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Wyniki wyszukiwania dla: detection methods
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Chemical Derivatization Processes Applied to Amine Determination in Samples of Different Matrix Composition
PublikacjaAmines are important biological compounds, and so their analysis and monitoring in various matrices is worthy of investigation and development.Due to the polar nature of amines, chromatographic analysis of free amines is generally unsatisfactory owing to adsorption and decomposition of the solute on the column, resulting in peak tailing and losses. Therefore, many derivatization reactions are employed to reduce the polarity, improve...
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Methylene Blue Near-Infrared Fluorescence Imaging in Breast Cancer Sentinel Node Biopsy
PublikacjaIntroduction: Fluorescence-based navigation for breast cancer sentinel node biopsy is a novel method that uses indocyanine green as a fluorophore. However, methylene blue (MB) also has some fluorescent properties. This study is the first in a clinical series presenting the possible use of MB as a fluorescent dye for the identification of sentinel nodes in breast sentinel node biopsy. Material and methods: Forty-nine patients with...
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Rapid and simple multi-analyte LC–MS/MS method for the determination of benzodiazepines and Z-hypnotic drugs in blood samples: Development, validation and application based on three years of toxicological analyses
PublikacjaBenzodiazepines (BZDs) and Z-drugs have been particularly important treatments for sleeping and anxiety disorders for many years. However, recently, a number of new benzodiazepines (named designer benzodiazepines, DBZDs) were synthesised, but some of them have never been used in the clinic; they reached the black drug market as new psychoactive substances and are used for recreational purposes. The abuse of these substances has...
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The effect of raw material type on endotoxin content .
Dane BadawczeThe datasets contain the results of determining the effect of raw material type on endotoxin content as well as the effect of purification methods. The endotoxin concentration was determined using the PyroGene Recombinant Factor C Endpoint Fluorescent Assay. Beckmann-Kenko sodium alginate and Chemat sodium salt of alginic acid were used for the assays....
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The SEM images of LSCNT reduced at 900 degrees C under H2
Dane BadawczeThe dataset includes SEM image of La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s sintered at 1200oC under air atmosphere for 12 h and reduced at 900oC under H2 for 10 h. Samples were produced using aqueous soft chemistry methods (Pechini).
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The XRD diffraction patterns of reduced LSCNT prepared using two methods and two sintering temperatures
Dane BadawczeThe dataset includes XRD diffraction patterns of La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s produced using two methods, namely organic (citrate assisted) and Pechini sintered at 1000 or 1200oC under air atmosphere and reduced at 900 for 12 h in wet H2.
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The SEM images of LSCNT reduced at 800 degrees C under H2
Dane BadawczeThe dataset includes SEM images of La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s sintered at 1200oC under air atmosphere for 12 h and reduced at 800oC under H2 for 10 h. Samples were produced using aqueous soft chemistry methods (Pechini).
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The SEM images of LSCNT reduced at 1000 degrees C under H2
Dane BadawczeThe dataset includes SEM images of La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s sintered at 1200oC under air atmosphere for 12 h and reduced at 1000oC under H2 for 10 h. Samples were produced using aqueous soft chemistry methods (Pechini).
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The SEM images of LSCNT sintered at 1200 degrees C in air
Dane BadawczeThe dataset includes SEM images of La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s sintered at 1200oC under air atmosphere for 12 h. Samples were produced using aqueous soft chemistry methods (Pechini). The grain structure can be seen on higher resolution image.
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BET (Brunauer-Emmett-Teller) surface area analysis of titanium dioxide coated nickel foams
Dane BadawczeThe data are presented for the BET surface results of nickel foams coated with titanium dioxide and heated 400, 500 and 600 degrees Celsius in an argon atmosphere. N2 sorption was performed at 77 K pore size distribution was determined by BJH and DFT methods.
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This dataset contains results of our investigation aiming in determination of antioxidant potential of the propolis extract produced in our laboratory.
Dane BadawczeThis dataset contains results of our investigation aiming in determination of antioxidant potential of the propolis extract produced in our laboratory. The propolis samples were delivered by Polish beekeepers. DPPH and FREAP methods were used. Moreover, total phenolic contents in the extracts were determined.
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Simultaneous measurements of ECG, body Impedance and temperature
Dane BadawczeThe data are complementary part of the experiment designed to demonstrate how to use the network protocols to transmit medical data. The dataset contains biomedical signals of ECG, Impedanc and temperature acquired simultaneously. The data allow students to become familiar with data acquisition methods (simulate data transmission by medical device over...
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DES - polarity, pH and antioxidant potential
Dane BadawczeThis physicochemical properties of selected deep eutectic solvents (DES) were tested. Polarity is important for extraction efficiency. The values of pH can importantly affect growing of bacteria and yeasts strains. Total phenolic content, DPPH and FRAP methods were used for determination of antioxidant potential of the extract produced with DES.
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Personal income tax - tax scales in 1992–2019
Dane BadawczeThe tax rate is the ratio (usually expressed as a percentage) at which a business or person is taxed. There are several methods used to present a tax rate: statory, average, marginal, and effective. These rates can also be presented using different definitions applied to a tax base: inclusive and exclusive.
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Sensory analysis of confectionery products.
Dane BadawczeThe data set presents the results of the sensory analysis of confectionery products, which was carried out by the sensory profiling analysis method based on the PN-ISO 11035: 1999 standard – “Sensory analysis - Identification and selection of descriptors for determining the sensory profile using multivariate methods”. The method was used to evaluate...
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Molecularly targeted nanoparticles: an emerging tool for evaluation of expression of the receptor for advanced glycation end products in a murine model of peripheral artery disease
PublikacjaAbstract Background: Molecular imaging with molecularly targeted probes is a powerful tool for studying the spatio-temporal interactions between complex biological processes. The pivotal role of the receptor for advanced glycation end products (RAGE) in numerous pathological processes, aroused the demand for RAGE targeted imaging in various diseases. In the study, we evaluated the use of a diagnostic imaging agent for RAGE quantification...
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Sensory analysis of bread samples with the addition of beetroot
Dane BadawczeThe data set presents the results of the sensory analysis of bread samples with the addition of beetroot, which was carried out by the sensory profiling analysis method based on the PN-ISO 11035: 1999 standard – “Sensory analysis - Identification and selection of descriptors for determining the sensory profile using multivariate methods”. The method...
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BET specific surface area measurements of silica-coated bismuth oxide (Bi2O3)/gadolinium oxide (Gd2O3) core-shell structures
Dane BadawczeThe BET specific surface area was measured using an N2 adsorption/desorption isotherm (Micromeritics ASAP 2460, Norcross, GA, USA).
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The AFM micrographs of pitting corrosion evolution on high-alloy steel 1.4301
Dane BadawczeThe dataset contains the results of topographic imaging of high-alloy stainless steel 1.4301 on which the pitting corrosion process was induced by electrochemical methods. The study of the effects of a local attack allows for conclusions about the intensity and mechanism of this type of corrosion. The file contains atomic force microscopy (AFM) data...
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XPS investigations of tge tin/tin oxides - CNT composites
Dane BadawczeThe composite of tin/tin oxide nanoparticles with graphene oxide and CMC based on laser ablation technique as an electrode material for energy storage devices were manufactured. The material exhibited a three-dimensional conducting graphene oxide network decorated with tin or tin oxide nanoparticles. The presence of tin/tin oxide in composites was...
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A novel method for drop in drop edible oils encapsulation with chitosan using a coaxial technique
Dane BadawczeThe dataset present a novel one step method for oil encapsulation. In this coaxial system the oil constitutes the core of the capsule, while the chitosan solution is the polymer shell surrounding the core to provide separation of the core from the external environment. In comparison to other encapsulation methods, the presented technique is much simpler...
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Computer controlled systems - 2022/2023
Kursy Onlinemateriały wspierające wykład na studiach II stopnia na kierunku ACR pod tytułem komputerowe systemy automatyki 1. Computer system – controlled plant interfacing technique; simple interfacing and with both side acknowledgement; ideas, algorithms, acknowledge passing. 2. Methods of acknowledgement passing: software checking and passing, using interrupt techniques, using readiness checking (ready – wait lines). The best solution...
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CCS-lecture-2023-2024
Kursy Onlinemateriały wspierające wykład na studiach II stopnia na kierunku ACR pod tytułem komputerowe systemy automatyki 1. Computer system – controlled plant interfacing technique; simple interfacing and with both side acknowledgement; ideas, algorithms, acknowledge passing. 2. Methods of acknowledgement passing: software checking and passing, using interrupt techniques, using readiness checking (ready – wait lines). The best solution optimization...
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The XRD diffraction patterns of Ce(Pr,Sm)O2-s samples
Dane BadawczeThe dataset includes XRD diffraction patterns of Ce(Pr,Sm)O2-s samples of various stoichiometries of Pr and Sm dopants. Samples were produced using aqueous soft chemistry methods (microemulsion method).
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Full CI ground state potential energy curves and one-electron relativistic corrections for hydrogen molecule in various basis sets
Dane BadawczeThis dataset consists of Full CI ground state Born-Oppenheimer potential energy curves and one-electron relativistic corrections for hydrogen dimer. Nonrelativistic energies, as well as one electron relativistic corrections (treated perturbatively with help of the Cowan-Griffin Hamiltonian) are presented for internuclear distances between 0.8 and 10...
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Communication methods at selected private universities in Gdańsk, Sopot and Gdynia in 2010
Dane BadawczeA university, including a private one, is an organization serving the environment. Therefore, a necessary condition (especially in today's market situation) is the development of cooperation between universities and the environment. Creating mutual relations between universities with the environment, belongs to an important area of activity of this...
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The electrical properties mesurements of SOFC with Ce0.8Pr0.15Sm0.05O2-s layer
Dane BadawczeThe dataset includes The electrical properties mesurements of SOFC with Ce0.8Pr0.15Sm0.05O2-s layer. Samples were produced using aqueous soft chemistry methods (microemulsion method) and applied in form of a layer onto the anode of the commercial SOFC. The SOFC was working under biogas feeding.
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The electrical properties mesurements of SOFC with Ce0.8Pr0.2O2-s layer
Dane BadawczeThe dataset includes The electrical properties mesurements of SOFC with Ce0.8Pr0.2O2-s layer. Samples were produced using aqueous soft chemistry methods (microemulsion method) and applied in form of a layer onto the anode of the commercial SOFC. The SOFC was working under biogas feeding.
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The electrical properties mesurements of SOFC with Ce0.8Sm0.2O2-s layer
Dane BadawczeThe dataset includes The electrical properties mesurements of SOFC with Ce0.8Sm0.2O2-s layer. Samples were produced using aqueous soft chemistry methods (microemulsion method) and applied in form of a layer onto the anode of the commercial SOFC. The SOFC was working under biogas feeding.
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The electrical properties mesurements of SOFC with Ce0.8Pr0.1Sm0.1O2-s layer
Dane BadawczeThe dataset includes The electrical properties mesurements of SOFC with Ce0.8Pr0.1Sm0.1O2-s layer. Samples were produced using aqueous soft chemistry methods (microemulsion method) and applied in form of a layer onto the anode of the commercial SOFC. The SOFC was working under biogas feeding.
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The electrical properties mesurements of SOFC with Ce0.8Pr0.05Sm0.15O2-s layer
Dane BadawczeThe dataset includes The electrical properties mesurements of SOFC with Ce0.8Pr0.05Sm0.15O2-s layer. Samples were produced using aqueous soft chemistry methods (microemulsion method) and applied in form of a layer onto the anode of the commercial SOFC. The SOFC was working under biogas feeding.
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Complementary Use of Multi-dimensional Gas Chromatography and Proton Transfer Reaction Mass Spectrometry for Identification of Rapeseed Oil Quality Indicators
PublikacjaThe change of concentration of various volatiles generated during frying may be an indicator of oil quality. Chemical compounds such as aldehydes, ketones, alcohols and carboxyl acids are the products of oxidation during thermal degradation of edible oils. Shown in this work is a complementary use of GC×GC-TOFMS and PTR-MS for the detection and determination of quality indicators of rapeseed oil. The former technique was used for...
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The XPS spectra of Ce0.8Ni0.2O2 prepared using microemulsion method
Dane BadawczeThe dataset includes XPS spectra of Ce0.8Ni0.2O2-s sintered under air atmosphere. Samples were produced using aqueous soft chemistry methods (microemulsion). The XPS spectra were collected for all species.
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Reflectance Measurements and iCone Calorimeter Burning Results of Charcoals Derived from Lake Żabińskie (North-Eastern Poland)
Dane BadawczeThe dataset presents the results of litter burning experiments using an iCone calorimeter to assess the flammability of the major tree species in the Lake Żabińskie catchment (NE Poland) and links this to the heat release during burning to understand the influence of fire and its effects on ecosystems. Samples of litter from Betula pendula, Pinus sylvestris,...
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The XPS spectra of Ce0.8Cu0.2O2 prepared using microemulsion method
Dane BadawczeThe dataset includes XPS spectra of Ce0.8Cu0.2O2-s sintered under air atmosphere. Samples were produced using aqueous soft chemistry methods (microemulsion). The XPS spectra were collected for all species.
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SEM micrographs of the austenitic stainless steel corrosion in asphalt fumes
Dane BadawczeThe dataset contains the scanning electron microscopy (SEM) studies of the austenitic stainless steels: AISI 304, AISI 316, AISI 321 and duplex stainless steel AISI 2205. The samples were polished and exposed to the installation carrying asphalt fumes at elevated temperatures (approx. ~210-240 Celsius). The exposition duration was three months. Some...
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The XPS spectra of LSCNT sintered at 1200C
Dane BadawczeThe dataset includes XPS spectra of La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s sintered at various temperatures under air atmosphere for 12 h. Samples were produced using aqueous soft chemistry methods (Pechini). The XPS spectra were collected for all species.
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The XPS spectra of Al2O3/5%Cu prepared using wet impregnation method
Dane BadawczeThe dataset includes XPS spectra of Al2O3/5%Cu catalyst sintered under air atmosphere. Samples were produced using aqueous soft chemistry methods and incipient wettness impregnation using nitrate solution. The XPS spectra were collected for all species.
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The XPS spectra of AlOOH/1%Cu prepared using wet impregnation method
Dane BadawczeThe dataset includes XPS spectra of AlOOH/1%Cu catalyst sintered under air atmosphere. Samples were produced using aqueous soft chemistry methods and incipient wettness impregnation using nitrate solution. The XPS spectra were collected for all species.
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The XPS spectra of ZrO2/5%Cu prepared using wet impregnation method
Dane BadawczeThe dataset includes XPS spectra of ZrO2/5%Cu catalyst sintered under air atmosphere. Samples were produced using aqueous soft chemistry methods and incipient wettness impregnation using nitrate solution. The XPS spectra were collected for all species.
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The XPS spectra of CeO2/5%Cu prepared using wet impregnation method
Dane BadawczeThe dataset includes XPS spectra of CeO2/5%Cu catalyst sintered under air atmosphere. Samples were produced using aqueous soft chemistry methods and incipient wettness impregnation using nitrate solution. The XPS spectra were collected for all species.
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The XPS spectra of SrTiO3/5%Cu prepared using wet impregnation method
Dane BadawczeThe dataset includes XPS spectra of SrTiO3/5%Cu catalyst sintered under air atmosphere. Samples were produced using aqueous soft chemistry methods and incipient wettness impregnation using nitrate solution. The XPS spectra were collected for all species.
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The XPS spectra of AlOOH/5%Cu prepared using wet impregnation method
Dane BadawczeThe dataset includes XPS spectra of AlOOH/5%Cu catalyst sintered under air atmosphere. Samples were produced using aqueous soft chemistry methods and incipient wettness impregnation using nitrate solution. The XPS spectra were collected for all species.
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A multi-analytical approach to the characterization of natural organic dyestuffs and inorganic substrates present in the 19th-century artistic oil paints manufactured by a French art materials supplier Richard Aines
PublikacjaThis paper presents a comprehensive analysis of artistic paints produced in the 19th century by a French art materials supplier Richard Ain`es. Improved mild extraction with hydrofluoric acid enabled the observation of intact organic dyes. Reversed-phase liquid chromatography with diode-array and mass spectrometry detection was utilised for the identification of 35 dyes present in yellow and red paint samples, and in selected plant...
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Study of the influence of the presence of Dr fimbriae on the sedimentation of recombinant Escherichia coli strains: AAEC191A and BL21(DE3)
Dane BadawczeCell sedimentation in the medium is a common phenomenon in most bacterial enviroments. This study specifically investigated the impact of Dr fimbriae presence on cell deposition. To explore this, recombinant Escherichia coli strains were employed, including BL21(DE3)/pCC90, BL21(DE3)/pACYCpBAD, BL21(DE3)/pCC90 Dra D-mut, BL21(DE3)/pCC90 D54-STOP, AAEC191A/pCC90,...
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Tax system in Poland - current situation and direction of changes
Dane BadawczeThe study conducted on a group of 259 entrepreneurs from various regions of Poland concerns the opinions of business owners on the current tax situation, as well as potential changes in the tax system.
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Why does the Agile leader mindset matter the most?
Dane BadawczeThe literature widely states that agility is not as much an issue of the technological-methodological management approach as it is an issue of an employee’s mindset. Given that leaders play a pivotal role in any organization, this study underscores the crucial role of the agile mindset of leaders. It aims to uncover how agile mindset leaders influence...
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Novel Desorber for Online Drilling Mud Gas Logging
PublikacjaThis work presents the construction solution and experimental results of a novel desorber for online drilling mud gas logging. The traditional desorbers use mechanical mixing of the liquid to stimulate transfer of hydrocarbons to the gaseous phase that is further analyzed. The presented approach is based on transfer of hydrocarbons from the liquid to the gas bubbles flowing through it and further gas analysis. The desorber was...
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Application of dynamic headspace and gas chromatography coupled to mass spectrometry (DHS-GC-MS) for the determination of oxygenated volatile organic compounds in refinery effluents
PublikacjaThe paper presents a new procedure for the determination of oxygenated volatile organic compounds (O-VOCs) in postoxidative effluents from the production of petroleum asphalt using dynamic headspace coupled to gas chromatography-mass spectrometry in the selected ion monitoring (SIM) mode (DHSGC-MS). Among the GC capillary columns tested, a polar SLB-IL111 column with the ionic liquid stationary phase was found to be superior due...
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The voltage across and current through the RC model object tested using pulse excitation in impedance spectroscopy measurement method
Dane BadawczeThe raw data (voltage across and current through RC model object ) obtained using pulse excitation EIS impedance spectroscopy measurement method. The data was acquired using 12-bit ADC (LTC1420) with sampling frequency changed in time segments. The 1V voltage pulse excitation duration was set to 0.1s and the total acqusition time was set to 1000s. For...