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wyświetlamy 1000 najlepszych wyników Pomoc
Wyniki wyszukiwania dla: NATURAL DEEP EUTECTIC SOLVENT ARSENIC AND ANTIMONY ANALYSIS LIQUID PHASE MICROEXTRACTION CENTRAL COMPOSITE DESIGN
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Controlling the size and morphology of precipitated calcite particles by the selection of solvent composition
PublikacjaCalcium carbonate particles were obtained in the reaction of calcium hydroxide with carbon dioxide at 65°C. Initial Ca(OH)2 suspensions were prepared in pure water and aqueous solutions of ethylene glycol or glycerol of the concentration range up to 20% (vol.). The course of reaction was monitored by conductivity measurements. Precipitated solids were analyzed by FTIR, XRD, SEM and the particles size distribution was determined...
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COMPOSITE INTERFACES
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Statistical analysis and robust design of circularly polarized antennas using sequential approximate optimization
PublikacjaIn the paper, reliable yield estimation and tolerance-aware design optimization of circular polarization (CP) antennas is discussed. We exploit auxiliary kriging interpolation models established in the vicinity of the nominal design in order to speed up the process of statistical analysis of the antenna structure at hand. Sequential approximate optimization is then applied to carry out robust design of the antenna, here, oriented...
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Optimization and Modeling of Cr (VI) Removal from Tannery Wastewater onto Activated Carbon Prepared from Coffee Husk and Sulfuric Acid (H2SO4) as Activating Agent by Using Central Composite Design (CCD)
PublikacjaThe primary goal of this research is to lower the hexavalent chromium (Cr (VI)) concentration that has occurred from the growth of the tannery industry. As a result, the potential for heavy metal concentration is increasing day by day. Industrial effluent containing Cr (VI) contributes significantly to water pollution. Chromium hexavalent ion (Cr (VI)) in wastewater is extremely hazardous to the environment. It is critical to address...
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The influence of intermolecular correlations on the infrared spectrum of liquid dimethyl sulfoxide
PublikacjaDimethyl sulfoxide (DMSO) is routinely applied as an excellent, water-miscible solvent and chemical reagent. Some of the most important data concerning its liquid structure were obtained using infrared (IR) spectroscopy. However, the actual extent of intermolecular correlations that connect the isolated monomer spectrum to the IR response of the bulk liquid is poorly studied thus far. Using ab initio molecular dynamics (AIMD) simulations,...
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Polarization rotaror - analysis and design
PublikacjaW artykule przedstawiono metodę analizy wielosekcyjnego polaryzatora złożonego z periodycznych szyków obiektów cylindrycznych. W celu analizy badanej struktury zastosowano metodę pełnofalową opartą na metodzie dopasowania rodzajów.
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Matrix solid-phase dispersion with sand in chromatographic analysis of essential oils in herbs
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Design of a most efficient fuel cell using noble metals and composite materials.
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Combined extraction and microextraction techniques: Recent trends and future perspectives
PublikacjaThe latest advancements in the analytical sample preparation indicate a trend of combining different extraction techniques with targeting an improvement in separation, cleanup, detection limits, enrichment factors, and dealing with complex matrices. This manuscript identifies mainly two groups of combined sample preparation techniques. The first group integrates conventional or enhanced extraction techniques with microextraction....
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Softwood-lignin/natural rubber composites containing novel plasticizing agent: Preparation and characterization
PublikacjaComposite materials based on natural rubber were obtained by using glycerolysate (decomposition prod- uct of polyurethane) as a novel plasticizer. In order to determine the effect of various lignin content, four different filler amounts were used, namely, 5 phr (parts per 100 parts of natural rubber) of lignin (WLI5G), 10 phr (WLI10G), 20 phr (WLI20G), and 40 phr (WLI40G). The reference specimen without lignin (WLI0G) was also...
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Structural design and sensitivity analysis of semi-rigid pavement of a motorway
PublikacjaThis paper presents application of mechanistic-empirical methods in design of semi-rigid pavement for a section of a motorway in Poland. The stage construction was assumed. Three fatigue criteria were applied in the design. For asphalt fatigue cracking and subgrade soil the criteria from the Asphalt Institute (USA) were applied. For fatigue cracking of cement stabilized bases the Dempsey (USA) and De Beer (South Africa) criteria...
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Design Thinking w edukacji
WydarzeniaCentrum Nowoczesnej Edukacji zaprasza na szkolenie „Design Thinking w edukacji”.
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Solid Phase Micro-Extraction, a Versatile and Handy Tool in Environmental Trace Organic Analysis, Gets a New Class of Coatings, Polymeric Ionic Liquids
PublikacjaSolid phase microextraction (SPME) fundamentals, characteristics and application are described. The special stress is put on characteristics of sorbents used as SPME fiber coatings. Description of commercially available fibers and the present-day trends in development of new sorbents for SPME are given. Discussion is focused on possibility of application of ionic liquids (IL) and polymeric ionic liquids (PIL) as SPME fiber coatings....
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Neural networks and deep learning
PublikacjaIn this chapter we will provide the general and fundamental background related to Neural Networks and Deep Learning techniques. Specifically, we divide the fundamentals of deep learning in three parts, the first one introduces Deep Feed Forward Networks and the main training algorithms in the context of optimization. The second part covers Convolutional Neural Networks (CNN) and discusses their main advantages and shortcomings...
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Andrzej Klimczuk
OsobyAndrzej Klimczuk, doktor nauk społecznych w zakresie nauki o polityce publicznej oraz socjolog. Adiunkt w Katedrze Polityki Społecznej Kolegium Ekonomiczno-Społecznego Szkoły Głównej Handlowej w Warszawie. W latach 2002-2009 redaktor i korespondent wydawnictw o grach komputerowych. W latach 2011-2013 wiceprezes Fundacji Laboratorium Badań i Działań Społecznych "SocLab". Ekspert zewnętrzny m.in. Komisji Europejskiej, programu URBACT,...
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Properties of Composite Oxide Layers on The Ti13Nb13Zr Alloy
PublikacjaThe development of composite oxide layers on the Ti13Nb13Zr alloy, their structure and properties have been demonstrated. Two subsequent methods were applied to prepare the composite layers. During the first stage gas oxidation produced a solid oxide layer, and subsequently oxide nanotubes were produced by using an electrochemical method. Scanning electron microscopy (SEM), chemical analysis, energy dispersive X-ray spectroscopy...
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Analysis of the design development of the sliding table saw spindles
PublikacjaProducers of sliding table saws constantly strive for improvement in sawing accuracy. One of the method is an upswing in a spindle behavior, since, it affects to a large degree sawing effects. The design development of sliding table saw spindles during the last quarter-century is presented. The spindle system of the modernized spindle of the sawing machine Fx550 is described.
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Experimental determination of dynamic properties of cylindrical steel tank model filled with liquid
PublikacjaIn technical branches, such as chemical or petroleum industries, cylindrical steel tanks are essential structures used for storage of liquid products. Any failure might have disastrous consequences, therefore their safety and reliability is essential. The aim of the present paper is to show the results of the experimental study which has been conducted on a scaled model of a real tank used in Poland. The investigation was carried...
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The vortex flow caused by sound in a bubbly liquid
PublikacjaGeneration of vorticity in the field of intense sound in a bubbly liquid in the free half-space is considered. The reasons for generation of vorticity are nonlinearity, diffraction, and dispersion. Acoustic streaming differs from that in a Newtonian fluid. Under some conditions, the vortex flow changes its direction. Conclusions concern streaming induced by a harmonic or an impulse Gaussian beam.
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Measurements of Two-phase Flows in Pipelines Using Radioisotopes and Statistical Signal Processing
PublikacjaThis paper presents an application of radiotracers and gamma absorption method in two-phase flow measurements in pipelines. Two different methods were implemented to analysis of acquired signals. Investigated methods are based on the cross-correlation function and the phase of the cross-spectral density distribution. The examples presented in the article illustrate the application of the radioisotopes to evaluation of liquid-gas...
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Buckling Analysis of a Micro Composite Plate with Nano Coating Based on the Modified Couple Stress Theory
PublikacjaThe present study investigates the buckling of a thick sandwich plate under the biaxial non-uniform compression using the modified couple stress theory with various boundary conditions. For this purpose, the top and bottom faces are orthotropic graphene sheets and for the central core the isotropic soft materials are investigated. The simplified first order shear deformation theory (S-FSDT) is employed and the governing differential...
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DESIGN AND THEORETICAL ANALYSIS OF A PROTOTYPE TILTING-PAD RADIAL BEARING WITH ADJUSTABLE CLEARANCE
PublikacjaThe article introduces a design and analysis results of a prototype ORC (organic Rankine cycle) turbo generator rotor assembly of 300kW power, supported by tilting-pad bearings of original design. The calculations were performed for a prototype turbo generator rotor. The shaft of this machine is supported with two radial bearings, lubricated with an unusual lubricant – a low-boiling-point agent. The main objective of the presented...
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Preparation and evaluation of 1,3-alternate 25,27-bis-(pentafluorobenzyloxy)-26,28-bis-(3-propyloxy)-calix[4]arene-bonded silics gel high performance liquid chromatography stationary phase
PublikacjaA 1,3-alternate 25,27-bis-(pentafluorobenzyloxy)-26,28-bis-(3-propyloxy)-calix[4]arene-bonded silica gel stationary phase (CalixBzF10) was synthesized, structurally characterized, and used as a selector in liquid chromatography. The selectivity study of this phase was done by using fluorine-containing compounds (fluorobenzenes, fluoro-pyrimidine bases), as well as non-fluorinated analytes (non-steroidal anti-inflammatory drugs,...
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Dariusz Mikielewicz prof. dr hab. inż.
OsobyDariusz Mikielewicz – urodził się 6 lutego 1967 roku w Gdańsku, w 1985r. zdał pomyślnie egzaminy wstępne na Wydział Budowy Maszyn Politechniki Gdańskiej, który ukończył z wynikiem bardzo dobrym w 1990 roku na specjalności Maszyny i Urządzenia Energetyczne. Zainteresowania pracą naukową skłoniły go do podjęcia badań na University of Manchester na wydziale mechanicznym i energetyki jądrowej (Mechanical and Nuclear Engineering Department)...
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Multicriteria decision analysis in ranking of analytical procedures for aldrin determination in water
PublikacjaThe study presents the possibility of multi-criteria decision analysis (MCDA) application when choosing analytical procedures with low environmental impact. A type of MCDA, Preference Ranking Organization Method for Enrichment Evaluations (PROMETHEE), was chosen as versatile tool that meets all the analytical chemists – decision makers requirements. Twenty five analytical procedures for aldrin determination in water samples (as...
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Deep Learning w Keras
Kursy OnlineKurs przeznaczony dla słuchaczy studiów podyplomowych Sztuczna inteligencja i automatyzacja procesów biznesowych w ujęciu praktycznym - edycja biznesowa.
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Silicon polypodands: a new class of efficient solid–liquid phase-transfer catalysts
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Application of a new class B-podands in solid–liquid phase transfer catalysis
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A new type of B-podand catalysts for solid–liquid phase transfer reactions
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Balance of pesticides mass in gas, liquid and solid phase after their chemical degradation.
PublikacjaOpisano metodę usuwania pestycydów z wody przy zastosowaniu fotodegradacji (UV) i katalizatora (TiO2). Efektywność procesu usuwania pestycydów była kontrolowana przy zastosowaniu chromatografu gazowego z detektorem wychwytu elektronów. Oznaczano zawartość pestycydów w wodzie, a także zaadsorbowanych na powierzchni stałej, oraz w fazie gazowej. Największa zawartość pestycydów znajdowała się na fazie stałej, następnie w cieczy i...
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Discussion:Horizontal stress increase induced by deep vibratory compaction
PublikacjaDeep compaction control of granular material using the results of field tests. The analysis include the CPTU and DMT tests terformed before and after compaction works.
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Design Analysis of Micro Gas Turbines in Closed Cycles
PublikacjaThe problems faced by designers of micro-turbines are connected with a very small volume flow rate of working media which leads to small blades’ height and high rotor speed. In the case of gas turbines this limitation can be overcome by the application of a closed cycle with very low pressure at the compressor inlet (lower than atmospheric pressure). In this way we may apply a micro gas turbine unit of accepted efficiency to work...
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Design analysis of ORC micro-turbines making use of thermal energy of oceans
PublikacjaThe article presents the results of the analysis of energy conversion cycles making use of thermal energy of oceans. The objects of analysis were two cases of closed Organic Rankine Cycle (ORC) power plants, which were: the cycle in which the vapour of the working medium was produced by warm oceanic water in the circum-equatorial zone, and the so-called “arctic” cycle in which this vapour was produced by non-frozen water in the circumpolar...
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JOURNAL OF PHASE EQUILIBRIA AND DIFFUSION
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Rain Gardens GC_MS analysis dataset
Dane BadawczeThis dataset contains the results of samples analysis (no-target analysis: scan mode) using gas chromatography coupled with mass spectrometry GC–MS (GC-2030 NEXIS MS, Shimadzu, Japan or Thermo Scientific, Waltham, USA).
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The Application of Cluster Analysis in the Research on Central European National Park Websites
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THERMAL ANALYSIS AND DESIGN OF HYBRID MICROCHANNEL-MICROJET TEST PROBE
PublikacjaThe paper presents the numerical investigation of a microjet- microchannel cooling module. In which microjets of water are impinging into the microchannels and forming a liquid film on the impingement surface. Applied technology takes benefits from two very attractive heat removal techniques. When lminar jets are impinging on the surface have a very high kinetic energy at the stagnation point, also in microchannels boundary layer...
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Opportunities and shortcomings of ionic liquids in single-drop microextraction
PublikacjaThe synergistic combination of ionic liquids (ILs) and single-drop microextraction (SDME) involves a powerful coupling toward the development of sustainable analytical methodologies. This overview provides a survey of the literature regarding the IL-SDME, including a database on relevant physicochemical properties of ILs for their application in SDME, the strategies implemented to combine IL-based SDME methods efficiently with...
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Theoretical analysis and experimental tests of tilting pad journal bearings with shoes made of polymer material and low-boiling liquid lubrication
PublikacjaSelecting the appropriate bearing system for the rotor requires a good knowledge of the available solutions and the operating conditions of the machine. For newly designed machinery operating in adverse conditions, selecting bearings that ensure correct and long-lasting operation can be extremely challenging. Difficulties in- crease when the machine’s operating parameters are beyond the technical capabilities of available technical solutions....
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Comparative study of bisphenols in e-cigarette liquids: evaluating fabric phase sorptive extraction, ultrasound-assisted membrane extraction, and solid phase extraction techniques
PublikacjaTo address the under-researched risk of bisphenols (BPs) in e-cigarette liquids, comprehensive studies have been conducted to propose optimum sample preparation and analysis methods. To determine twelve BPs in refill liquids for e-cigarettes, three sample preparation methods based on distinct operational and working principles were employed. These included fabric phase sorptive extraction (FPSE), ultrasound-assisted solvent extraction...
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Recent advances in extraction and analysis procedures of natural chlorogenic acids
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On geometrically non-linear FEA of laminated FRP composite panels
PublikacjaThe paper presents a state-of-art review on Finite Element Analysis (FEA) of geometrically non-linear problems for laminated composite plates and shells made as fibre reinforced polymer (FRP) laminates. Besides a subjective overview of the historical development of geometrically non-linear FEA of laminated FRP composite panels, some remarks on possible future issues in this research area are given
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Optimization of liquid chromatographic separation of pharmaceuticals within green analytical chemistry framework
PublikacjaThe contribution is aimed at the development of methodology that allows to consider green analytical chemistry criteria during optimization of liquid chromatographic separation with design of experiment. The objectives of the optimization are maximization of peak areas of five non-steroid anti-inflammatory drugs, maximization of resolution between peaks, with simultaneous shortening of chromatographic separation time and minimization...
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Sequential Analysis-Design Methods and Applications
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Headspace Solid-Phase Microextraction Coupled with Gas Chromatography–Mass Spectrometry for the Determination of Volatile Organic Compounds in Urine
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Theoretical analysis of solvent effects on nitrogen NMR chemical shifts in oxazoles and oxadiazoles
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Optimization of adsorption of methyl orange from aqueous solution by magnetic CoFe2O4/ZnAl-layered double hydroxide composite using response surface methodology
PublikacjaThe CoFe2O4/ZnAl-layered double hydroxide (LDH) composite was successfully developed through a facile co-precipitation method, characterized, and applied as an effective adsorbent for the removal of methyl orange (MO) dye from aqueous solutions. The central composite design (CCD) of the response surface methodology (RSM) was employed to estimate and optimize process variables such as initial MO concentrations, solution pH, adsorbent...
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Selected aspects of modern X-ray structural analysis 2025 kopia 1
Kursy OnlineSelected Aspects of Modern X-ray Structural Analysis. The aim of the lecture is to provide the PhD students, studying at natural sciences departments, an overview of contemporary X-ray structural analysis. The presented subject is exploited in many distant areas of modern technologies, materials science, crystal engineering, organic or inorganic synthesis of new chemicals, drug design, molecular biology, etc. It becomes necessary...
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Rural Design Studio- 2024
Kursy OnlineSummer practice - rural analysis, works on the map, in a terrain and with the people and subsequent Design Studio in winter semester of 2024/25
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Estimation of interior-permanent-magnet-synchronous-motor rotor position by analysis of phase-current derivatives
PublikacjaThis paper describes an algorithm for estimation of IPMSM rotor angular position. The algorithm uses derivatives of motor phase currents resulting from PWM modulation to obtain the rotor position. The presented method is designed for medium- and high-speed range, since it is based on determination of the EMF vector. Calculation of the motor position is performed in every PWM cycle. The standard SV-PWM method is used to determine...