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Applications of sample preparation techniques in the analysis of pesticides and PCBS in food
PublikacjaPestycydy oraz anality z grupy polichlorowanych bifenyli (PCB), można znaleźć w żywności w niewielkich stężeniach, jednak ich zdolność do kumulacji i toksyczność powodują konieczność oznaczanie tych związków w żywności. Analiza próbek żywności pod kątem obecności pestycydów i analitów z grupy PCB przysparza wiele trudności ze względu na specyfikę przygotowania próbki w oparciu o wieloetapowe operacje oczyszczania próbki zawierającej...
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Improving quality of life in automotive by professional preparation to external audits
PublikacjaZaproponowano podniesienie jakości procesów zarządzania w przemyśle samochodowym w oparciu o rozbudowany model profesjonalnego przygotowania i późniejszego wykorzystania wyników zewnętrznych audytów.
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Use of Ginger Nanofibers for the Preparation of Cellulose Nanocomposites and Their Antimicrobial Activities
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Exploiting isohexide scaffolds for the preparation of chiral ionic liquids tweezers
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AN ORIGINAL APPROACH IN THE FIELD OF PREPARATION REFERENCE MATERIALS OF VOLATILE ANALYTES
PublikacjaStandard gas mixtures (SGM) are indispensable reference materials for ensuring the reliability of analytical work. Reference materials are an excellent tool for the quality control and assurance of analytical results. Standard gas mixtures are unique among reference materials. The rapid progress of SGM production is connected with the instability of gaseous analytes which make them difficult to obtain. The use of standards with...
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Sample preparation techniques for determination of pesticide residues in food samples
PublikacjaPesticides are very important in increasing the efficiency and quality of agricultural production. They are applied in many spheres of life, not only in agriculture, and their applications are expanding. Despite their numerous merits, pesticides are some of the most toxic substances contaminating our environment and have a negative impact on the human health. Properties of pesticides such as stability, ability to bioaccumulation...
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Preparation and physicochemical characterization of ceramic supports for supported liquid membranes
PublikacjaImmobilizowane membrany ciekłe stały się przedmiotem intensywnych badań w ostanich latach, głównie w procesach oczyszczania strumieni gazowych. Kluczowym czynnikiem mającym wpływ na efektywność tych procesów ma czas życia układu membranowego, a zatem odpowiedni dobór nośnika i fazy membranowej. W porównaniu do nośników polimerowych, ceramiczne charakteryzują się większą grubością, jednak są bardziej stabilne termicznie. Praca...
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Preparation of the porous biomaterial based on titanium alloy for orthopaedic implants
PublikacjaObecnie tytan i jego stopy (Ti-6Al-4V lub Ti-13Nb-13Zr) są szeroko stosowane jako biomateriały dla implantów ortopedycznych. Stale prowadzone są badania nad ich najlepszą odpornością na korozję i zużycie ścierne oraz biozgodnością i bioaktywnością. Obecne badania również skoncentrowane są na projektowaniu, wytwarzaniu i właściwościach materiałów porowatych na podstawie na przykład stopu tytanu (Ti-13Nb-13Zr), które mogą być stosowane...
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New analytical sample preparation techniques in food flavour analysis
PublikacjaIn this chapter sample preparation techniques were broadly characterized and their applications in field of food analysis were presented. Usefulness of three extraction methods: SPME, SAFE and SDE for isolation of aroma compounds from complex food matrices was compared. Additionally, requirements for sample preparation methods using in food flavour analysis were detailed.
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Microwave-assisted preparation of potato starch silicated with silicic acid
PublikacjaApplication of microwave irradiation for the silication of granular potato starch with silicic acid, and the properties of silicated starch were investigated. Potato starch was esterified on 20 min microwave irradiation of starch with silicic acid, applying the power of 450 or 800Wand, for comparison, on 120 min convectional heating of the reagent blend at 100 ◦C. The degree of esterification and the reaction efficiency did not...
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Optimization of 1,2-Diaminopropane Preparation by the Ammonolysis of Waste 1,2-Dichloropropane
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Copolyester-coated mineral fertilizers – preparation, characterization, and nutrient release
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Sample preparation and chromatographic analysis of acidic herbicides in soils and sediments
PublikacjaW pracy przedstawiono różne techniki przygotowania próbek i oznaczania herbicydów z grupy pochodnych fenoli i pochodnych kwasów karboksylowych w próbkach gleby. Opisano wybrane metody wzbogacania i izolacji analitów, m. in.: ekstrakcję za pomocą wodnych roztworów zasad i rozpuszczalników organicznych płynem w stanie nadkrytycznym, wodą w stanie podkrytycznym, cieczą pod zwiększonym ciśnieniem, cieczą wspomaganą mikrofalami. Niski...
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Use of Ginger Nanofibers for the Preparation of Cellulose Nanocomposites and Their Antimicrobial Activities
PublikacjaHere, we report, for the first time, the isolation of ginger nanofibers (GNF) from ginger rhizomes spent by acid hydrolysis and followed by high-pressure homogenization. Scanning electron microscopy was utilized to identify the surface morphology of the GNF and the widths ranged between 130 to 200 nm. Structural analysis of GNF was identified by Fourier transform infrared spectroscopy, Differential scanning calorimetry, and X-ray...
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Surfactants application in sample preparation techniques: Insights, trends, and perspectives
PublikacjaSince the implementation of Green Chemistry into analytical practice, significant efforts have been made to improve the sustainability of chemical analysis. These include reducing the use of hazardous chemicals and solvents, minimizing waste, and improving energy efficiency. Surfactants can be applied in chemical analysis as an environmentally friendly alternative to conventional solvents and chemicals. The use of surfactants can...
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Preparation and Characterization of Films Based on Disintegrated Bacterial Cellulose and Montmorillonite
PublikacjaThe food packaging materials from natural polymers including polysaccharides offer an ecologically important alternative to commonly used synthetic, non-biodegradable counterparts. The purpose of this work was to modify of bacterial cellulose (BC) leading to the improvement of its functional properties in terms of use as a food packaging material. Effects of disintegration of BC and addition of montmorillonite (MMT) on its water...
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Preparation of Well-Compatibilized PP/PC Blends and Foams Thereof
PublikacjaThe performance of polypropylene-poly(ethylene brassylate) block and graft copolymers and a polypropylene-polycaprolactone graft copolymer as compatibilizers for polypropylene-rich polypropylene/bisphenol A polycarbonate (PP/PC, 80/20 wt/wt) blends was elucidated. The copolymers were synthesized either by metal-catalyzed ring-opening polymerization or transesterification of a presynthesized polyester, initiated by hydroxyl-functionalized...
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Manganese Phosphatizing Coatings: The Effects of Preparation Conditions on Surface Properties
PublikacjaManganese phosphate coating could be used to protect the surface of steel products. However, it is essential to determine the effects which process parameters, as well as the types of additives used, have on the efficiency of coating deposition. Thus, we present here a process of phosphatization of low-alloy steel (for 15 min at 95 ◦C) in manganese/nickel baths followed by a passivation process with the use of a silicon and zircon...
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Preparation and characterization of biodegradable and compostable PLA/TPS/ESO compositions
PublikacjaIn this study, biodegradable and compostable compositions, derived from totally natural feedstock/raw materials, namely polylactide (PLA), potato thermoplastic starch (TPS) and plant glycerin have been made by melt extrusion with epoxydized soybean oil (ESO) as reactive modifier in order to improve PLAs ductility and reduce the products cost without compromising biodegradation. The obtained PLA/mTPS(0,5ESO)[75/25] and PLA/ mTPS(2ESO)[75/25]...
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Sample preparation and recent trends in volatolomics for diagnosing gastrointestinal diseases
PublikacjaThe analysis of the human volatilome can be successfully used for rapid and non-invasive diagnostics of gastrointestinal diseases. However, the introduction of techniques based on detection of volatiles is limited, among other factors, by difficulties which arise during the sampling stage and instrumental analysis. The aim of this article was to review and discuss medical and analytical literature on the analysis of volatiles in...
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Convenient and Efficient Diastereoselective Preparation of Functionalized Z -Alkenyl Sulfides
PublikacjaWe have developed an efficient and convenient regio‐ and stereoselective reduction of the alkynyl sulfides with pinacolborane in the presence of copper(I) chloride to produce (Z)‐alkenyl sulfides in good and very good yields. The functionalized alkynyl sulfides are readily available based on the reaction of lithium acetylides with thiotosylates under mild conditions.
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Alternative Methods of Preparation of Soluble Keratin from Chicken Feathers
PublikacjaHuge amount of keratinous waste, especially birds’ feathers, demands more value-added application instead of dumping. The present work reports the results of experiments aimed at preparing soluble keratin useful for novel bioproduct formation. The effect of thermo-chemical treatments with various reducing agents, i.e. 2-mercaptoethanol, dithiothreitol, sodium m-bisulphite, and sodium bisulphite, as well as sodium hydroxide, on...
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Preparation and photocatalytic activity of iron-modified titanium dioxide photocatalysts
PublikacjaTiO2 modyfikowany żelazem otrzymano dwiema metodami: metodą zol-żel oraz metodą impregnacji powierzchniowej. Fotokatalizatory kalcynowano w temperaturze 400C. Jako matrycę TiO2 zastosowano komercyjnie dostępne proszki ditlenku tytanu: P25 (Evonik, Niemcy, 50m2/g) oraz ST-01 (Ishihara Sangyo, Japonia, 300m2/g). Charakterystyka otrzymanych fotokatalizatorów obejmowała wyznaczenie właściwości absorpcyjnych, powierzchni właściwej BET...
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Preparation of nano-tubular oxide layers on titanium alloy Ti13Nb13Zr
PublikacjaThe article presents results of oxidation tests and corrosion investigations of titanium alloy Ti13Nb13Zr preformed at different conditions. The oxide layers have been formed using electrochemical method in 2M H3PO4 + 0,3% HF solution for 30 min. and 1h at 20V constant voltage. The corrosion tests heve been made with poteniodynamic method in Ringer's solution at pH ranged 3 and 7. It has been shown that the nano-oxide films, which...
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Group 11 complexes with a phosphanylphosphaalkene ligand: preparation and stability study
PublikacjaThe reactivities of two selected phosphanylphosphaalkenes, Ph2C=P-PtBu2 (1a) and (p-MeO-Ph)2C=P-PtBu2 (1b), toward CuCl, AgCl and (tht)AuCl (tht = tetrahydrothiophene) were investigated. As a result, new phosphanylphosphaalkene dimeric and monomeric complexes were formed (Cu and Ag dimeric and Au monomeric). All obtained products were air and moisture stable and light insensitive.
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