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Wyniki wyszukiwania dla: MICROPOLAR SOLIDS
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Metal Supported Solid Oxide Fuel Cells - Selected Aspects
PublikacjaW artykule przedstawiono wyniki badań nad tlenkowymi ogniwami paliwowymi zbudowanymi na stalowym interkonektorze.
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Fabrication and characterization of anode supported solid oxide fuel cells
PublikacjaW tej pracy, napylanie aerozolowe zawiesiny proszków jest oceniane jako metoda osadzania cienkich elektrolitów tlenkowych ogniw paliwowych. Metoda ta jest tania, prosta i mam zalety w stosunku do szeroko stosowanej metody sitodruku. Wpływ parametrów osadzania: stężenie zawiesiny, ciśnienie robocze są w artykule omawiane.
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Solid Oxide Fuel Cells with Ni infiltrated perovskite anode
PublikacjaNiobium-doped strontium titanate was used as the anode for a solid oxide fuel cell. Electrolyte-supported cells were prepared with pure perovskite and composite perovskite–yttria–stabilized-zirconia (YSZ) anodes. Fuel cell tests demonstrated significant improvement in power density after infiltration with a small amount of Ni. The obtained values of power densities are comparable with conventional Ni/YSZ cermet anode. In addition,...
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Possibilities of radioisotope measuring in control of an unstable solid particles hydrotransport
PublikacjaThe paper presents γ-radiation proposal to control a multiphase flow, independently from circumstances. So this method may be applied even in compound industrial or environmental processes. Moreover in many cases, it is the only method for applications for dense mixture containing coarse angular grains. The constructed equipment allows continuous measurement of density as well as solid phase for both concentration and average velocity....
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Modern trends in solid phase extraction: New sorbent media
PublikacjaBased on the recently published literature, this review provides an update of the most important features and application of formats and devices employed in solid phase extraction (SPE). Special attention was paid on new trapping media proposed in SPE prior the chromatography analysis, based on the use of nanostructured materials, including carbon nanomaterials, electrospun nanofibers, dendrimes and magnetic nanoparticles, molecular...
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The effect of surfactants mixtures composition on wetting of different solid materials
PublikacjaThe wetting properties of surfactants mixtures were investigated. Three types of compounds were used: nonionic gemini α, α'-[2,4,7,9-tetramethyl-5-decyne-4,7-diyl]bis[ω-hydroxyl-olioxyethylene] (S-10), anionic sodium dodecyl sulphates (SDS) and cationic dodecyl trimethyl ammonium bromide (DTAB). The materials used in wetting experiments were steel and methyl polymethacrylate. These materials differ...
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Solid oxide fuel cells with Ni-infiltrated perovskite anode
PublikacjaWytworzono próbki na bazie tytanianu strontu domieszkowanego niobem i przebadano wpływ nasączania niklem na właściwości tych materiałów.
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A modern solid waste management strategy – the generation of new by-products
PublikacjaTo benefit the environment and society, EU legislation has introduced a ‘zero waste’ strategy, in which waste material should be converted to resources. Such legislation is supported by the solid waste hierarchy concept, which is a set of priorities in waste management. Under this concept, municipal solid waste plants (MSWPs) should be equipped with sorting and recycling facilities, composting/incineration units and landfill prisms...
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THE ROLE OF THIN FUNCTIONAL LAYERS IN SOLID OXIDE FUEL CELLS
PublikacjaWidespread commercialization of solid oxide fuel cells requires lowering its cost. It is generally accepted that to lower the cost of solid oxide fuel cells it is necessary to use metal alloys as interconnectors and, consequently, lower its operating temperature to slow down interconnectors degradation. As a result the area specific resistance of the cathodes should be lowered to sustain the performance of the cells. In order to...
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Ammonia Gas Sensors: Comparison of Solid-State and Optical Methods
PublikacjaHigh precision and fast measurement of gas concentrations is important for both understanding and monitoring various phenomena, from industrial and environmental to medical and scientific applications. This article deals with the recent progress in ammonia detection using in-situ solid-state and optical methods. Due to the continuous progress in material engineering and optoelectronic technologies, these methods are among the most...
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New Architecture of Solid-State High-Voltage Pulse Generators
PublikacjaThe application of the nanosecond pulsed electric field (nsPEF) for biomedical treatments has gained more interest in recent decades due to the development of pulsed power technologies which provides the ability to control the electric field dose applied during tests. In this context, the proposed paper describes a new architecture of solid-state high-voltage pulse generators (SSHVPG) designed to generate fully customised sequences...
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On rotational instability within the nonlinear six-parameter shell theory
PublikacjaWithin the six-parameter nonlinear shell theory we analyzed the in-plane rotational instability which oc- curs under in-plane tensile loading. For plane deformations the considered shell model coincides up to notations with the geometrically nonlinear Cosserat continuum under plane stress conditions. So we con- sidered here both large translations and rotations. The constitutive relations contain some additional mi- cropolar parameters...
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Paremetrization of sounds for recognizing hazarodus events
PublikacjaNowoczesne systemy monitoringu działają na zasadzie automatycznego wykrywania niebezpiecznych zdarzeń na podstawie analizy obrazu z kamer i dźwięku z mikrofonów. W niniejszej publikacji skupiono się na pierwszym etapie rozpoznawania zdarzeń dźwiękowych, jakim jest parametryzacja dźwięku. Podstawą do skutecznego działania systemu jest znalezienie parametrów, których zmienność najlepiej odzwierciedla cechy charakterystyczne dźwięku...
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Solid phase extraction of explosives on Ni-doped carbosils prepared by mechanochemistry
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High temperature corrosion of stainless steels for Solid Oxide Fuel Cells
PublikacjaW pracy przedstawiono wyniki korozyjności wysokotemperaturowej stali litych i porowatych stosowanych w tlenkowych ogniwach paliwowych.
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Investigation of sour substances by a set of all-solid-state membrane electrodes
PublikacjaTestowano elektrody typu all solid state (ASS) w roztworach elektrolitów zawierających substancje o smaku kwaśnym. Elektrody typu ASS zawierają dwa typy membran. Badano wpływ grubości membrany oraz stosunku związek lipofilowy/ chlorek poliwinilu na odpowiedzi elektrod. Stwierdzono, że grubość elektro aktywnego polimeru, nie ma wpływu na czułość i stabilność elektrod w przeciwieństwie do grubości membrany składającej się ze związku...
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Description of the silo flow and bulk solid pulsations detection using ECT
PublikacjaW artykule przedstawiono wyniki zastosowania tomografii pojemnościowej do analizy pulsacji występujących w bezkohezyjnym materiale sypkim podczas opróżniania silosu cylindrycznego. Przeanalizowano wpływ parametrów zmiennych (zagęszczenia początkowego, szorstkości ściany, prędkości opróżniania) na wielkość dynamicznych pulsacji)
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Ordered FePdCu nanoisland arrays made by templated solid-state dewetting
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From Hollow to Solid Carbon Spheres: Time-Dependent Facile Synthesis
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Chemical and thermal stability of core-shelled magnetite nanoparticles and solid silica
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Solventless sample preparation techniques based on solid- and vapour-phase extraction
PublikacjaThe main objective of this review is to critically evaluate recent developments in solventless sample preparation techniques. The potential of a variety of sample preparation techniques based on solid- and vapour-phase extraction techniques is evaluated. Direct thermal extraction and derivatization processes to facilitate the extraction of analytes in different areas are included. The applicability, disadvantages and advantages...
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Detection and classification of gaseous compounds by solid electrolyte cyclic voltammetry sensors
PublikacjaW pracy omówiono właściwości i ostatnie wyniki badań dotyczące czujników elektrokatalitycznych.
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A review of theoretical and practical aspects of solid-phase microextraction in food analysis.
PublikacjaSPME (mikroekstrakcja do fazy stacjonarnej) to szybka, nowoczesna technika przygotowania próbki do analizy. W niniejszej pracy dokonano przeglądu zastosowania techniki SPME do badania zanieczyszczeń żywności i analizy jej naturalnych składników. Praca zawiera również krótki teoretyczny opis zasad działania techniki SPME.
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Properties of a lithium solid electrolyte gas sensor based on reaction kinetics
PublikacjaW artykule przedstawiono zasadę działania, budowę i właściwości czujnika gazu na bazie elektrolitu stałego z mobilnymi jonami litu. Czujnik został przygotowany w technologii grubowarstwowej. Przedstawiono wyniki badań czujnika w mieszaninach gazów toksycznych.
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Triplet exciton interactions in solid films of an elektrophosphorescent Pt(II) porphyrin
PublikacjaW pracy pokazano, że fosforescencja porfiryny platynowej (PtOEP) jest wygaszana na skutek oddziaływania między monomerowymi i dimerowymi ekscytonami trypletowymi. Stała oddziaływania dla monomerowych ekscytonów trypletowych wynosi 8x10-12 cm3/s a dla ekscytonów dimerowych 8x10-15 cm3/s.
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Impedance Spectroscopy as a Diagnostic Tool of Degradation of Solid Oxide Fuel Cells
Publikacjaw pracy przedstawiono wyniki badań degradacji tlenkowych ogniw paliwowych przeprowadzone metodą spektroskopii impedancyjnej. Ogniwa paliwowe zostały przetestowane w eksperymentalnych warunkach, które pozwalają na uzyskanie szybkiego spadku wydajności ogniw paliwowych. impedancja i parametry uzyskane z dopasowania widm do elektrycznego obwodu zastępczego zostały skorelowane z poziomem degradacji elementów ogniw paliwowych - anody...
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Influence of anodes fabrication conditions on properties of solid oxide fuel cells
PublikacjaW pracy zamieszczono wyniki badań tlenkowych ogniw paliwowych różniących się warunkami przygotowania anody. Poszczególnego ogniwa różniły się ciśnieniem ściskania, temperaturą spiekania i składem anody.
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Construction and investigation of SO2 amperometric sensor with a solid polymer electrolyte membrane
Publikacjan this paper a sensor for detection of the sulphur dioxide based on three electrode cell configuration with a liquid electrolyte, a mercury sulphate reference electrode and a solid polymer electrolyte working electrode is presented. Working elec- trode was obtained by using Takenaka-Torikai chemical deposi- tion method by precipitation of Au particles into the pores of the Nafion membrane. Sensors characteristics measurements were...
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Is the Solid Electrolyte Interphase an Extra-Charge Reservoir in Li-Ion Batteries?
PublikacjaAdvanced metal oxide electrodes in Li-ion batteries usually show reversible capacities exceeding the theoretically expected ones. Despite many studies and tentative interpretations, the origin of this extra-capacity is not assessed yet. Lithium storage can be increased through different chemical processes developing in the electrodes during charging cycles. The solid electrolyte interface (SEI), formed already during the first...
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Evidence for solid state electrochemical degradation within a small molecule OLED
PublikacjaAcridone derivative have been synthesised and used as OLED (Organic Light Emitting Diode) emitters which were found to be electroactive. Electrochemical investigations showed a side reaction takes place inside an active layer which diminished the overall device efficiency. By using a dopant and host active layer architecture, the formation of the by product was removed. The by-product was identified as a σ-dimer formed inside an...
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RARE-EARTH ELEMENTS DOPING OF BARIUM CERATE AND ZIRCONATE SOLID SOLUTION
PublikacjaThe properties of doped barium cerate barium zirconate solid solution are presented in presented work. It was found that doping of solid solution of barium cerate and zirconate by rare-earth elements have an influence on microstructure and electrical properties of the samples.
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FURTHER REMARKS ON THE SURFACE VIS IMPRESSA CAUSED BY A FLUID-SOLID CONTACT
PublikacjaIt is well-known that, nano-mechanics should take into account not only physical phenomena occuring within the bulk but, first of all, the physical phenomena appropriate for a surface of two materials contact. The huge volume density of internal surfaces as well countours lines located within the nanomaterial results in our interest in, apart from classical form of mass, momentum and entropy transport, those modes of transportation...
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Potentiometric Solid-Contact Multisensor System for Simultaneous Measurement of Several Ions
PublikacjaThe design and performance of potentiometric multisensor system made in solid-contact technology is described. Both, the measuring electrodes as well as the reference electrode are in a compact cell. The system allows for simultaneous measurement of various ions. The characteristics of the electrodes for Na+, K+ and Ca2+ ions were determined using the designed system and compared with ISEs of the same membrane composition in classical...
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Preparation and characterization of asphaltene based adsorbents for gas-solid adsorption systems
PublikacjaThe dissertation presents results of the experimental research on asphaltene-based adsorbents (support coated with asphaltene layer) for gas-solid adsorption systems, with special reference to volatile organic compounds (VOCs) removal from gas streams. Analysis of gas adsorption properties revealed that asphaltenes isolated from oxidized bitumen have strong affinity toward VOCs. Interactions with target gas molecules, and selectivity...
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Enhanced energy conversion as a result of fluid-solid interaction in micro- and nanoscale
PublikacjaIt is known that nano- and micromechanics require new approaches to right describing of surface-like phenomena which lead to an enhanced energy conversion. In this work, a general form of surface forces that consist of a contribution from both the friction and mobility components has been extended to collect the effects of bulk and surface motion of a fluid. Quite similar impact can be observed for a solid-fluid mixture, where...
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Histaminol and Its Complexes with Copper(II) - Studies in Solid State and Solution
PublikacjaHistaminol [4(5)-(B-hydroxyethyl)imidazole, 4-(1H-imidazol-2-yl)ethanol, L] is an analogue of histamine and its minor metabolite. So far its properties have not been studied in detail due to the synthetic difficulties. Here, the structure and acid-base properties of histaminol, as well as the results of studies on its copper(II) complexes in solid state and aqueous solution are reported. Stability constants of the histaminol–CuII...
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Interface layers between electrolyte and cathodes for solid oxide fuel cells
PublikacjaW pracy przebadano możliwość zastosowania warstwy CGO ((CeO2)0.8 (Gd2O3)0.1) w tlenkowych ogniwach paliwowych. Do wytworzenia warstwy użyto pirolizy aerozolowej.
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Thin Layer Deposition Methods in Solid Oxide Fuel Cell Technology
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Infiltration - an alternative method to prepare composites for Solid Oxide Fuel Cells
PublikacjaPrzedstawiono różne techniki nasączania pozwalające na uzyskanie materiałów o mieszanym przewodnictwie jonowo-elektronowym do zastosowań w tlenkowych ogniwach paliwowych
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Stabilization of Solid Residues Obtained During Sewage Sludge Thermal Treatment
PublikacjaCurrently wastewater treatment plants are still dealing with the problem of ecological management of sewage sludge. Nowadays, thermal utilization is considered the most eco-friendly way of processing excess sludge. However, during mentioned process, fractions of ashes and dusts are generated. Such wastes, especially dusts fraction, can be potentially harmful for the environment and wastes should be stabilized before further management....
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NANOCRYSTALLINE CATHODES FOR SOLID OXIDE FUEL CELLS MADE OF NOBLE METALS
PublikacjaCathodes for solid oxide fuel cells prepared by the infiltration method at 600 °C are presented. The infiltration method allows to produce stable, nanostructured electrodes. Cathodes were prepared using gold, platinum, La2NiO4+δ (L2N) and La0.6Sr0.4Co0.2Fe0.8O3 δ (LSCF). Symmetrical cathode/electrolyte/cathode samples were prepared and examined with SEM microscopy and electrochemical impedance spectroscopy. Despite successful deposition...
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Formation of intermetallic compounds in the solid-liquid composites of the Ga-Ni system
PublikacjaThe processes of formation of intermetallic compounds in the composite system of liquid gallium-nickel powder by the methods of x-ray diffraction, scanning electron microscopy and differential thermal analysis have been studied. A change in the phase composition was discovered and the influence of thermal treatment of the composites under investigation on the phase formation processes was analyzed. The mechanism of gallium enriched...
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Investigation of solid polymer electrolyte gas sensor with different electrochemical techniques
PublikacjaIn this work solid polymer electrolyte (SPE) amperometric sulphur dioxide sensor is investigated. Nafion was used as a membrane electrode and 1M sulphuric acid as an internal electrolyte. Sensor response to sulphur dioxide was measured. Besides traditional constant voltage amperometry also different electrochemical techniques were used. Results obtained by these methods are compared.
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Effect of interconnect coating procedure on solid oxide fuel cell performance
PublikacjaChromium (Cr) species vaporizing from chromia-forming alloy interconnects is known as a source of degradation in solid oxide fuel cell (SOFC) stacks called “cathode poisoning”. (Mn,Co)3O4 spinel coatings offer good protection against Cr evaporation during operation. In this study, Crofer 22 APU steel interconnects were electrophoretically deposited in different mediums to obtain high packing of green coating layer. The optimized...
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Magnetoelectric effect in (BiFeO3)x–(BaTiO3)1-x solid solutions
PublikacjaThe aim of the present work was to study magnetoelectric effect (ME) in (BiFeO3)x–(BaTiO3)1x solid solutions in terms of technological conditions applied in the samples fabrication process. The rapidly growing interest in these materials is caused by their multiferroic behaviour, i.e. coexistence of both electric and magnetic ordering. It creates possibility for many innovative applications, e.g. in steering the magnetic memory...
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Effect of bulk solid on strength of cylindrical corrugated silos during filling.
PublikacjaW artykule przedstawiono wyniki MES dla metalowych silosów z blachy falistej o kształcie cylindrycznym. Obliczenia wykonano podczas stanu napełnienia silosów z uwzględnieniem materiału sypkiego. Materiały sypki został opisany hipoplastycznym modelem konstytutywnym. W obliczeniach wzięto pod uwagę wstępne imperfekcje geometryczne. Wyniki porównano dla silosów pustych. Zaobserwowano pozytywny efekt obecności materiału sypkiego.
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Heavy metals partition between leachate and soilds the course of municipal sewage treatment.
PublikacjaAnalizowano zawarotści metali ciężkich w cieczy nadosadowej i zawiesinie w ściekach oraz osadach ściekowych po stabilizacji oraz odwadnianiu.Badania prowadzono w miejskiej oczyszczalni ścieków ''Wschód'' w Gdańsku.
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Experimental and first-principles studies of high-pressure effects on the structural, electronic, and optical properties of semiconductors and lanthanide doped solids
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Sano-Tachiya-Noolandi-Hong, Onsager and Braun models vs Monte Carlo simulation of charge photogeneration in organic solids
PublikacjaThe Sano-Tachiya-Noolandi-Hong (STNH), Onsager, and Braun models as well as Monte Carlo (MC) simulations of charge recombination/separation have been applied for the first time to reproduce the results of the electromodulated photoluminescence measurements in vacuum-evaporated films of fluorescent materials commonly used in optoelectronic devices. The values of the electron-hole pair final recombination speed in the monomer emitters:...
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Wilms’ tumour-the reality of tissue analysis in the Polish Paediatric Solid Tumours Group
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