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Search results for: ELECTROCATALYTIC GAS SENSOR
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Development of gas chromatography - tandem mass spectrometry procedure for development of pesticide residues in honey and honeybee samples
PublicationA new analytical procedure of determination of multiresidue of pesticides based on application of the modified QuEChERS approach at the step of sample preparation and technique GC-MS/MS has been developed and applied for studies the real honey and honeybee samples. Samples were collected from northern Poland (Pomerania). The proposed procedure enables for the determination of 34 and 30 pesticides residues respectively on honey...
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Efficiency of Electricity Production Technology from Post-Process Gas Heat: Ecological, Economic and Social Benefits
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A comprehensive review of sectorial contribution towards greenhouse gas emissions and progress in carbon capture and storage in Pakistan
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Effects of Heat and Momentum Gain Differentiation during Gas Detonation Spraying of FeAl Powder Particles into the Water
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Thermal analysis of macro-encapsulated phase change material coupled with domestic gas heater for building heating
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Using the MultiRAEPro Gas Detector to Monitor Odour Emissions from Biogas Plants Processing Municipal Waste
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Utilization of thermal decomposition of immobilized compounds for the generation of gaseous standard mixtures used in the calibration of gas analysers
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Study of a method for the preparation of standard gas mixtures based on thermal decomposition of surface compounds. Application to isothiocyanates
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Identification of organic acids as potential biomarkers in the urine of autistic children using gas chromatography/mass spectrometry
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Direct Screening ofWater Samples for Benzene Hydrocarbon Compounds by Headspace Liquid-Phase Microextraction--Gas Chromatography
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Direct screening of ground water samples for fuel oxygenates by headspace liquid phase microextraction–gas chromatography
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Application of single drop extraxtion (SDE) gas chromatography method for the determination of carbonyl compounds in spirits and vodkas
PublicationW pracy przedstawiono metodę oznaczania związków karbonylowych w spirytusach i wódkach, wykorzystującą do izolacji i wzbogacania technikę mikroekstrakcji do pojedynczej kropli (SDE)po derywatyzacji analitów O-(2,3,4,5,6-pentafluorobenzylo)hydroksylaminą. Określono optymalne parametry izolacji i wzbogacania aldehydów z roztworów alkoholowych (objętość próbki, objętość kropli, zawartość alkoholu, temperaturę i czas ekstrakcji)....
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Environmental aspects of using gas chromatography for determination of pharmaceutical residues in samples characterized by different composition of the matrix
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Ammonia in Fly Ashes from Flue Gas Denitrification Process and its Impact on the Properties of Cement Composites
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Use of pyrolysis and gas chromatography for the determination of acrylic acid concentration in acrylic copolymers containing carboxylic groups
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Precise Evaluation of Gas–Liquid Two-Phase Flow Pattern in a Narrow Rectangular Channel with Stereology Method
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The use of gas chromatography combined with chemical and sensory analysis to evaluate nuisance odours in the air and water environment
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The application of checklists in the field of complex operation based on the operating experiences of a liquefied petroleum gas handling simulator.
PublicationOmówiono pojęcie list sprawdzających (z ang. checklists). Podano charakterystykę techniczną symulatora operacji ładunkowych gazowca typu LPG znajdującego się w laboratorium Katedry Siłowni Okrętowych Akademii Morskiej w Gdyni wraz z jego możliwościami dydaktycznymi. Przedstawiono zasady tworzenia list sprawdzających czynności obsługowe wraz z przykładem takiej listy.
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Parameter of nonlinearity B/A of three-component systems with separate volumes of liquid, its vapor and a neutral gas
PublicationOtrzymane zostało wyrażenie dla zaburzenia entropii substancji o trzech komponentach jako funkcja zaburzeń jej ciśnienia i gęstości. Na podstawie wzoru prędkość i parametru nieliniowosci fali akustycznej zostały wyliczone jako funkcje i ciśnienia i koncentracji pary i powietrza. Rezultaty są przedstawione w postaci wykresów.
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Gas chromatographic determination of volatile aliphatic and selected aromatic amines, without derivatization: solid phase microextraction
PublicationW pracy opisano wykorzystanie techniki chromatografii gazowej do oznaczania śladowych stężeń lotnych amin alifatycznych i wybranych amin aromatycznych w próbkach o różnym składzie matrycy. W tym przypadku aminy nie podlegają procesowi derywatyzacji przed etapem końcowym a na etapie pobierania próbek analitów jest wykorzystana technika mikroekstrakcji do fazy stacjonarnej (SPME).
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MATCHED FILTER APPROACH FOR MICROSEISMIC SIGNAL PROCESSING OF REAL DATA FROM EAST POMERANIA SHALE GAS
PublicationThe microseismic monitoring is a method of monitoring of fracture propagation during hydraulic fracturing (HF)process. An array of several hundred geophones is placed on the surface to record little ground tremors induced by fracturing process. Filtration and summation of signals from geophones is essential to identify and locate fracturing events from underground. Authors propose a method of matched filtering, that is usually...
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Effect of gas content in macropores on hydraulic fracturing in rocks using a fully coupled DEM/CFD approach
PublicationW pracy skupiono się na wpływie zawartości gazu w makroporach skał na proces szczelinowania hydraulicznego. Proces został zasymulowany przez połączenie metody elementów dyskretnych (DEM) z obliczeniową dynamiką płynów (CFD) w ramach dwuwymiarowych (2D) warunków izotermicznych. Mechaniczne zachowanie skały zostało zasymulowane za pomocą DEM, a CFD została wykorzystana do opisu zachowanie przepływu laminarnego, dwufazowego płynu...
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Body Sensor Networks
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The presence of polycyclic aromatic hydrocarbons in disposable baby diapers: A facile determination method via salting-out assisted liquid-liquid extraction coupled with gas chromatography-mass spectrometry
PublicationIn this paper we demonstrate the development of the extraction procedure of polycyclic aromatic hy- drocarbons from baby diapers along with their quantification by gas chromatography-mass spectrometry. Apart from covering plastic foil, disposable baby diapers contain sorbents intended to absorb urine and feces. A hygroscopic, adsorptive, and tough-to-homogenize fibrous sorbent, represents an analytical chal- lenge to analytical...
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An odor-sensing system - powerful technique for foodstuff studies
PublicationThis work examines gas sensor array technology combined with multivariate data processing methods and demonstrates a promising potential for rapid, non-destructive analysis of food. Main attention is focused on detailed description of sensor used in e-nose instruments, construction, and principle of operation of these systems. Moreover, this paper briefly reviews the progress in the field of artificial olfaction and future trends...
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A Novel Electrochemical Sensor Based on Graphene Oxide Nanosheets and Ionic Liquid Binder for Differential Pulse Voltammetric Determination of Droxidopa in Pharmaceutical and Urine Samples
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Jacek Stefański prof. dr hab. inż.
PeopleJJacek Stefański received M.Sc., Ph.D. and D.Sc. degrees in telecommunications engineering from Gdansk University of Technology (GUT), Poland, in 1993, 2000 and 2012, respectively. Awarded title of Professor by the President of Poland in 2020. Currently, he works as a professor at the Department of Radio Communication Systems and Networks (DRCSN) in GUT. From 2005 to 2009, he worked as an assistant professor in the National Institute...
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FTIR spectra of gas mixtures from the process of biogas dry reforming using Al2O3/5%Cu catalyst
Open Research DataThe dataset contains the FTIR spectra collected during the catalytic measurements of dry reforming of biogas (60/40 CH4-CO2) using AlOOH/1%Cu nanocatalyst. The specatra were collected every 1 minute from 800C to 500C. Reagent flow was set to 20ml/min.
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FTIR spectra of gas mixtures from the process of biogas dry reforming using CeO2/5%Cu catalyst
Open Research DataThe dataset contains the FTIR spectra collected during the catalytic measurements of dry reforming of biogas (60/40 CH4-CO2) using CeO2/5%Cu nanocatalyst. The specatra were collected every 1 minute from 800C to 500C. Reagent flow was set to 20ml/min.
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FTIR spectra of gas mixtures from the process of biogas dry reforming using Al2O3/5%Cu catalyst
Open Research DataThe dataset contains the FTIR spectra collected during the catalytic measurements of dry reforming of biogas (60/40 CH4-CO2) using Al2O3 (TMDAR)/5%Cu nanocatalyst. The specatra were collected every 1 minute from 800C to 500C. Reagent flow was set to 20ml/min.
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Simulation of the weight averaging of pulse frequency modulated sensor output signal
Open Research DataThe aim of the research is investigation of the efficiency of weight averaging of pulse frequency modulated signal. It was shown that from the point of view of the reduction of the sampling error the best are polynomial weighing functions, for which the maximum of this component error decreases proportionally to the appropriate power of the number of...
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International Frequency Sensor Association Publishing
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A probabilistic concept of assessment of amount of noxious substances contained in exhaust gas emitted from self-ignition engines
PublicationPrzedstawiono probabilistyczną koncepcję oceny toksyczności spalin silników o zapłonie samoczynnym. Ocena taka jest istotna, ponieważ bez niej nie jest możliwe określenie walorów proekologicznych różnych środków transportowych z napędem spalinowym, w tym śródlądowych statków pasażerskich. W koncepcji tej uwzględniony został model procesu rozruchu silników o zapłonie samoczynnym. Model ten przedstawiono w formie procesu semimarkowskiego,...
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Comprehensive two-dimensional gas chromatography and three-dimensional fluorometry for detection of volatile and bioactive substances in some berries
PublicationThe volatilefractionsofCapegooseberryandblueberryweredeterminedbyheadspacesolid-phase microextractioncoupledwithcomprehensivetwo-dimensionalgaschromatographywithtime-of-flight mass spectrometry(HS-SPME/GCGC-TOFMS).Thehighestamountofalcohol(51.8%),ester(32.8%)and carboxylicacid(6.9%)wasinblueberryincomparisonwithgooseberryandoppositelyketones(14.7%), aldehydes(9.9%)andterpenes(8%)werefoundingooseberry.Thebioactivecompoundsandantioxidant capacities...
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Application of dispersive liquid-liquid microextraction for the determination of selected organochlorine pesticides in honey by gas chromatography - mass spectrometry
PublicationDispersive liquid-liquid microextraction (DLLME) is a rapid and easy technique that consumes minute amounts of organic solvents. In this work, we present chemometric study on optimization of DLLME parameters for the extraction of aldrin, endrin, lindane, alfa-endosulfan, 4,4'-DDT and its metabolites from honey matrix. Method quantification limits (MQLs) vary between 0.3 ng/g for 2,4'-DDE and 4,4'-DDE to 13.2 ng/g for alfa-endosulfan...
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Salt saturated single-drop microextraction of malondialdehyde from human plasma before its determination by gas chromatography
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Enantioselective comprehensive two-dimensional gas chromatography. A route to elucidate the authenticity and origin ofRosa damascena Milleressential oils
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Extraction of mass spectra free of background and neighboring component contributions from gas chromatography/mass spectrometry data
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Examination of the influence of macro and microscopic parameters of limestone on the effectiveness of gas phase desulphurisation according to the method of wet limestone
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Rapid and sensitive determination of fluoride in toothpaste and water samples using headspace single drop microextraction-gas chromatography
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Application of normal-phase high-performance liquid chromatography followed by gas chromatography for analytics of diesel fuel additives
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LABORATORY STUDY ON INFLUENCE OF AIR DUCT THROTTLING ON EXHAUST GAS COMPOSITION IN MARINE FOUR-STROKE DIESEL ENGINE
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A new silylation reagent dimethyl(3,3,3-trifluoropropyl)silyldiethylamine for the analysis of estrogenic compounds by gas chromatography–mass spectrometry
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Determination of twenty pharmaceutical contaminants in soil using ultrasound-assisted extraction with gas chromatography-mass spectrometric detection
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The Problem of Wastewater in Shale Gas Exploitation The Influence of Fracturing Flowback Water on Activated Sludge at a Wastewater Treatment Plant
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Possibility of NOx emission reduction from combustion process using sewage sludge gasification gas as an additional fuel
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Headspace Solid-Phase Microextraction Coupled with Gas Chromatography–Mass Spectrometry for the Determination of Volatile Organic Compounds in Urine
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Thin layer headspace gas chromatography for biological monitoring of persons exposed to volatile organohalogen compounds from water
PublicationCelem pracy było zbadanie możliwości wykorzystania analizy fazy nadpowierzchniowej nad cienką warstwą cieczy z samoczynną generacją ciekłego sorbentu (TLHS)do izolacji i wzbogacania THM w próbkach moczu i krwi ludzkiej. Umożliwiło to następnie wykorzystanie prostej techniki bezpośredniego nastrzyku próbki do kolumny chromatografu gazowego, wyposażonego w detektor wychwytu elektronów (DAI-GC-ECD).Przy pomocy tak opracowanej metody...
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Gas hold up and time dependent slurry viscosity during the the precipitation of fine grained silicon dioxide particles.
PublicationBadano zmiany stopnia zatrzymania gazu i lepkości zawiesiny podczas precypitacji dwutlenku krzemu z krzemianu sodowego za pomocą dwutlenku w reaktorze airlift z wewnętrzną cyrkulacją. Badano wpływ parametrów procesowych na akumulację mikropęcherzy w zawiesinie.
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Modelling of high temperature air/steam gasification of biomassand solid wastes in view of hydrogen-rich gas production
PublicationPrzedstawiono zaawansowane technologie produkcji gazu bogatego w wodór z biomasy i odpadów komunalnych. Przeprowadzono badania eksperymentalne na stanowisku pomiarowym wykonanym w skali półprzemysłowej. Otrzymano obiecujące rezultaty podczas zgazowania palet drewnianych gazem o różnej zawartości pary wodnej.