MESI (Membrane Extraction with Sorbent...
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Detection system for optical coherence tomography: Czerny-Turner spectrometer
PublikacjaResearch methods based on spectral analysis have powerful impact on development in many field of science. Signal spectrum can be a source of useful and important data. It enables to obtain information about physical and chemical properties of tested materials. This paper has been devoted to describe optical design for high resolution spectrometer, which is significant element of optical coherence tomography (OCT) systems. Designed...
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Dopants and gas modifiers in ion mobility spectrometry
PublikacjaThe ion mobility techniques, including the most commonly used drift-tube ion mobility spectrometry (IMS) and differential mobility spectrometry (DMS), are used successfully for the detection of a wide range of organic compounds in the gas phase. In order to improve detection quality, admixtures are added to gas streams flowing through the detector. Dopants mostly prevent the ionization of interfering chemicals however, better detection...
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Drawing maps with advice
PublikacjaRozważamy następujący problem obliczeniowy. Agent zostaje umieszczony w wierzchołku nieznanego mu grafu. Wierzchołki grafu są nierozróżnialne, natomiast krawędzie posiadają numery portów. Zadaniem agenta jest wyznaczenie mapy, tzn. obliczenie izomorficznej kopii grafu, lub obliczenie dowolnego drzewa spinającego grafu. Bez dodatkowej informacji zadań tych nie można wykonać. W artykule wyznaczamy oszacowania na minimalną liczbę...