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Chiral and achiral crystals, charge-assisted hydrogen-bond patterns and self-organization of selected solid diaminium thiosulfates
PublikacjaAbstract A series of diaminium thiosulfates, derivatives of diamines: NH2CH2CH(CH3)NH2 (1) and NH2(CH2)nNH2, n = 3-6 (2-5 respectively)and thiosulfuric acid were prepared and their structures determined by crystal X-ray diffraction analysis. Compounds 1, 2 and 4 turned out to be hydrates. The crystal structure of 1,2-proylenediaminium thiosulfate is chiral and exhibits spontaneous resolution. Crystals for both enantiomers...
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Expedited Feature-Based Quasi-Global Optimization of Multi-Band Antenna Input Characteristics with Jacobian Variability Tracking
PublikacjaDesign of modern antennas relies—for reliability reasons—on full-wave electromagnetic simulation tools. In addition, increasingly stringent specifications pertaining to electrical and field performance, growing complexity of antenna topologies, along with the necessity for handling multiple objectives, make numerical optimization of antenna geometry parameters a highly recommended design procedure. Conventional algorithms, particularly...
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Synthesis of compounds with C-P-P and C=P-P bond systems based on the phospha-Wittig reaction
PublikacjaA reactivity study of a β-diketiminate titanium(III) phosphanylphosphido complex [MeNacNacTi(Cl){η2-P(SiMe3)-PtBu2}] (1) towards ketones such as benzophenone, 9-fluorenone, acetophenone, cyclopentanone, cyclohexanone and cycloheptanone is reported. The reactions of 1 with aromatic ketones (without α-protons) directly lead to the Ti(III) complex [MeNacNacTi(μ2-Cl)(OSiMe3)] (5) as well as Ti(IV) complexes with the pinacol condensation...
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Does the low optical band gap of yellow Bi3YO6 guarantee the photocatalytical activity under visible light illumination?
PublikacjaBi3YO6, which is known as an ionic conductor, was tested here as an electrode and photoanode in contact with aqueous electrolytes. Bi3YO6 was deposited onto the Pt substrate and the such prepared electrode was polarized in various aqueous electrolytes. The optical energy band gap of the material equal to 1.89 eV was determined using the Kubelka-Munk function resulting from the UV-Vis spectrum (allowed indirect transition) and also...
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Band engineering of BiOBr based materials for photocatalytic wastewater treatment via advanced oxidation processes (AOPs) – A review
PublikacjaSemiconductor based photocatalysts have been an efficient technology for water and wastewater remediation, addressing the concepts of green chemistry and sustainable development. Owing to narrow and suitable band structure, BiOBr is a promising candidate for efficient wastewater treatment via photocatalysis. Enhancement of photocatalytic properties can be obtained by various techniques like doping, element rich strategy, facet...
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Understanding the interactions between protein stabilizers and the peptide bond through the analysis of the volumetric and compressibility properties for the model systems
PublikacjaThis work confirms our earlier supposition, that volumetric and acoustic parameters for simple model proposed by us are directly related to stabilizing/destabilizing effect of osmolytes on proteins structure. The apparent molar volumes, V and the apparent molar isentropic compressions, KS,, of glycine and N,N,N –trimethylglycine (betaine) were determined from densities and speed of sound measurements in aqueous solution of N-methylacetamide...
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Global EM-Driven Optimization of Multi-Band Antennas Using Knowledge-Based Inverse Response-Feature Surrogates
PublikacjaElectromagnetic simulation tools have been playing an increasing role in the design of contemporary antenna structures. The employment of electromagnetic analysis ensures reliability of evaluating antenna characteristics but also incurs considerable computational expenses whenever massive simulations are involved (e.g., parametric optimization, uncertainty quantification). This high cost is the most serious bottleneck of simulation-driven...
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A Wideband Corrugated Ridged Horn Antenna with Enhanced Gain and Stable Phase Center for X- and Ku-Band Applications
PublikacjaIn this letter, a structure and design procedure of a novel double-flared conical horn antenna with an improved gain and a stable phase center is presented. The antenna incorporates a hybrid ridged and corrugated structure. A double-ridged section is responsible for ensuring a wideband operation, whereas the corrugated section supports the hybrid mode. The antenna impedance bandwidth (VSWR < 2) is 6 GHz to 20 GHz. Excellent performance...
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Multi-Beam Antenna for Ka-Band CubeSat Connectivity Using 3-D Printed Lens and Antenna Array
PublikacjaIn this paper, the design of a passive multi-beam lens antenna is proposed for the CubeSat space communication system as an alternative application of a 2-D microstrip antenna array that has originally been designed for a 39 GHz 5 G MU-MIMO system. The half-ellipsoid lens is 3-D printed using stereolithography (SLA) technology. The antenna prototype is capable of selecting the main beam between 16 different directions with a gain...
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Predicting cutting power for band sawing process of pine and beech wood dried with the use of four different methods
PublikacjaWood drying is an important stage in the woodworking process. After drying, wood is subject to a re-sawing process, for which a high quality surface, low material loss, and high efficiency are often required. In this paper, forecasted values were presented of cutting power for the re-sawing process of pine and beech wood that were dried with four different methods. Forecasting of cutting power for an industrial band saw machine...
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Fast Re-Design of Multi-Band Antennas by Means of Orthogonal-Direction Geometry Scaling and Local Parameter Tuning
PublikacjaApplication-driven design of antenna systems fosters a reuse of structures that have proven competitive in terms of their electrical and field performance, yet have to be re-designed for a new application area. In practice, it most often entails relocation of the operating frequencies or bandwidths, which is an intricate endeavor, normally requiring utilization of numerical optimization techniques. If the center frequencies of...
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Computational investigations of acoustic radiation from end shields of small-power electric motor
PublikacjaW artykule omówiono rozwój metod modelowania własności akustycznych maszyn elektrycznych. Wskazano na pomijalny dotąd, znaczący udział drgań tarcz łożyskowych w emitowaniu hałasu przez silniki małej mocy. Na podstawie równania falowego potencjału prędkości wyprowadzono analityczne formuły do obliczeń akustycznych w polu bliskim tarczy łożyskowej. Zamieszczono uzyskane z serii obliczeń dla pracującego silnika, rozkłady ciśnienia...
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On a method of modelling and simulation of vibration surveillance during ball end milling of flexible details
PublikacjaPraca dotyczy nadzorowania drgań podczas frezowania przedmiotów podatnych smukłym frezem kulistym, z uwzględnieniem zgodności parametrów modelu modalnego. Przeprowadzono analizę dynamiki procesu frezowania. Następnie przedstawiono analizę niestacjonarnego układu drgającego, w którym wyodrębniono podukłady: modalny, strukturalny i łączący. Do minimalizacji poziomu drgań zastosowano dopasowanie prędkości obrotowej wrzeciona do optymalnego...
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Modelling and investigation of vibration surveillance during ball end milling of curved flexible details
PublikacjaPraca dotyczy nadzorowania drgań podczas frezowania zakrzywionych przedmiotów podatnych smukłym frezem kulistym, z uwzględnieniem zgodności parametrów modelu modalnego. Dokonano analizy dynamiki niestacjonarnego układu drgającego, w którym wyodrębniono podukłady: modalny, strukturalny i łączący. Do minimalizacji poziomu drgań zastosowano dopasowanie prędkości obrotowej wrzeciona do optymalnego kąta przesunięcia fazowego. Zasadność...
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On a method of modelling and simulation of vibration surveillance during ball end milling of flexible details
PublikacjaPraca dotyczy nadzorowania drgań podczas frezowania przedmiotów podatnych smukłym frezem kulistym, z uwzględnieniem zgodności parametrów modelu modalnego. Przeprowadzono analizę dynamiki procesu frezowania. Następnie przedstawiono analizę niestacjonarnego układu drgającego, w którym wyodrębniono podukłady: modalny, strukturalny i łączący. Do minimalizacji poziomu drgań zastosowano dopasowanie prędkości obrotowej wrzeciona do optymalnego...
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The effect of fixed adsorption bed height on adsorption of gaseous mixture of volatile organic compounds
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Prediction of cutting forces during micro end milling considering chip thickness accumulation
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Global variation in anastomosis and end colostomy formation following left‐sided colorectal resection
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Tool Life and Process Dynamics in High Speed Ball End Milling of Hardened Steel
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Photocatalytic degradation of volatile and non volatile organics on titanium dioxyde particles in fluidized bed.
PublikacjaPrzeprowadzono degradację metyloetyloketonu w obecności dwutlenku tytanu jako fotokatalizatora. Badano wpływ początkowego stężenia substancji i stężenia fotokatalizatora na szybkość fotokatalitycznego rozkładu.
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Do the New Requirements for the Use of Energy Efficient Lighting Design Mean the End of Creativity?,
PublikacjaThis paper addresses issues strongly connected to recent environmental discussions which are currently taking place in Europe, Asia, America, Australia and other parts of the world about global warming, the Greenhouse Effect, light pollution and other negative impacts artificial lighting has on our planet and what can be done about it. The author also attempts to answer indirectly two of the most important questions for lighting...
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The application of Monod equation to denitrification kinetics description in the moving bed biofilm reactor (MBBR)
PublikacjaIn this paper, the kinetic constants Vmax and KCOD occurring in the Monod equation, which describe the denitrification process in the moving bed, are determined. For this purpose, a laboratory moving bed biofilm reactor (MBBR) was used. The filling of the reactor consisted of EvU Perl carriers. The experiment was carried out with an excess of nitrate, and denitrification rate was dependent on the concentration of external organic...
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Moment resistance of I-section end-plate roof girder splices; a case study
PublikacjaThis article deals with the problem of determining the resistance of end-plate connections. A nonlinear FEM model of the joint was constructed in order to predict its carrying capacity. A standard code procedure was done as well. The analyses have been done to assess atypical end-plate joints designed and constructed as a part of roof structures.
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Energy policy and the role of bioenergy in Poland
PublikacjaPrzedstawiono sytuacje energetyczną kraju. Omówiono poszczególne sektory wytwarzania energii oraz zapotrzebowania na energię i paliwa. Omówiono przekształcenia sektorów energetycznych w Polsce na przestrzeni lat 1990-2002. Na tym tle przedstawiono techniczne, ekonomiczne, społeczne i prawne aspekty rozwoju energetyki źródeł odnawialnych a w szczególności opartych o bioenergię. Przedstawiono wnioski dla Polski płynące z dotychczasowych...
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Wspomaganie oceny czynności układu oddechowego u chorych na cukrzycę, w oparciu o badania eksperymentalne oraz modelowanie procesów dyfuzji i wymiany gazowej z wykorzystaniem integracji danych wielomodalnych
PublikacjaMało poznanym negatywnym skutkiem cukrzycy jest mikroangiopatia płuc. Obecnie stosowana metoda identyfikacji mikroangiopatii polega na porównaniu dwóch pomiarów pojemności dyfuzyjnej płuc wykonanych w pozycji stojącej i pozycji leżącej. Celem przeprowadzonych badań było opracowanie metody wsparcia procesu diagnostycznego mikroangiopatii płucnej w przebiegu cukrzycy na podstawie rutynowo wykonywanych badań układu oddechowego przy...
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A Study of RME-Based Biodiesel Blend Influence on Performance, Reliability and Emissions from Modern Light-Duty Diesel Engines
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Model silnika spalinowego w formie grafów wiązań (GW).A model of the IC engine in the form of the bond graph (BG).
PublikacjaPrzedstawiono uzasadnienie użycia metody grafów wiązań do do modelowania silnika spalinowego jako źródła energii w systemach energetycznych składających się z elementów o różnej naturze fizycznej, na przykład w pojazdach hybrydowych. Przedstawiono propozycję formalizacji charakterystyki silników spalinowych wynikającą z przyjętej metody modelowania. Analityczną formę charakterystyki przedstawiono jako wielowymiarową funkcję wektorową....
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Peptide bond modification. I. Simple and efficient method of Boc-Gly[CH(OH)CH2]Gly-OH synthesis.
PublikacjaZaprezentowano prostą i efektywną metodę syntezy obu enancjomerów t-butoksykarbonylo chronionego pseudo dipeptydu (R) oraz (S)-Boc-Gly[CH(OH)CH2]Gly-OH.
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Expedited Re-Design of Multi-Band Passive Microwave Circuits Using Orthogonal Scaling Directions and Gradient-Based Tuning
PublikacjaGeometry scaling of microwave circuits is an essential but challenging task. In particular, the employment of a given passive structure in a different application area often requires re-adjustment of the operating frequencies/bands while maintaining top performance. Achieving this necessitates utilization of numerical optimization methods. Nonetheless, if the intended frequencies are distant from the ones at the starting point,...
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Cost‐efficient performance‐driven modelling of multi‐band antennas by variable‐fidelity electromagnetic simulations and customized space mapping
PublikacjaElectromagnetic (EM) simulations have become an indispensable tool in the design of contemporary antennas. EM‐driven tasks, for example, parametric optimization, entail considerable computational efforts, which may be reduced by employing surrogate models. Yet, data‐driven modelling of antenna characteristics is largely hindered by the curse of dimensionality. This may be addressed using the recently reported domain‐confinement...
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Cu-Doped Layered Double Hydroxide Constructs the Performance-Enhanced Supercapacitor Via Band Gap Reduction and Defect Triggering
PublikacjaLayered double hydroxides (LDHs) are regarded as the excellent electrode materials for supercapacitors because of their high theoretical capacitance and abundance. However, the poor conductivity and limited reaction kinetics of LDHs restrict their practical application severely. Herein, Cu is chosen from groups VIII/IB/IIB as dopants for Co-based LDH (CuCo-LDH). The designed metal–organic framework-derived hierarchical CuCo-LDH...
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A novel method for vibration surveillance during high speed ball end milling of flexible details
PublikacjaPraca dotyczy nadzorowania drgań podczas obróbki zakrzywionych przedmiotów podatnych frezem kulistym, z uwzględnieniem zgodności parametrów modelu modalnego. Przedstawiono analizę dynamiki niestacjonarnego okładu drgającego, z którego wydzielono podukład modalny, strukturalny i łączący. Zastosowano minimalizację poziomu drgań z dopasowaniem prędkości obrotowej wrzeciona do optymalnego kąta przesunięcia fazowego. Eksperymenty doświadczalne...
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A novel method for vibration surveillance during high speed ball end milling of flexible details
PublikacjaPraca dotyczy nadzorowania drgań układów niestacjonarnych modelowanych metodą elementów skończonych. Obróbka frezem kulistym przedmiotów podatnych jest często stosowana w przypadku nowoczesnych centrów obróbkowych. Drgania względne narzędzie-przedmiot obrabiany mogą doprowadzić do utraty stabilności i powstania drgań samowzbudnych typu chatter. W pracy proponuje się metodę minimalizacji poziomu drgań poprzez dopasowanie prędkości...
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Effect of Metal and Carbon Nanotube Additives on the Thermal Diffusivity of a Silica Gel-Based Adsorption Bed
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Implementation of Fluidized Bed Concept to Improve Heat Transfer in Ecological Adsorption Cooling and Desalination Systems
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Towards enhanced heat and mass exchange in adsorption systems: The role of AutoML and fluidized bed innovations
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SURFACE TEXTURE ANALYSIS AFTER BALL END MILLING WITH VARIOUS SURFACE INCLINATION OF HARDENED STEEL
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Optimisation of machining parameters during ball end milling of hardened steel with various surface inclinations
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RECODIS: Resilient Communication Services Protecting End-user Applications from Disaster-based Failures
PublikacjaDisaster-based failures can seriously disrupt any communication network, making its services unavailable. Such disruptions may be caused by natural disasters, technology-related failures, or malicious attacks, and they are observably increasing in number, intensity and scale. When network services that are a part of critical infrastructure become unavailable, commercial and/or societal problems are inevitable. The issue of limiting...
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Optimal spindle speed determination for vibration reduction during ball-end milling of flexible details
PublikacjaIn the paper a method of optimal spindle speed determination for vibration reduction during ball-end milling of flexible details is proposed. In order to reduce vibration level, an original procedure of the spindle speed optimisation, based on the Liao–Young criterion, is suggested. As the result, an optimal, constant spindle speed value is determined. For this purpose, on-stationary computational model of machining process is...
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Instrumented End Notched Flexure - Crack propagation and process zonemonitoring. Part I: Modelling and analysis
PublikacjaAnalysis of the three-point bending, End Notched Flexure (ENF), test is presented for exploitation with a new experimental methodology using the backface strain monitoring technique. The model consists oftwo Timoshenko beams joined with a two parameter elastic foundation, to evaluate stress and strain fields in both adherends and the adhesive layer, together with the specimen compliance and energyrelease rate. This model is compared...
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Methodology for assessing end-user requirements in the Ella4Life project: elders’ perspectives about self-monitoring
PublikacjaThe purpose of this paper is to explore elders’ perspectives about self-monitoring and using specially developed sensor technology for measuring health indicators. The qualitative research method is focus-groups with guidelines that were designed for understanding elder’s requirements about monitoring health indicators. We present them two devices: the first sensor is a device for monitoring of cardiac action potential fixed into...
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A New Approach to the PWM Modulation for the Multiphase Matrix Converters Supplying Loads with Open-End Winding.
PublikacjaThis article presents three variants of the Pulse Width Modulation (PWM) for the Double Square Multiphase type Conventional Matrix Converters (DSM-CMC) supplying loads with the open-end winding. The first variant of PWM offers the ability to obtain zero value of the common-mode voltage at the load's terminals and applies only six switches within the modulation period. The second proposal archives for less Total Harmonic Distortion...
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End-of-life management of single-use baby diapers: Analysis of technical, health and environment aspects
PublikacjaSingle-use baby diapers belongs to an important group of products used in the parenting journey because of their high performance and convenience. Single-use baby diapers are normally thrown away after one-time use, resulting in a waste management problem. The goal of this paper was to better understand main environmental concerns of different types of diapers and address how to reduce them, with a special consideration of waste...
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Mechanical Performance and Environmental Assessment of Sustainable Concrete Reinforced with Recycled End-of-Life Tyre Fibres
PublikacjaThe presented research’s main objective was to develop the solution to the global problem of using steel waste obtained during rubber recovery during the tire recycling. A detailed comparative analysis of mechanical and physical features of the concrete composite with the addition of recycled steel fibres (RSF) in relation to the steel fibre concrete commonly used for industrial floors was conducted. A study was carried out using...
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Nitrogen removal in vertical flow constructed wetlands: influence of bed depth and high nitrogen loadings
PublikacjaThe aim of the study was to evaluate the nitrogen removal and its effects on the plant’s growth and leaves morphology. using two subsurface vertical flow (VF bed), with different depths (0.24 m2 × 0.70 m; 0.24 m2 × 0.35 m) and nitrogen load increments. The VF bed were planted with Vetiveria zizanioides, filled with light expanded clay aggregates (Leca®NR 10/20) and fed in parallel mode with synthetic wastewater. High ammonium nitrogen...
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Fatigue of titanium alloy Ti6Al4V with diamond structure obtained by Laser Power Bed Fusion method
PublikacjaThis paper presents the results of fatigue tests conducted on Ti6Al4V titanium alloy with diamond structure obtained by the Laser Power Bed Fusion method. Samples used in tests were printed with porosities: 81%, 73%, 50%, 34% and near-zero porosity. Samples were subjected to cyclic tests with a constant stress amplitude. The number of cycles until sample failure was registered. Obtained fatigue test results made it possible to...
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Enhancing the bioconversion rate and end products of black soldier fly (BSF) treatment – A comprehensive review
PublikacjaFood security remains a pressing concern in the face of an increasing world population and environmental challenges. As climate change, biodiversity loss, and water scarcity continue to impact agricultural productivity, traditional livestock farming faces limitations in meeting the growing global demand for meat and dairy products. In this context, black soldier fly larvae (BSFL) have emerged as a promising alternative for sustainable...
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Reduction of vibration level by the spindle speed optimisation during ball end milling of flexible details
PublikacjaPraca dotyczy nadzorowania drgań podczas skrawania przedmiotów podatnych frezem kulistym. Przedsatwiono wspomaganą komputerowo procedurę nadzorowania z optymalizacją prędkości obrotowej narzędzia. Przy modelowaniu wykorzystano niestacjonarny model obliczeniowy. Rezultatem modelowania jest układ hybrydowy, w którym oddzielono podukłady: modalny, łączący i strukturalny. Metoda wymaga identyfikacji częstości własnych co może być wykonane...
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Inhibitor kinazy Brutona u chorych z nawrotowym lub opornym na leczenie chłoniakiem z komórek płaszcza – wyniki międzynarodowego, wieloośrodkowego, badania II fazy z ibrutynibem (PCI-32765) – EHA Encore
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