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Wyniki wyszukiwania dla: experimental characterization
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Characterization of structural, thermal and mechanical properties of bismuth silicate glasses
Publikacjahe influence of heating and reduction processes on the structural, thermal and mechanical properties of bismuth-silicate glasses has been investigated. Two compositions of glasses: 40Bi2O3–60SiO2 (Bi0.57Si0.43Ox) and 27Bi2O3–73SiO2 (Bi0.43Si0.57Ox) were fabricated by a typical melt quenching technique. Then the reduction in hydrogen at 380 °C for 20, 42 or 67 h was performed. It was found that a 50 μm-thick layer was formed on...
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Synthesis and characterization of novel aliphatic polyurethanes for tissue engineering applications
PublikacjaSummarizing, in this thesis was described the synthesis of novel PUR system, which was obtained by using aliphatic diisocyanate (HDI), amorphous macrodiol (PEBA) and chain extender (BDO). This PUR system was established as suitable for TE purpose and successfully modified with AA, which as expected improved its biocompatibility. According to this, AA-modified HDI-based PURs is the PUR system ready for further studies including...
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Preparation and characterization of biodegradable and compostable PLA/TPS/ESO compositions
PublikacjaIn this study, biodegradable and compostable compositions, derived from totally natural feedstock/raw materials, namely polylactide (PLA), potato thermoplastic starch (TPS) and plant glycerin have been made by melt extrusion with epoxydized soybean oil (ESO) as reactive modifier in order to improve PLAs ductility and reduce the products cost without compromising biodegradation. The obtained PLA/mTPS(0,5ESO)[75/25] and PLA/ mTPS(2ESO)[75/25]...
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Identification and characterization of Staphylococcus spp. and their susceptibility to insect apolipophorin III
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Characterization of NiTi SMA in its unusual behaviour in wear tests
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Synthesis and characterization of ruthenium and rhenium dyes with phosphonate anchoring groups
PublikacjaRe(L1)–Re(L3), a series of rhenium(I) tricarbonyl chloride complexes with bpy-R2 derivatives L1–L3 (bpy = 2,2′-bipyridine, R represents the substitution at the 4- and 4′-positions), and their corresponding trishomoleptic Ru(L1)3–Ru(L3)3 as well as heteroleptic ruthenium(II) complexes Ru(tbbpy)2(L1) and Ru(tbbpy)2(L2) have been synthesized and characterized. Their applicability as immobilizable metal–organic chromophores in solar...
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Characterization of d-xylose reductase, XyrB, from Aspergillus niger
PublikacjaD-xylose reductase is a member of the aldo-keto reductase family, and is involved in D-xylose and L-arabinose conversion through the Pentose Catabolic Pathway (PCP) in fungi. In this study, we biochemically characterized a newly identified second D-xylose reductase (XyrB) from Aspergillus niger. This NADPH-dependent reductase is able to efficiently convert D-xylose and L-arabinose, and it has the highest affinity for these sugars...
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Characterization of metabolites in different kiwifruit varieties by NMR and fluorescence spectroscopy
PublikacjaIt is known from our previous studies that kiwifruits, which are used in common human diet, have preventive properties of coronary artery disease. This study describes a combination of 1H NMR spectroscopy, multivariate data analyses and fluorescence measurements in differentiating of some kiwifruit varieties, their quenching and antioxidant properties. A total of 41 metabolites were identified by comparing with literature data...
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Characterization of fatty acid composition in Eurasian badger (Meles meles)
PublikacjaPolyunsaturated fatty acids (PUFAs, LA and ALA) are not synthesized in mammals in the absence of their essential fatty acid precursors. However, hibernating animals and animals sleeping through the winter need sufficiently high amounts of these acids. The Eurasian badger does not hibernate, but sleeps over winter. In the autumn the body weight of adult badgers increases even twofold, since they put on fat before the winter. Fat...
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Numerical Characterization of Thresholds for the Focusing 1d Nonlinear Schrödinger Equation
PublikacjaThe focusing nonlinear Schrödinger equation arises in various physical phenomena and it is therefore of interest to determine mathematical conditions on the initial data that guarantee whether the corresponding solution will blow up in finite time or exist globally in time. We focus on solutions to the mass‐supercritical nonlinear Schrödinger equation (1) in 1D case. In particular, we investigate numerical thresholds between blow...
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Preparation and Characterization of Films Based on Disintegrated Bacterial Cellulose and Montmorillonite
PublikacjaThe food packaging materials from natural polymers including polysaccharides offer an ecologically important alternative to commonly used synthetic, non-biodegradable counterparts. The purpose of this work was to modify of bacterial cellulose (BC) leading to the improvement of its functional properties in terms of use as a food packaging material. Effects of disintegration of BC and addition of montmorillonite (MMT) on its water...
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The progress in characterization of polyurethanes morphology with different microscopic methods----WYJAŚNIĆ-----
PublikacjaW pracy opisano wyniki badań dotyczące analizy morfologii poliuretyanów określanej różnymi metodami. Omówiono mikroskopię optyczną, elektronową, mikroskopię termiczną, mikroskopię fluoroscencyjną, mikro-Ramana i mikroskopię sił atomowych.
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Preparation and physicochemical characterization of ceramic supports for supported liquid membranes
PublikacjaImmobilizowane membrany ciekłe stały się przedmiotem intensywnych badań w ostanich latach, głównie w procesach oczyszczania strumieni gazowych. Kluczowym czynnikiem mającym wpływ na efektywność tych procesów ma czas życia układu membranowego, a zatem odpowiedni dobór nośnika i fazy membranowej. W porównaniu do nośników polimerowych, ceramiczne charakteryzują się większą grubością, jednak są bardziej stabilne termicznie. Praca...
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Synthesis and Characterization of Poly(zwitterionic) Structures for Energy Conversion and Storage
PublikacjaZwitterions are unique class of molecules that possess two functional groups bearing electric charges, one positive and second negative. This setup results in peculiar properties such as high water retention and anti-fouling capability. Therefore, zwitterionic coatings and gels are commonly applied in e.g. biosensing and bioelectronic devices. Despite those applications, there are other perspectives for zwitterionic materials....
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Characterization of the c-BN/TiC, Ti3SiC2 systems by element selectivespectroscopy.
PublikacjaPomimo dużego technologicznego zainteresowania tytanowymi kompozytami bazującymi na c-BN daje się zauważyć wyraźny brak danych dotyczących lokalnego otoczenia atomów Ti w tego typu materiałach. Główna przyczyna tego stanu rzeczy tkwi w trudności związanej z analizą układu wielofazowego o dużej twardości za pomocą konwencjonalnych metod. Praca poświęcona jest analizie składu i struktury tytanowych kompozytów za pomocą atomowo-selektywnych...
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Characterization of the Co-base layers obtained by laser cladding technique.
PublikacjaBadano zawory wydechowe napawane dwoma stopami kobaltu, w tym mikrostrukturę strefy wierzchniej i strefy w pobliżu podłoża. Badano także rozkład pierwiastków w warstwie napawanej. Stwierdzono podobny skład chemiczny warstw i proszków.
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Characterization of the Co-base layers obtained by laser cladding technique.
PublikacjaBadano zawory wylotowe pokrywane stopami kobaltu: mikrostrukturę warstw w strefie wierzchniej i przy granicy napoina - metal. Badano rozkład pierwiastków w warstwach. Zarówno mikrostruktura, jak i skład chemiczny warstw były podobne w przypadku dwóch stosowanych stopów kobaltu.
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Characterization of wave structures containing sets of bow-tie resonators
PublikacjaArtykuł opisuje metodę analizy rozpraszania fali elektromagnetycznej układzie rezonatorów motylkowych w strukturach otwartych i zamkniętych. W artykule zaprezentowano przykłady aplikacji układów mikrofalowych zawierające opisywane elementy.
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Low-Coherence Interferometer with Nanocrystalline Diamond Films with Potential Application to Measure Small Biological Samples
PublikacjaThe study investigates a case of a low-coherence fiber-optic Fabry–Prerot interferometer with a nanocrystalline diamond (NCD) mirror. The method of achieving double density of interference fringes is proposed by the application of birefringent material in the cavity of the interferometer. It can be used to reduce sample volume in comparison to conventional interferometers. The use of a biocompatible diamond mirror makes it specifically...
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Direct estimation of linear and nonlinear functionals of quantum state
PublikacjaWe present a simple quantum network, based on the controlled-SWAP gate, that can extract certain properties of quantum states without recourse to quantum tomography. It can be used as a basic building block for direct quantum estimations of both linear and nonlinear functionals of any density operator. The network has many potential applications ranging from purity tests and eigenvalue estimations to direct characterization of...
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Characterization of single-stranded DNA-binding proteins from the psychrophilic bacteria
PublikacjaSingle-stranded DNA-binding proteins (SSBs) are indispensable elements in the cells of all living organisms. SSB proteins interact with ssDNA insequence in an independent manner, preventing them from forming secondary structures and from degradation by nucleases. In this way, SSB-binding proteins participate in all processes involving ssDNA, such as replication, repair and recombination. Although there are differences in amino...
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Characterization of single-stranded DNA-binding proteins from the psychrophilic bacteria
PublikacjaSingle-stranded DNA-binding proteins (SSBs) are indispensable elements in the cells of all living organisms. SSB proteins interact with ssDNAinsequence in an independent manner, preventing them from forming secondary structures and from degradation by nucleases. In this way, SSB-binding proteins participate in all processes involving ssDNA, such as replication, repair and recombination.Although there are differences in amino acid...
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Microwave Characterization of Dielectric Sheets in a Plano-Concave Fabry-Perot Open Resonator
PublikacjaDespite its long history, a double-concave (DC) Fabry-Perot open resonator (FPOR) has recently gained popularity in the characterization of dielectrics in the 20–110 GHz range, mainly due to such novel accomplishments as full automation of the measurement process and the development of even ore accurate and computationally efficient electromagnetic model. However, it has been discovered that such a DC resonator suffers from unwanted...
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Preparation and characterization of Pt/Pd-modified titanium dioxidenanoparticles for visible light irradiation
PublikacjaSeries of Pt/Pd–TiO2photocatalysts were obtained using the sol–gel method. The Pt/Pd–TiO2nanocom-posites showed significant visible light photoactivity. X-ray diffraction, STEM microscopy, UV–visspectroscopy and BET characterization allowed to conclude that the photocatalysts at the best perfor-mance had the anatase structure, 91 m2/g specific surface area, Pt/Pd alloy structure and 1–4 nm particlesize. The photocatalytic activity...
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Characterization of PVDF/Graphene Nanocomposite Membranes for Water Desalination with Enhanced Antifungal Activity
PublikacjaSeawater desalination is a worldwide concern for the sustainable production of drinking water. In this regard, membrane distillation (MD) has shown the potential for effective brine treatment. However, the lack of appropriate MD membranes limits its industrial expansion since they experience fouling and wetting issues. Therefore, hydrophobic membranes are promising candidates to successfully deal with such phenomena that are typical...
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Characterization of Modified Silica Gel as a Source of Ethene for Standard Gaseous Mixtures
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Synthesis and in vitro characterization of freeze-dried doxorubicin-loaded silica xerogels
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Characterization and Technical Application of Fine Photocatalytical Particles - A Study of the Immobilization of Photocatalysts
PublikacjaThe main aim of this dissertation was the transfer of photocatalytical laboratory scale experiments to semi-technical scale. Preliminary experiments of the purification of organic chlorine-loaded waters and the immobilization of photocatalysts were performed, which yielded the research back to the roots of synthesis. The first applied research was carried out on treatment of recreational water. Several light sources, particularly...
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Synthesis and electrochemical characterization of poly(3,4-ethylenedioxythiophene) modified by iron hexacyanocobaltate
PublikacjaPraca dotyczy sposobu syntezy oraz elektrochemicznej charakterystyki materiału kompozytowego złożonego z poli(3,4-etylenodioksytiofenu) i heksacyjanokobaltanu(III) żelaza(II). Wybrany materiał badany był przy użyciu spektroskopii impedancyjnej, chronopotencjometrii oraz woltamperometrii cyklicznej w kontakcie z elektrolitem wodnym (KCl) oraz aprotycznym (LiPF6 w mieszaninie węglanu etylenu i węglanu propylenu). Materiał charakteryzuje...
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Two tests for adhesive bonding long term characterization: principles and applications
PublikacjaThis article describes recent refinement of the traditional wedge test technique used to characterize durability of the adhesive joints. We propose two types of measuring protocols to monitor precisely and continuously the propagation of an "effective" crack during long term mode I fracture mechanic test. First method is directly derived from the traditional wedge test technique and consist in monitoring the surface strain of adherent...
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Characterization and photocatalytic activity of rare earth metal-doped titanium dioxide
PublikacjaW publikacji została przedstawiona metoda otrzymywania fotokatalizatorów na bazie TiO2 modyfikowanego erbem i iterbem. Otrzymane nanocząstki zostały scharakteryzowane za pomocą powierzchni właściwej BET, objętości porów. Zostały przedstawione widma absorpcyjne UV-Vis oraz właściwości fluorescencyjne otrzymanych nanoproszków. Dokonano również przedstawienia wyników pomiaru aktywności fotokatalitycznej pod wpływem promieniowania...
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Characterization of FeCo based catalyst for ammonia decomposition. The effect of potassium oxide
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From dolomite waste to katoite-based binder: Synthesis, performance and characterization
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Dynamic Nanoimpedance Characterization of the Atomic Force Microscope Tip-Surface Contact
PublikacjaNanoimpedance measurements, using the dynamic impedance spectroscopy technique, were carried out during loading and unloading force of a probe on three kinds of materials of different resistivity. These materials were: gold, boron-doped diamond, and AISI 304 stainless steel. Changes of impedance spectra versus applied force were registered and differences in the tip-to-sample contact character on each material were revealed. To...
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Chemical characterization of dew water collected in different geographic regions of Poland
PublikacjaPrzedstawiono wyniki badań składu chemicznego próbek rosy zebranych na terenie Polski w okresie od 2004 do 2006 roku na terenach: rolniczym (Wrocław, Dziemiany), miejskim w strefie wybrzeża (Gdańsk, Gdynia, Sopot), miejskim, położonym poza strefą wybrzeża (Bytów, Kraków, Mława). Próbki rosy badano w celu uzyskania informacji o składzie jakościowym i ilościowym. Celem badań było dostarczenie informacji o składzie chemicznym (i wybranych...
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Synthesis, characterization, and electrochemical testing of carbon nanotubes derivatized with azobenzene and anthraquinone.
PublikacjaWielościenne i jednościenne nanorurki węglowe modyfikowano na ścianach bocznych związkami elektrochemicznie aktywnymi, takimi jak azobenzen i antrachinon. Funkcjonalizowane nanorurki badano technikami spektroskopowymi i elektrochemicznymi oraz wykorzystując mikroskopię elektronową. Wyniki tych badań potwierdziły chemiczną modyfikację.
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Characterization of magnesium doped lanthanum orthoniobate synthesized by molten salt route
PublikacjaMolten salt synthesis method has been used to prepare the single phase magnesium doped lanthanum orthoniobate. The phase composition has been checked by X-ray diffraction method and the microstructure studies have been performed by scanning electron microscopy. The high temperature properties of the material have been investigated by thermogravimetry and electrochemical impedance spectroscopy. A dependence between sample total...
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Compatibility and rheological characterization of asphalt modified with recycled rubber-plastic blends
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Identification, characterization and purification of the lantibiotic staphylococcin T, a natural gallidermin variant
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Copolymerization of Styrene and Pentadecylphenylmethacrylate (PDPMA): Synthesis, Characterization, Thermomechanical and Adhesion Properties
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Polylactide Films with the Addition of Olive Leaf Extract—Physico-Chemical Characterization
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Biodegradable macromolecular conjugates of citropin: Synthesis, characterization and in vitro efficiency study
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Characterization of aggregate interlocking in hot mix asphalt by mechanistic performance tests
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Characterization of Chemically Activated Carbons Prepared from Miscanthus and Switchgrass Biomass
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Synthesis and characterization of resorcinol–formaldehyde resin chars doped by zinc oxide
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Synthesis and structural characterization of new cyclic siloxane with functionalized organic substituents
PublikacjaOcta(2-pyridyloxy)cyclotetrasiloxane was isolated as the product of the reaction between silicon disulfide and 2-hydroxypyridine. The new compound has been characterised by single crystal X-ray analysis, revealing a planar eight-membered ring with functionalized organic substituents on the silicon atoms.
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Fabrication and characterization of boron-doped nanocrystalline diamond-coated MEMS probes
PublikacjaFabrication processes of thin boron-doped nanocrystalline diamond (B-NCD) films on silicon-based micro- and nano-electromechanical structures have been investigated. Nanocrystalline boron doped -diamond (B-NCD) films were deposited using Microwave Plasma Assisted Chemical Vapour Deposition (MW PA CVD) method. The variation of B-NCD morphology, structure and optical parameters were particularly investigated. The use of truncated...
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Characterization of PVC-based polymer inclusion membranes with phosphonium ionic liquids
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Pincer Complexes Based on Phosphinoaminopyridines: Synthesis, Structural Characterization and Catalytic Applications
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CHARACTERIZATION OF MIXED LANGMUIR MONOLAYERS OF CYCLOSPORINE A WITH THE PHOSPHOLIPID DPPC AT THE CHITOSAN SUBPHASE
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