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Wyniki wyszukiwania dla: liquid metals and alloys
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Fermi-liquid behavior of binary intermetallic compounds Y3 M (M = Co, Ni, Rh, Pd, Ir, Pt)
PublikacjaA series of polycrystalline samples of Y3 M (M = Co, Ni, Rh, Pd, Ir, Pt), intermetallic binary compounds were synthesized by the arc-melting method. Powder x-ray diffraction (pXRD) confirmed the orthorhombic cementite-type crystal structure and allowed for the estimation of the lattice parameters. Physical properties were investigated by means of electrical resistivity and heat capacity measurements between 1.9 K and 300 K. All...
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Facile formation of self-organized TiO2 nanotubes in electrolyte containing ionic liquid - ethylammonium nitrate and their remarkable photocatalytic properties
PublikacjaThe oriented TiO2 nanotube arrays (NTs) are identified as a stable, active and recyclable photocatalytic surface. However, their photoactivity is strictly depended on morphology (especially length), which could be controlled by anodic oxidation parameters, including electrolyte properties. To control the morphology, were successfully synthesized a series of NTs by a novel approach where ionic liquid (IL), ethylammonium nitrate...
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Influence of surface topography on RBS measurements: case studies of (Cu/Fe/Pd) multilayers and FePdCu alloys nanopatterned by self-assembly
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Determination of nine high-intensity sweeteners in various foods by high-performance liquid chromatography with mass spectrometric detection
PublikacjaAn analytical procedure involving solid-phase extraction (SPE) and high-performance liquid chromatography-mass spectrometry has been developed for the determination of nine high-intensity sweeteners authorised in the EU; acesulfame-K (ACS-K), aspartame (ASP), alitame (ALI), cyclamate (CYC), dulcin (DUL), neohesperidin dihydrochalcone (NHDC), neotame (NEO), saccharin (SAC) and sucralose (SCL) in a variety of food samples (i.e. beverages,...
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Silicon occurrence, uptake, transport and mechanisms of heavy metals, minerals and salinity enhanced tolerance in plants with future prospects: A review
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Heavy metals in lake surface sediments in protected areas in Poland: concentration, pollution, ecological risk, sources and spatial distribution
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Identification and characterization of the Indian Yellow dyestuff and its degradation products in historical oil paint tube by liquid chromatography mass spectrometry
PublikacjaAn analytical protocol for identification of dyes using reversed phase liquid chromatography-mass spectrometry with atmospheric pressure electrospray ionization (LC-ESI/MS) is presented. The developed method has been successfully applied in identification of euxanthic acid and euxanthone, the main components of the Indian Yellow dye in a historical oil paint tube produced by Richard Ain`es, a recognizable French company supplying...
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Determination of phenylbutazone, sulfamethazine, carbendazim and linuron using a novel pine bark biosorbent for solid-phase extraction (SPE) with high-performance liquid chromatography (HPLC)
PublikacjaThe paper presents a novel pine bark based biosorbent for solid-phase extraction (SPE). The morphology and composition of the pine bark were characterized using Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM). The biosorbent was used for the preparation of wastewater for the determination of phenylbutazone, sulfamethazine, carbendazim, and linuron by high performance liquid chromatography with...
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Optimization of vortex-assisted hydrophobic magnetic deep eutectic solvent-based dispersive liquid phase microextraction for quantification of niclosamide in real samples
PublikacjaIn this manuscript, a green and fast vortex-assisted hydrophobic magnetic deep eutectic solvent-based dispersive liquid phase microextraction (VA-HMDES-DLPME) method was developed for the selective extraction and determination of niclosamide in read samples, including rice, medicine tablets, and water samples. Here, hydrophobic magnetic deep eutectic solvents were used as the extracting solvent without requiring any centrifugation...
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Simultaneous Determination of Indolic Compounds in Plant Extracts by Solid-Phase Extraction and High-Performance Liquid Chromatography with UV and Fluorescence Detection
PublikacjaA high-performance liquid chromatographic method with UV and fluorescence detection (HPLC-DAD-FLD) was developed for simultaneous determination of indolic compounds in plant material. Indole-3-carbinol (I3C), indole-3-acetic acid (I3AA), indole-3-acetonitrile (I3ACN), and 3,3′-diindolylmethane (DIM) were used as representative compounds that cover a wide spectrum of indole structures occurring in nature. For concentration and purification...
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Comparison of classical and modern approach of determination of highly polar compounds by High Performance Liquid Chromatography coupled with Tandem Mass Spectrometry
PublikacjaAbstract: Sugars and sugar alcohols are known as highly polar compounds. Four analytes were taken into consideration for comparison of classical and modern approach of separation of highly polar substances. Mannitol was chosen as an example of simple sugar alcohol, sucrose and lactulose as examples of disaccharides and structural isomers, raffinose as an example of complex trisaccharide. Raffinose was also used as internal standard...
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Micellar liquid chromatography for lipophilicity determination of new biologically active 1,3‐purinodiones
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Chromatographic behaviour of ionic liquid cations in view of quantitative structure-retention relationship
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Influence of rotating magnetic field on gas-liquid volumetric mass transfer coefficient
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Headspace liquid phase microextraction for quantitation of hexanal in potato crisps by gas chromatography
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Gas to liquid mass transfer in mixing system with application of rotating magnetic field
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Modular Ceramic-Polymeric Device for Analysis of Selected Elements in Liquid Using Microplasma
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Review of the applicability of ionic liquid matrices for the quantification of small molecules by MALDI MS
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About nutrient liquid flow between potential flow and cartilage surface in bioreactor
PublikacjaW niniejszej pracy wyznaczony został przepływ cieczy odżywczej o właściwościach nienewtonowskich w cienkiej warstwie granicznej w pobliżu powierzchni komórek chrząstki (chondrocytu) podczas hodowli w bioreaktorze. Ruch cieczy w warstwie granicznej jest wywołany wydatkiem przepływu dostarczanej cieczy do bioreaktora. Ponadto prędkość przepływu cieczy w warstwie granicznej wokół hodowanych komórek chrząstki stawowej jest uzależniona...
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Turbulent heat transfer in thin liquid films at low and high heat fluxes
PublikacjaW pracy przedstawiono rozważania turbulentnej wymiany ciepła w cienkich filmach cieczowych powstałych w wyniku uderzenia strugi przy małych i dużych strumieniach ciepła. W ostatnim przypadku może dojść do wrzenia filmu cieczowego. Oba zjawiska zamodelowano i uzyskano odpowiednie rozkłady temperatury i pedkosci.
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Experimental Determination of Limit Adhesive Shear Strtess between Solid Wall and Liquid
PublikacjaTheoretically slip of a fluid with respect to the solid wall should occur even at a very low velocity of motion. However theoretical analysisand some empirical data suggest that there must be a limit value of shear stress, below which the slip does not appear. A simple metyhod of this stress determination was proposed in the paper.
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Silicon polypodands: a new class of efficient solid–liquid phase-transfer catalysts
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Application of a new class B-podands in solid–liquid phase transfer catalysis
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A new type of B-podand catalysts for solid–liquid phase transfer reactions
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Deep Learning-Based, Multiclass Approach to Cancer Classification on Liquid Biopsy Data
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Kinetics of spinodal decomposition in the Ising model with dynamic lattice liquid (DLL) dynamics
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From the Dynamic Lattice Liquid Algorithm to the Dedicated Parallel Computer – mDLL Machine
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On the inappropriate fit of diffusion functions at thermal decomposition of some azomonoethers in liquid state
PublikacjaW celu analizy rozkładu termicznego tytułowych barwników azowych zastosowano mechanizmy D1, D2, D3 i D4. W wyniku przeprowadzonych badań stwierdzono, że rozkład zachodzi w fazie ciekłej, zaś w celu wyznaczenia parametrów aktywacji oraz wyznaczenia funkcji przemiany zastosowano koncepcje homo- i heterogeniczne.
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On the Mechanism of Coupled Transport of Cu(II) Ions Through Bulk Liquid Membranes.
PublikacjaTransport jonów Cu(II) przez ciekłe membrany za pomocą 5 - nonylosalicyloaldoksimu jako przenośnika wymaga obecności kompleksu o stosunku metalu do przenośnika 1:2. Zbadano dwie możliwości mechanizmu jego tworzenia. Roztrzygnięcie, który mechanizm jest prawidłowy nie jest możliwe w oparciu jedynie o kinteykę chemiczną.
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Balance of pesticides mass in gas, liquid and solid phase after their chemical degradation.
PublikacjaOpisano metodę usuwania pestycydów z wody przy zastosowaniu fotodegradacji (UV) i katalizatora (TiO2). Efektywność procesu usuwania pestycydów była kontrolowana przy zastosowaniu chromatografu gazowego z detektorem wychwytu elektronów. Oznaczano zawartość pestycydów w wodzie, a także zaadsorbowanych na powierzchni stałej, oraz w fazie gazowej. Największa zawartość pestycydów znajdowała się na fazie stałej, następnie w cieczy i...
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The utilization of sludge generated in coagulation of fish processing wastewater for liquid feed production
PublikacjaWykorzystano koagulację do wydzielenia ze ścieków z przemysłu rybnego białek i tłuszczów. Uzyskany osad pokoagulacyjny dodawano do produkcji rybnych hydrolizatów białkowych. Zmodyfikowano proces wytwarzania rybnych hydrolizatów z wykorzystaniem kwasów siarkowego (VI) oraz ortofosforowego (V).
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High resolution liquid chromatography and time of flight mass spectrometry in perfume analysis
PublikacjaPerfumes consist of a wide range of natural and synthetic compounds that belongs to different chemical classes. Most of these compounds are generally determined by GC. However, in this study RP-HPLC-Q-TOF-MS and HILIC-Q-TOF-MS technique was applied for the determination of ingredients of original perfumes and their imitations. Antioxidants and compounds specific to fragrances of animal \origin were found in original...
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The effect of imidazolium ionic liquid on the morphology of Pt nanoparticles deposited on the surface of SrTiO3 and photoactivity of Pt–SrTiO3 composite in the H2 generation reaction
PublikacjaPhotocatalytic water splitting has great potential in solar-hydrogen production as a low-cost and environmentally friendly method. Different unique techniques used to obtain photocatalysts with various modifications to improve H2 generation have been introduced. In the present work, SrTiO3 was successfully synthesized via the solvothermal method in the presence of ionic liquid (IL) - 1-butyl-3-methylimidazolium bromide ([BMIM][Br])...
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Differentiation of the concentration of heavy metals and persistent organic pollutants in lake sediments depending on the catchment management (Lake Gopło case study)
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Mocz jako źródło informacji o narażeniu zawodowym na metale = Urine as a source of information on occupational exposure to metals- a review
PublikacjaW pracy przedstawiono informacje na temat możliwości wykorzystywania próbek moczu ludzkiego jako materiału do badań analitycznych ukierunkowanych na uzyskanie informacji o narażeniu zawodowym na metale. Szczególną uwagę zwrócono na:-techniki izolacji i wzbogacania metali i ich metabolitów z próbek moczu,-techniki oznaczania metali w otrzymywanych ekstraktach,-zebranie informacji literaturowych odnośnie oznaczanych stężeń metali...
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Efficiency of ozonation process with calcium peroxide in removing heavy metals (Pb, Cu, Zn, Ni, Cd) from aqueous solutions
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Interactive assessment of lignite and bamboo-biochar for geochemical speciation, modulation and uptake of Cu and other heavy metals in the copper mine tailing
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Nowoczesne metody termochemicznej konwersji biomasy w paliwa gazowe, ciekłe i stałe = Modern methods of thermochemical biomass conversion into gas, liquid and solid fuels
PublikacjaBiomass utilization through direct- or co-combustion with coal, based on coal, hydrogen and oxygen compounds chemical energy conversion into heat in boilers, is simultaneously the cheapest and - according to experts - economically least effective solution. In case of heat and electricity production in cogeneration process in biomass fueled heat and power stations (wood, straw, energetic plants, RDF etc), investment costs are little...
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Photocatalytically Active TiO2/Ag2O Nanotube Arrays Interlaced with Silver Nanoparticles Obtained from the One-Step Anodic Oxidation of Ti–Ag Alloys
PublikacjaThe development of a photocatalyst with remarkable activity to degrade pollutants in aqueous and gas phase requires visible lightresponsive stable materials, easily organized in the form of a thin layer (to exclude the highly expensive separation step). In this work, we present a one-step strategy for synthesizing material in the form of a self-organized TiO2/Ag2O nanotube (NT) array interlaced with silver nanoparticles (as in a...
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Determination of eight artificial sweeteners and common Stevia rebaudiana glycosides in non-alcoholic and alcoholic beverages by reversed-phase liquid chromatography coupled with tandem mass spectrometry.
PublikacjaThe method for the determination of acesulfame-K, saccharine, cyclamate, aspartame, sucralose, alitame, neohesperidin dihydrochalcone, neotame and five common steviol glycosides (rebaudioside A, rebaudioside C, steviol, steviolbioside and stevioside) in soft and alcoholic beverages was developed using high-performance liquid chromatography and tandem mass spectrometry with electrospray ionisation (HPLC-ESI-MS/MS). To the best of...
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Effect of Processing Parameters on Strength and Corrosion Resistance of Friction Stir-Welded AA6082
PublikacjaThe friction stir welding method is increasingly attracting interest in the railway sector due to its environmental friendliness, low cost, and ease of producing high-quality joints. Using aluminum alloys reduces the weight of structures, increasing their payload and reducing fuel consumption and running costs. The following paper presents studies on the microstructure, strength, and corrosion resistance of AA6082 aluminum alloy...
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Recent theoretical and practical applications of micellar liquid chromatography (MLC) in pharmaceutical and biomedical analysis
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(Vapour + liquid) equilibrium in (n,n-dimethylacetamide + ethanol + water) at the temperature 313.15 K
PublikacjaW pracy prezentowane są pomiary całkowitej prężności pary dla tytułowego układu trójskładnikowego oraz dla składowych układów binarnych. Uzyskane w pracy wyniki porównane zostały z wcześniejszymi danymi dla podobnych układów. Znaleziono w przybliżeniu liniową zależność pomiędzy wartościami nadmiarowej entalpii swobodnej Gibbsa a objętością molową amidu, spełnianą w układach dwuskładnikowych: amid + alkohol alifatyczny.
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Polyfunctional chemically bonded stationary phase for reversed phase high-performance liquid chromatography
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Quantitative structure–retention relationships of ionic liquid cations in characterization of stationary phases for HPLC
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Liquid chromatography tandem mass spectrometry study of urinary nucleosides as potential cancer markers
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Suppression of deleterious effects of free silanols in liquid chromatography by imidazolium tetrafluoroborate ionic liquids
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Comparative study of surface topography of high performance liquid chromatography columns in terms of hydrophobicity
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Development of multilayer coatings for forming dies and tools of aluminium alloy from liquid state
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Headspace Liquid-Phase Microextraction of Chlorobenzenes in Soil with Gas Chromatography-Electron Capture Detection
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