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Wyniki wyszukiwania dla: microextraction techniques
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Structural and Material Determinants Influencing the Behavior of Porous Ti and Its Alloys Made by Additive Manufacturing Techniques for Biomedical Applications
PublikacjaOne of the biggest challenges in tissue engineering is the manufacturing of porous structures that are customized in size and shape and that mimic natural bone structure. Additive manufacturing is known as a sufficient method to produce 3D porous structures used as bone substitutes in large segmental bone defects. The literature indicates that the mechanical and biological properties of scaffolds highly depend on geometrical features...
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Comparative Study on Assisted Solvent Extraction Techniques for the Extraction of Biologically Active Compounds from Sideritis raeseri and Sideritis scardica
PublikacjaThe plants in the Sideritis genus are postulated to exhibit several important medicinal properties due to their unique chemical composition. To isolate the targeted phytochemical compounds, the selection of a suitable extraction method is of primary importance. In this work, a comparative study on the phytochemical profiles of various Sideritis raeseri and Sideritis scardica extracts has been carried out. An untargeted metabolomics...
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Miniaturized solid phase extraction techniques for different kind of pollutants analysis: State of the art and future perspectives – PART 2
PublikacjaDetermination of pollutants present in environmental samples at a low concentration level very often requires the analytical protocol that includes analytes isolation and/or enrichment prior to the final quantification. Miniaturized SPE offers an interesting alternative to LLE. Nowadays, many types of sorbents are available and can be used as selective materials for extraction of varied analytes in different kinds of samples. The...
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Mapping of Flood-Prone Areas Utilizing GIS Techniques and Remote Sensing: A Case Study of Duhok, Kurdistan Region of Iraq
PublikacjaOne of the most common types of natural disaster, floods can happen anywhere on Earth, except in the polar regions. The severity of the damage caused by flooding can be reduced by putting proper management and protocols into place. Using remote sensing and a geospatial methodology, this study attempts to identify flood-vulnerable areas of the central district of Duhok, Iraq. The analytical hierarchy process (AHP) technique was...
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Application of INAA and ETAAS techniques for human samples analysis in evaluation of the impact of Gdansk Phosphatic Fertilizer Plant on its workers
PublikacjaW pracy przedstawiono wyniki badań wpływu Gdańskich Zakładów Nawozów Fosforowych na zdrowie pracowników. Oznaczano stężenia (techniką INAA) Al, As,Au, Br, Ca, Cl, Cu, Dy, I, In, K, La, Mg, Mn, Mo, Na, S, Sb, Sm, Ti, U, V,W, Zn we włosach, paznokciach i filtrach z pyłem zebranych od 21 pracowników fabryki oraz 5 osób z grupy kontrolnej nie związanej z zakładem. Ponadto oznaczono Cd, Cr, Cu, Fe, Mo, Ni i Zn w moczu przy użyciu...
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Simplified simulation technique of rotating, induction heated, calender rolls for study of temperature field control
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Time Delay Estimation in Two-Phase Flow Investigation Using the γ-Ray Attenuation Technique.
PublikacjaTime delay estimation is an important research question having many applications in a range of technologies. Measurement of a two-phase flow in a pipeline or an open channel using radioisotopes is an example of such application. For instance, the determination of velocity of dispersed phase in that case is based on estimation of the time delay between two stochastic signals provided by scintillation probes. The proper analysis...
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New PCR test for detection of Candida glabrata based on the molecular target chosen by the RAPD technique
PublikacjaRapid, reliable diagnosis is a necessary condition for the successful treatment of infections. Such diagnostic assays are continually being developed. #e paper presents a method for selecting the molecular target for PCR-based diagnostics based on the comparison of RAPD patterns. A sequence encoding Candida glabrata CBS138 hypothetical protein was selected. The limit of detection for PCR and real-time PCR reactions with DNA extracted...
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A Novel Coupling Matrix Synthesis Technique for Generalized Chebyshev Filters With Resonant Source–Load Connection
PublikacjaThis paper reports a novel synthesis method for microwave bandpass filters with resonant source–load connection. In effect, a network realizing N+1 transmission zeros (where N is the number of reflection zeros) is obtained. The method is based on a prototype transversal coupling matrix (N+2, N+2) with source and load connected by a resonant circuit formed by a capacitor in parallel with a frequency-invariant susceptance. To complement...
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Hybrid Technique Combining the FDTD Method and Its Convolution Formulation Based on the Discrete Green's Function
PublikacjaIn this letter, a technique combining the finite-difference time-domain (FDTD) method and its formulation based on the discrete Green's function (DGF) is presented. The hybrid method is applicable to inhomogeneous dielectric structures that are mutually coupled with wire antennas. The method employs the surface equivalence theorem in the discrete domain to separate the problem into a dielectric domain simulated using the FDTD method...
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Application of passive sampling technique in monitoring research on quality of atmospheric air in the area of Tczew, Poland.
PublikacjaThis paper presents the results of atmospheric air quality research in Tczew (adjacent to the Vistula River) on the content of BTEX compounds. Analytical procedure applied during the sampling of the analytes from the air used the passive sampling technique (diffusive passive sampler, Radiello®). For determination of BTEX compounds in atmospheric air, two-stage thermal desorption technique combined with gas chromatography (TD-GC-FID)...
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Liquid crystal technique application for heat transfer investigation in afin-tube heat exchanger element
PublikacjaPublikacja przedstawia rezultaty prac autorów w zakresie wykorzystania termografii ciekłokrystalicznej w badaniach wymiany ciepła dla różnych elementów wymienników ciepła. Technika ta z powodzeniem została zastosowana do analizy zabudowy wymiennika na jego efektywność.
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Liquid crystal technique application for heat transfer investigation inafin-tube heat exchanger element
PublikacjaPublikacja przedstawia rezultaty prac autorów w zakresie wykorzystania techniki ciekłokrystalicznej w badaniach wymiany ciepła dla elementów wymiennika ciepła. Technika ta z powodzeniem została zastosowana do analizy sposobu zabudowy wymiennika na jego efektywność.
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Usefulness of the PCR technique for bacterial DNA detection in blood of the patients after ''oppened heart'' operations.
PublikacjaOperacje kardiochirurgiczne w krążeniu pozaustrojowym (KPU) poprzez ogromny uraz, powodowanie występowania zaburzeń odporności oraz uszkodzenie barier anatomicznych stwarzają sytuację wybitnie sprzyjającą rozwojowi powikłań infekcyjnych u tych chorych. Prowadzenie terapii antybiotykowej profilaktycznej i leczniczej, a także selektywna dekontaminacja przewodu pokarmowego może utrudniać i przedłużać czas rozpoznania obecności bakterii...
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Measurements of glucose content in scattering media with time-of-flight technique: comparison with Monte Carlo simulations.
PublikacjaZbadano możliwości pomiaru koncentracji glukozy w materiale silnie rozpraszającym światło z wykorzystaniem techniki czasu przelotu. Badania przeprowadzono wykorzystując ''Intralipid'' będącym fantomem tkanki. Stężenie glukozy wynosiło 100, 200, 300, 500, 1000, 2000,4000 lub 8000 mg/dl. Wyniki pomiarów porównano z wynikami uzyskanymi na drodze modelowania matematycznego.
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Determination of pesticides in water using new solid phase extraction technique - speedisk and speedisk column.
PublikacjaW publikacji opisano zastosowanie nowych narzędzi do ekstrakcji do fazy stałej: szybkie dyski i szybkie kolumienki (speedisk i speedisk column). Zaprezentowano ich zastosowanie do ekstrakcji pestycydów z próbek wody, przy zastosowaniu różnych rozpuszczalników.
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Critical evaluation of employment possibilities of OTT technique for isolation of the PAHs and PCBs from samples of water
PublikacjaW pracy przedstawiono krótki przegląd technik wykorzystywanych na etapie izolacji i/lub wzbogacania analitów z grupy WWA i PCB z próbek wody. W części doświadczalnej dokonano oceny możliwości wykorzystania krótkiego odcinka kapilarnej kolumny chromatograficznej jako pułapki sorpcyjnej na etapie izolacji i wzbogacania analitów z grupy WWA i PCB z próbek wody. Ponadto przedstawiono wpływ zjawiska sorpcji analitów na ściankach używanych...
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Satellite Laser Ranging technique as a tool for the determination of the Schwarzschild, de Sitter and Lense-Thirring effects
PublikacjaSatellite Laser Ranging (SLR) is a modern technique used in various research areas and applications related to geodesy and geodynamics. It is commonly used for tasks such as establishing the International Terrestrial Reference Frame (ITRF), monitoring Earth Orientation Parameters (EOP), determining the geocenter, measuring fundamental physical constants, calibrating microwave tracking techniques, conducting time transfer experiments,...
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Simple screening technique for determination of adsorbed and absorbed mercury in particulate matter in atmospheric and aquatic environment
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The analysis of human leukocyte antigen‐G level in patients with endometrial cancer by Western blot technique
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Reactions of NO2 with chromium(III) complexes with histamine and pyridoxamine ligands studied by the stopped-flow technique
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Quantitative determination of diazepam, nitrazepam and flunitrazepam in tablets using thin-layer chromatography–densitometry technique
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CdS thin films obtained by thermal treatment of cadmium(II) complexprecursor deposited by MAPLE technique
PublikacjaCienkie warstwy kompleksu [Cd{SSi(O-But)3}(S2CNEt2)]2 zostały osadzone na podłożach Si przy użyciu techniki MAPLE (ablacja laserowa z zamrożoną matrycą). Otrzymanie warstw CdS było możliwe dzięki zastosowaniu obróbki termicznej podłoży z naniesionym prekursorem. Powierzchnia filmów była analizowana pod kątem morfologii przy użyciu mikroskopii sił atomowych (AFM) oraz pomiarów elipsometrycznych (SE).
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Construction and Validation of Simulation Models of Samples Made from 316L Steel by Applying Additive Technique
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CrossTalk opposing view: Which technique for controlling resistant hypertension? Carotid chemoreceptor denervation/modulation
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Immobilization technique for enhanced production of the immunosuppressant mycophenolic acid by ultraviolet and gamma-irradiated Penicillium roqueforti
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Analysis of Floodplain Inundation Using 2D Nonlinear Diffusive Wave Equation Solved with Splitting Technique
PublikacjaIn the paper a solution of two-dimensional (2D) nonlinear diffusive wave equation in a partially dry and wet domain is considered. The splitting technique which allows to reduce 2D problem into the sequence of one-dimensional (1D) problems is applied. The obtained 1D equations with regard to x and y are spatially discretized using the modified finite element method with the linear shape functions. The applied modification referring...
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Greedy Multipoint Model-Order Reduction Technique for Fast Computation of Scattering Parameters of Electromagnetic Systems
PublikacjaThis paper attempts to develop a new automated multipoint model-order reduction (MOR) technique, based on matching moments of the system input–output function, which would be suited for fast and accurate computation of scattering parameters for electromagnetic (EM) systems over a wide frequency band. To this end, two questions are addressed. Firstly, the cost of the wideband reduced model generation is optimized by automating a...
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Evaluation of Ambient Air Odour Quality in Vicinity of Municipal Landfill Using Electronic Nose Technique
PublikacjaThe paper presents the results of investigation on ambient air quality evaluation with respect to concentration of odorants in a vicinity of municipal landfill. The investigation was carried out with a prototype of electronic nose and a team of panelists utilizing the Nasal Ranger field olfactometers. The prototype was equipped with a set of six semiconductor sensors by FIGARO Co. and one PID-type sensor. Performed measurements...
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IDENTIFICATION OF ODOR OF VOLATILE ORGANIC COMPOUNDS USING CLASSICAL SENSORY ANALYSIS AND ELECTRONIC NOSE TECHNIQUE
PublikacjaThe paper compares two methods of analysis of odour of volatile organic compounds: classical sensory analysis and electronic nose technique. Eight volunteers participated in the classical sensory analysis investigations, which lasted two weeks. An instrumental odour analysis involved a prototype of 6-sensor electronic nose designed by the authors. The research performed with this device provided higher reproducibility and reliability...
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A 3D-FEM mesh technique for fast analysis of waveguide problems containing rotatable tuning elements
PublikacjaIn this paper a meshing technique for 3D Finite Element Method is presented. It allows for fast analysis and optimization of the waveguide structures, which contain rotatable tuning elements. In the proposed procedure a thin layer of varying cylindrical mesh buffer is introduced in order to reuse unchanged mesh and FEM matrices in the rest of the domain.
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The Thin-Layer Microchromatography (μTLC) and TLC–FID Technique as a New Methodology in the Study of Lubricating Oils
PublikacjaThis paper concerns the possibility of using TLC coupled with a flame ionization detector (FID) and micro-TLC (μTLC) as precursors for microfluidized devices of analytical techniques to identify and determine the presence and content of the petroleum/vegetable oil base in the lubricating oils applied in cutting devices (chainsaws). This research is related to the problem of ensuring, in compliance with the requirements of environmental...
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Neutral point balancing technique for 3-level neutral point clamped converter with servo system
PublikacjaNeutral point voltage drift compensation technique in 3-level NPC multilevel converter and servo system is described in the paper. Analytical expressions are obtained for power subsystem elements parameters of servo drive system. Simulation of servo system, based on PMSM motor with 3-level NPC converter is considered.
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Relationship between heavy metal distribution in sediment samples and their ecotoxicity by the use of the Hasse diagram technique
PublikacjaOpisane badania wskazują, że istnieje nowe podejście oszacowywania ryzyka zanieczyszczenia określonych przedziałów środowiska morskiego dzięki równoczesnemu monitorowaniu zawartości metali ciężkich i parametrów ekotoksykologicznych. Rutynowe podejście stosuje oddzielnie wskaźniki zawartości metali ciężkich i wskaźniki ekotoksykologiczne w celu wykrycia zależności między poziomami zawartości metali ciężkich a mierzalnymi parametrami...
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Green energy extraction for sustainable development: A novel MPPT technique for hybrid PV-TEG system
PublikacjaThe Photovoltaic (PV) module converts only a small portion of irradiance into electrical energy. Most of the solar energy is wasted as heat, resulting in a rise in PV cell temperature and a decrease in solar cell efficiency. One way to harvest this freely available solar thermal energy and improve PV cell efficiency is by integrating PV systems with thermoelectric generators (TEG). This cogeneration approach of the hybrid PV-TEG...
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Driving Performance Indicators of Electric Bus Driving Technique: Naturalistic Driving Data Multicriterial Analysis
PublikacjaThe issue of electric energy saving in public transport is becoming the key area of interest. By improving of driving techniques and the implementation of eco-driving, it is possible to save electric energy. Systems that help to decrease energy consumption and to reduce fuel emissions are becoming popular in vehicles powered by diesel engines. However, these methods have not yet gained popularity in electric vehicles. Therefore,...
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La construction d`une chambre d`etalonnage a l`Universite Technique de Gdańsk.
PublikacjaOmówiono konstrukcję stanowiska badawczego komory kalibracyjnej. Przedstawiono stosowane warunki brzegowe z systemem sterowania oraz kalibrację pływakowych czujników przemieszczeń. Podano sposób formowania masywu gruntowego.
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Chromatic monitoring technique for thickness measurementof thin transparent films.IV Workshopon Atomic and Molecular Physics.
PublikacjaW pracy opisano nową technikę monitorowania grubości cienkich warstw podczas procesu ich syntezy. Jest to optyczna metoda oparta na zdegenerowanej analizie widmowej tzw. modulacji chromatycznej. Umożliwia ona precyzyjny ciągły pomiar zmian grubości wzrastających warstw stosowanych w optyce.
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Improved energy management technique in pipe-embedded wall heating/cooling system in residential buildings
PublikacjaEffective and environmentally responsive techniques of energy management in residential buildings are desirable for the resulting reduction of energy costs and consumption. In this paper, an improved and efficient technique of energy management in pipe-embedded wall heating/cooling systems, called the Thermal Barrier, is described. Specifically, the Thermal Barrier is a technique focused on the management and control of heat...
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Improved energy management technique in pipe-embedded wall heating/cooling system in residential buildings
PublikacjaEffective and environmentally responsive techniques of energy management in residential buildings are desirable for the resulting reduction of energy costs and consumption. In this paper, an improved and efficient technique of energy management in pipe-embedded wall heating/cooling systems, called the Thermal Barrier, is described. Specifically, the Thermal Barrier is a technique focused on the management and control of heat supply...
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Development of an orbital shaker-assisted fatty acid-based switchable solvent microextraction procedure for rapid and green extraction of amoxicillin from complex matrices: Central composite design
PublikacjaIn this study, a cheap, fast and simple orbital shaker-assisted fatty acid-based switchable solvent microextraction (OS-FASS-ME) procedure was developed for the extraction of amoxicillin (AMOX) in dairy products, pharmaceutical samples and wastewater prior to its spectrophotometric analysis. Fatty acid-based switchable solvents were investigated for extracting AMOX. The key factors of the OS-FASS-ME procedure were optimized using...
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Investigation of vortex assisted magnetic deep eutectic solvent based dispersive liquid–liquid microextraction for separation and determination of vanadium from water and food matrices: Multivariate analysis
PublikacjaA new and simple vortex assisted magnetic deep eutectic solvent dispersive liquid–liquid microextraction procedure (VA-MDES-DLLME) was developed for the determination of vanadium (V) in food and water samples by flame atomic absorption spectrometry (FAAS). In the extraction medium, a bis(acetylpivalylmethane) ethylenediimine (H2APM2en) was used for the complexation of V(V) in sample solution at pH 6. The VA-MDES-DLLME was optimized...
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Application of headspace-solid phase microextraction followed by gas chromatography-mass spectrometry to determine short-chain monocarboxylic acids in cattle farm wastewater and waste landfill leachates
PublikacjaZaproponowano metodykę oznaczania krótkołańcuchowych kwasów monokarboksylowych w ściekach z hodowli bydła i odciekach ze składowisk zawierających organiczne odpady, oparta na technice mikroekstrakcji do fazy stacjonarnej z fazy nadpowierzchniowej próbek ciekłych, w połączeniu ze sprzężonym układem GC-MS.
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Green, simple analytical method for biogenic amines determination in fruit juice samples using salting-out assisted liquid-liquid microextraction and gas chromatography-mass spectrometry
PublikacjaSalting-out assisted liquid-liquid microextraction (SALLME) was integrated with the derivatization procedure to establish a one-step sample pre-treatment approach for rapid analysis of 14 biogenic amines (BAs) in fruit juices. The methodology consists of salting-out of analytes, derivatization with ethyl chloroformate (ECF), extraction with ethyl acetate (EtAc), and the analysis of the derivatized BAs using gas chromatography-mass...
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An air-assisted dispersive liquid phase microextraction method based on a hydrophobic magnetic deep eutectic solvent for the extraction and preconcentration of melamine from milk and milk-based products
PublikacjaIn the current research, a fast and sustainable air-assisted hydrophobic magnetic deep eutectic solvent-based dispersive liquid phase microextraction followed by UV–Vis spectrophotometry measurements was optimized for the extraction and determination of melamine in milk and milk-based products. The central composite design was applied for the optimization of factors affecting the recovery of melamine. Quantitative extraction of...
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Combination of homogeneous liquid–liquid extraction and vortex assisted dispersive liquid–liquid microextraction for the extraction and analysis of ochratoxin A in dried fruit samples: Central composite design optimization
PublikacjaThis paper presents a new analytical procedure based on combination of homogeneous liquid–liquid extraction (HLLE) and vortex-assisted dispersive liquid–liquid microextraction (VA-DLLME) for the accurate and reliable determination of ochratoxin A (OTA) in dried fruit samples. To enable selective extraction of the OTA, six hydrophobic deep eutectic solvents (hDESs) were prepared and tested as extraction solvents. Optimization of...
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Combination of High-Pressure Processing and Freeze-Drying as the Most Effective Techniques in Maintaining Biological Values and Microbiological Safety of Donor Milk
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Comparative Analysis of Different Spread-Spectrum Techniques for Reduction of Conducted Emissions Generated by Magnetic Resonant Wireless Power Transfer Systems
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PRESERVATION THROUGH DIGITIZATION - STANDARDIZATION IN DOCUMENTATION OF BUILD CULTURAL HERITAGE USING CAPTURING REALITY TECHNIQUES AND HERITAGE/HISTORIC BIM METHODOLOGY
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Origin of bitumen fractions in the Jurassic-early Cretaceous Vaca Muerta Formation in Argentina: insights from organic petrography and geochemical techniques
PublikacjaThis paper investigates chemical functional groups of the two extracted bitumen fractions in shales of the Jurassic to early Cretaceous Vaca Muerta Formation of the Neuquén Basin in Argentina, South America. The results indicate that Bitumen I is strongly aliphatic and appears to be genetically related to fluorescent amorphous organic matter. In contrast, Bitumen II consists of highly condensed, aromatic hydrocarbons, and has some...