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wyświetlamy 1000 najlepszych wyników Pomoc
Wyniki wyszukiwania dla: ETHANOL BIOMARKERS DETERMINATION
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Direct determination of paraquat herbicide by square-wave voltammetry by two-step transfer mechanism at heterogeneous boron-doped carbon nanowall electrodes
PublikacjaBoron-doped carbon nanowalls (B:CNW) versus boron-doped diamond (BDD) materials were investigated for the effective electrochemical detection of highly toxic herbicide paraquat (PQ). Depending on the surface morphology and functional groups of BDD and B:CNWs, the electrochemical absorption and detection of the target analyte PQ revealed different detection mechanisms. The surface absorption mechanism was mainly observed for BDD,...
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Application of high performance liquid chromatography with ultraviolet diode array detection and refractive index detection to the determination of class composition and the analysis of gasoline.
PublikacjaZaprezentowano nową metodę HPLC oznaczania składu grupowego benzyn i komponentów benzyn tj. oznaczania zawartości olefin, węglowodorów aromatycznych i parafinowo-naftenowych.
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Oznaczanie lotnych kwasów tłuszczowych w ściekach metodą chromatografii gazowej =Determination of volatile fatty acids in wastewater using gas chromatography.
PublikacjaPrzedstawiono metody oznaczania lotnych kwasów tłuszczowych (LKT) w ściekachze szczególnym uwzględnieniem chromatografii gazowej. Omówiono rolę LKT wprocesie biologicznego oczyszczania ścieków. Scharakteryzowano poszczególneetapy procedury analitycznej, począwszy od pobrania próbek rzeczywistych askończywszy na sposobie detekcji. Ze względu na znaczną złożoność matrycyjaką stanowią ścieki, główny nacisk położono na techniki...
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Analysis of MArkers of Exposure to Constituents of Environmental Tobacco Smoke (ETS)
PublikacjaTobacco smoke is a complex mixture of more than 4000 chemical compounds, many of which are harmful to human health. These compounds belong to various chemical classes, including amides, imides, lactams, carboxylic acids, aldehydes, ketones, alcohols, phenols, amines, hydrocarbons, ethers, and inorganic compounds. There are three types of tobacco smoke streams: the mainstream, the sidestream, and environmental tobacco smoke (ETS)....
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Suspension and process parameters selection for electrophoretic deposition of Mn–Co spinel coating on steel interconnects
PublikacjaMetallic interconnect coatings, consisting of MnCo2O4 spinel, were effectively applied to Crofer 22 APU using the electrophoretic deposition (EPD) method in both H2O: ethanol and pure ethanol solvents. The primary goal of this method was to prevent chromium migration, minimize evaporation, and control the oxidation rate. The study aimed to assess the quality, adhesion, and thickness of the Mn–Co coating, with the objective of...
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Application of analytical procedure based on accelerated solvent extraction and ion chromatography technique for determination of thiocyanate and other inorganic ions in human placenta samples
PublikacjaExposure of a pregnant woman during pregnancy is a special case of exposure to toxic substances. Samples of placenta collected for the studies had been prepared with the technique of accelerated solvent extraction and later analyzed for the presence of thiocyanate ion and other inorganic ions, with the use of the technique of ion chromatography. The concentration of thiocyanate ion in placenta samples collected from active smokers...
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On the coupling of hydride generation with atmospheric pressure glow discharge in contact with the flowing liquid cathode for the determination of arsenic, antimony and selenium with optical emission spectrometry
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Simultaneous determination of hydrophobicity and dissociation constant for a large set of compounds by gradient reverse phase high performance liquid chromatography–mass spectrometry technique
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Nowe metodyki oznaczania dodatków do paliw z zastosowaniem rozdzielenia wielopomiarowego = New procedures for fuel additives determination by multidimensional separation systems
PublikacjaW pracy przedstawiono wyniki badań nad opracowaniem metodyki oznaczania wybranych dodatków "myjących" w paliwie diesla. Porównano metodyki jednoetapowe z wykorzystaniem chromatografii gazowej z detektorem płomieniowo-jonizacyjnym (GC-FID) lub spektrometrem mas (GC-MS) oraz wysokosprawnej chromatografii cieczowej z detektorem UV z matrycą fotodiodową (HPLC-UV-DAD), z metodykami dwuetapowymi, w których do wstępnej izolacji składników...
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Determination of pterins in urine by HPLC with UV and fluorescent detection using different types of chromatographic stationary phases (HILIC, RP C8, RP C18)
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A Novel Electrochemical Sensor Based on Graphene Oxide Nanosheets and Ionic Liquid Binder for Differential Pulse Voltammetric Determination of Droxidopa in Pharmaceutical and Urine Samples
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Synthesis of UiO-66-OH zirconium metal-organic framework and its application for selective extraction and trace determination of thorium in water samples by spectrophotometry
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Highly Sensitive Determination of Bisphenol A in Bottled Water Samples by HPLC after Its Extraction by a Novel Th-MOF Pipette-Tip Micro-SPE
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Simultaneous voltammetric determination of Cd2+, Pb2+, and Cu2+ ions captured by Fe3O4@SiO2 core-shell nanostructures of various outer amino chain length
PublikacjaIn the present study, we examined a novel functionalised magnetic nanoparticles Fe3O4@SiO2-Nn as a nano adsorbent for binding of Cd2+, Pb2+, Cu2+ ions in an aqueous solution. First, we obtained the nanoparticles functionalised with various carbon chains containing different number of amino groups: (3-amino)propyltriethoxysilane (Fe3O4@SiO2-N1), N-(2-aminoethyl)-3-aminopropyltrimethoxysilane (Fe3O4@SiO2-N2) and N1-(3-trimethoxysilylpropyl)diethylenetriamine...
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Determination of polycyclic aromatic hydrocarbons (PAHs) and other organic pollutants in freshwaters on the western shore of Admiralty Bay (King George Island, Maritime Antarctica).
PublikacjaOrganic contamination in freshwater samples has never been investigated at the western shore of Admiralty Bay. Therefore, the presence of polycyclic aromatic hydrocarbons (PAHs) in five different sites distributed along a shore running from the Arctowski Station to the Baranowski Glacier was studied. Moreover, organic compounds such as n-alkanes, toluene and ethylbenzene were also noted. Increased ΣPAHs in late Austral summer 2016...
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Modification of gradient HPLC method for determination of small molecules' affinity to human serum albumin under column safety conditions: Robustness and chemometrics study
PublikacjaIn the early stages of drug discovery, beyond the biological activity screening, determining the physicochemical properties that affect the distribution of molecules in the human body is an essential step. Plasma protein binding (PPB) is one of the most important investigated endpoints. Nevertheless, the methodology for measuring %PPB is significantly less popular and standardized than other physicochemical properties, like lipophilicity....
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Determination of organotin compounds in biological samples using accelerated solvent extraction, sodium tetraethylborate ethylation, and multicapillary gas chromatography flame photometric detection.
PublikacjaPrzedstawiono metodę oznaczania związków cynoorganicznych w próbkach biologicznych. Procedura oparta jest na wykorzystaniu ekstrakcji pod zwiększoną temperaturą i ciśnieniem (ASE) do izolacji związków cynoorganicznych z próbek wątroby morświnów odłowionych w Morzu Bałtyckim. Walidacji metody dokonano na podstawie analizy materiału odniesienia NIES No 11.
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Związki metaloorganiczne w glebach i osadach dennych - występowanie, przemiany i oznaczanie = Metallorganic compounds in soils and sediments - occurence, transformations and determination
PublikacjaW oparciu o literaturę poświęconą występowaniu i sposobom oznaczania wybranych związków metaloorganicznych rtęci, cyny, ołowiu, selenu i arsenu, przedstawiono źródła ich występowania, zastosowanie oraz mechanizm toksycznego działania. Przedstawiono podstawowe zagadnienia związane z analityką specjacyjną oraz scharakteryzowano podstawowe etapy procedury analitycznej, stosowanej do oznaczania związków metaloorganicznych (Hg, Sn,...
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Determination of non-steroidal anti-inflammatory drugs in natural waters using off-line and on-line SPE followed by LC coupled with DAD-MS
PublikacjaOpisano dwie metody pozwalające na jednoczesne oznaczanie zawartości niesterydowych leków przeciwzapalnych (difluisal, diklofenak, naproksen, tolmetin, fenoprofen, ibuprofen) w próbkach wodnych. Próbki przygotowywano do analizy z użyciem techniki ekstrakcji do fazy stałej (off-line i on-line). Natomiast oznaczeń końcowych dokonano z użyciem LC-DAD-MS. Sprawdzono kilka różnych kolumienek ekstrakcyjnych i wybrano RP-18 jako najlepsze...
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Comparison of Ozonation and Evaporation as Treatment Methods of Recycled Water for Bioethanol Fermentation Process
PublikacjaThe paper compared the performance of the ethanol yield after alcoholic fermentation with samples of rejected (RW) and permeate water (PW), RW and PW treated by oxidation with ozone (O3) (5 and 15 min) and evaporation, aiming the recirculation back to the bioethanol process. RW and PW were collected after an anaerobic bioreactor (AnBR) used for stillage treatment. Nine types of fermentations were made, where one used 100% tap...
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Proteomic and Metabolomic Changes in Psoriasis Preclinical and Clinical Aspects
PublikacjaSkin diseases such as psoriasis (Ps) and psoriatic arthritis (PsA) are immune-mediated inflammatory diseases. Overlap of autoinflammatory and autoimmune conditions hinders diagnoses and identifying personalized patient treatments due to different psoriasis subtypes and the lack of verified biomarkers. Recently, proteomics and metabolomics have been intensively investigated in a broad range of skin diseases with the main purpose...
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Determination of flow properties of a serial connection of a directional control valve with (C=5.7, b=0.32) and a air blow gun from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient...
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Determination of flow properties of a serial connection of a directional control valve with (C=2.1, b=0.14) and a air blow gun from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient...
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Determination of flow properties of a serial connection of a pressure relief valve with (C=7.3, b=0.49) and a air blow gun from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a serial connection of a directional control valve with (C=2.8, b=0.25) and a air blow gun from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient...
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Determination of flow properties of a serial connection of a directional control valve with (C=5.5, b=0.37) and a air blow gun from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient...
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Determination of flow properties of a serial connection of a pressure relief valve with (C=6.4, b=0.45) and a air blow gun from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a serial connection of a pressure relief valve with (C=6.2, b=0.38) and a air blow gun from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a serial connection of a directional control valve with (C=2.4, b=0.26) and a air blow gun from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient...
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Determination of flow properties of a serial connection of a pressure relief valve with (C=3.3, b=0.40) and a air blow gun from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a serial connection of a directional control valve with (C=2.0, b=0.11) and a air blow gun from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient...
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Determination of flow properties of a serial connection of a pressure relief valve (C=6.4, b=0.45) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...
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Determination of flow properties of a serial connection of a directional control valve (C=2.4, b=0.26) and a silencer (C=1.4) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.4, b=0.26) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.4, b=0.26) and a silencer (C=3.4) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.4, b=0.26) and a silencer (C=3.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.8, b=0.25) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=5.7, b=0.32) and a silencer (C=1.4) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.1, b=0.14) and a silencer (C=1.4) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=5.7, b=0.32) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a pressure relief valve (C=6.2, b=0.38) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...
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Determination of flow properties of a serial connection of a directional control valve (C=5.5, b=0.37) and a silencer (C=1.4) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.0, b=0.11) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.0, b=0.11) and a silencer (C=3.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.8, b=0.25) and a silencer (C=3.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.1, b=0.14) and a silencer (C=6.8) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=5.7, b=0.32) and a silencer (C=3.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a pressure relief valve (C=3.3, b=0.40) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient atmosphere, (2) pressure source...
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Determination of flow properties of a serial connection of a directional control valve (C=2.0, b=0.11) and a silencer (C=1.4) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...
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Determination of flow properties of a serial connection of a directional control valve (C=2.1, b=0.14) and a silencer (C=7.0) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a silencer arranged in-line. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere, (2) pressure...