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Thermodynamic Properties of Inorganic Salts in Nonaqueous Solvents. VI. Apparent Molar Volumes, Expansibilities, and Compressibilities of Divalent Transition Metal Ions in Methanol and Dimethylsulfoxide
PublikacjaThe temperature dependence of the density of divalent transition metal perchlorates in dimethylsulfoxide as well as cobalt(II), nickel(II) perchlorates, and copper(II) trifluoromethanesulfonate in methanol was determined. Moreover, sound velocities for solutions of cobalt(II), nickel(II) perchlorates, and copper(II) trifluoromethanesulfonate in methanol have been measured at 298.15 K. From these data, the partial molar volumes,...
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Corrosivity of environment and the current state of the steel elements at the former Auschwitz concentration camp
PublikacjaThe objective of this study was to assess corrosivity of the atmospheric environment in the former Auschwitz I and Auschwitz II-Birkenau concentration and extermination camp, and to identify the protective properties of existing corrosion products in order to estimate the actual corrosion rate of original steel elements located there. The current atmospheric corrosivity of the former Auschwitz camp, specified during one year of exposure...
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Naphthyl-vs. anthrylpyridine-2,6-dicarboxamides in cation binding studies. Synthesis and spectroscopic properties
PublikacjaPyridine-2,6-carboxamides bearing - or -naphthyl- and - or -anthryl- residues were prepared using simple method from pyridine-2,6-carboxylic acid dichloride and the respective aromatic amines. For the obtained receptors selective binding of lead(II), and copper(II) was found. Ion-receptor interactions were studied using UV-vis spectroscopy, spectrofluorimetry, 1H NMR, and FTIR spectroscopy. The reversible lead(II) and copper(II)...
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Cover Feature: Anilate Tethered Neutral Tetrahedral Pd(II) Cages Exhibiting Selective Encapsulation of Xylenes and Mesitylene (Chem. Eur. J. 19/2020)
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Front Cover: Chiral Molecular Cages Based on Cyclotriveratrylene and Sucrose Units Connected with p ‐Phenylene Linkers (Eur. J. Org. Chem. 6/2021)
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Organic-inorganic composites consisted of poly(3,4-ethylenedioxythiophene)and Prussian Blue analogues
PublikacjaThe organic-inorganic material consisted of poly(3,4-ethylenedioxythiophene) (pEDOT) and copper hexacyanoferrate (Cuhcf) was synthesized. The pEDOT film with Fe(CN)63−/4− as counter-ions potentiodynamically polarized in aqueous CuCl2 electrolyte brings about stable hybrid material (pEDOT/Cuhcf) performing single redox activity of FeII/III at a formal potential Ef = 0.61 V (vs. Ag/AgCl/0.1 M KCl) and less clearly shaped two redox...
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Properties of surface layers of duplex stainless steel after burnishing processes
PublikacjaStress corrosion cracking resistance of cold worked layers of 25 Cr duplex stainless steel grade UR52N+ has been investigated. The surface layers were performed through burnishing treatment. The residual stresses at surface layers were determined using grazing angle incidence X-ray diffraction method (g-sin2 Ψ). Corrosion tests were performed with the use of Slow Strain Rate Test technique in boiling 35% MgCl2 solution. It has...
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New Method of Non-Linear Electrochemical Impedance Spectroscopy with an Amplitude-Modulated Perturbation Signal
PublikacjaThe paper presents a new method of non-linear electrochemical impedance spectroscopy (NLEIS), which allows fast and nondestructive evaluation of the corrosion rate and determination of the Tafel coefficients values for a corrosion system under investigation. This method employs amplitude modulation of the ac perturbation signal. The study demonstrated that it was possible to obtain impedance characteristic as a function of the...
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Electrochemical investigations on corosivity of de-icing liquids for railway infrastructure
PublikacjaThe paper presents the results of electrochemical tests of the de-icing fluid for railway infrastructure. DC and AC electrochemical tests were performed to determine the corrosion rates of structural steel, cast iron and aluminium in the newly produced fluid. The results were compared with the corrosion rates of the same materials in the fluid without corrosion inhibitors. The obtained test results indicate a low corrosion risk...
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A Review on Deactivation and Regeneration of Catalysts for Dimethyl Ether Synthesis
Publikacjahe deactivation of catalysts and their regeneration are two very important challenges that need to be addressed for many industrial processes. The most quoted reasons for the deterioration of dimethyl ether synthesis (DME) concern the sintering and the hydrothermal leaching of copper particles, their migration to acid sites, the partial formation of copper and zinc hydroxycarbonates, the formation of carbon deposits, and surface...
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Beata Krawczyk-Bryłka dr
OsobyPsycholog, doktor nauk humanistycznych w dziedzinie zarządzania, adiunkt w Katedrze przedsiębiorczości. 2018 - 2021: Kierownik projektu NCN: „Efektuacyjny model zespołu przedsiębiorczego. Jak działają przedsiębiorcze zespoły odnoszące sukces" od 2016: Quality Standards Lead filaru People management & personal development na studiach MBA Politechniki Gdańskiej 2008 – 2012: Prodziekan ds kształcenia Wzydziału Zarządzania i Ekonomii...
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Assessment of Trace Metals Leaching During Rainfall Events from Building Rooftops with Different Types of Coverage – Case Study
PublikacjaRunoff water is an important medium transporting various types of pollution originating from the atmosphere and washed out from roofing materials. The study presents a quality assessment of runoff from different roofs in the context of trace metal concentrations. The analysed rooftops were covered with copper, tar paper and ceramic tile. The quality of the rain water collected at the same time satisfies the demands of the first...
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Advanced numerical modelling for predicting residual compressive strength of corroded stiffened plates
PublikacjaAn advanced methodology for predicting the residual compressive strength of corroded stiffened plates is developed here using the non-linear finite element method. The non-uniform loss of a plate thickness is accounted for on a macro-scale. In contrast, mechanical properties are changed using the constitutive model to reflect the corrosion degradation impact on a micro-scale. Three different stiffened plate thicknesses are considered,...
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Influence of laser melting on surface layer properties of titanium alloy Ti6Al4V
PublikacjaIn time of rapid technology and medicine progress, implants are becoming more widely used in the human body, ranging from dental implants, stabilizing plates, screws, orthopaedic prostheses. For example, there are many types of hip prostheses used for hip replacement as well as various types of materials used for these orthopaedic prostheses. Properties of titanium alloys used in hip prostheses combined with good strength properties,...
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Reliability of Corroded Stiffened Plate Subjected to Uniaxial Compressive Loading
PublikacjaThe work is focused on the reliability of corroded stiffened plates subjected to compressive uniaxial load based on the progressive collapse approach as stipulated by the Common Structural Rules for Bulk Carriers and Oil Tankers, employing the limit state design. Two different cases have been investigated. In the first model, the corrosion degradation led to uniform thickness loss, whereas the mechanical properties were unchanged,...
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Zagrożenia korozyjne stali nierdzewnych w przemyśle spozywczym
PublikacjaPrzedstawiono przyczyny występowania zagrożeń korozyjnych stali nierdzewnych w przemyśle spożywczym. Szczegółowo omówiono mechanizm oraz sposób zapobiegania korozji wżerowej, szczelinowej oraz pękania korozyjnego. Zaprezentowano dokumentację fotograficzną omówionych typów korozji. Wskazano podstawowe problemy związane z doborem materiałów konstrukcyjnych do budowy instalacji w przemyśle spożywczym.
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Korozja w środowisku ropy naftowej. Czynniki i monitorowanie
PublikacjaPrzedstawiono analizy właściwości ropy naftowej z punktu widzenia zawartych w niej czynników korozyjnych oraz ich wpływu na korozję stali w trakcie procesu destylacji ropy naftowej. Krytycznej analizie poddane zostały możliwości oferowane przez współczesne techniki pomiarowe. Wskazano na istotność prowadzenia kompleksowego programu oceny ropy, monitorowania korozji oraz stosowania ochrony inhibitorowej w celu ochrony instalacji...
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Superconductivity in the superhard boride WB4.2
PublikacjaWe show that the superhard boride WB4.2 is a superconductor with a Tc of 2.05(5) K. Temperature-dependent magnetic susceptibility, electrical resistivity, and specific heat measurements were used to characterize the superconducting transition. The Sommerfeld constant γ for WB4.2 is 2.07(3) mJ mol−1 K−2 and the ΔC/γTc=1.56, which is somewhat higher than what is expected for weakly coupled Bardeen–Cooper–Schrieffer type superconductors....
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Ionic thermoelectric effect in Cu2-δSe during phase transition
PublikacjaThe ionic Seebeck coefficient was studied in copper selenide with Cu1.99Se, Cu1.95Se and Cu1.8Se stoichiometry which was synthesized with a melt crystallization method. To measure the ionic Seebeck coefficient of copper ions, 0.15C6H12N4CH3I + 0.85CuI solid-state electrolyte was prepared. Electrolyte layers were pressed with copper selenide powder into a sandwich-like structure. At the temperature of 410 K, the materials have ionic...
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Experimental and numerical investigations of ultimate strength of degradated structures
PublikacjaThe presented work investigates the corrosion influence on the structural behaviour of structural elements. Nine welded large-scale stiffened plates, and 30 standard small specimens have been subjected to the accelerated marine immersed conditions. After corrosion testing, the specimens have been accurately measured in terms of surface characteristics. The coupon specimens were furtherly subjected to tensile loading to develop...
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Cover Feature: Electronic Circular Dichroism Imaging (ECD i ) Casts a New Light on the Origin of Solid‐State Chiroptical Properties (Chem. Eur. J. 4/2022)
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Use of Impedance Spectroscopy to Characterize Lining Performance in Simulated Flue Gas Desulfurization Systems
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Nickel-nanodiamond coatings electrodeposited from tartrate electrolyte at ambient temperature
PublikacjaIn this study, nanocrystalline Ni and Ni-diamond coatings were obtained by electrodeposition from tartrate electrolyte at ambient temperature aiming at improving corrosion and wear properties of the material. The created surfaces were investigated with regard to microhardness, adhesion, wear- and corrosion-resistance. The various methods such as atomic force microscopy, scanning electron microscopy, electrochemical impedance spectroscopy...
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The Creation of an Antimicrobial Coating on Contact Lenses by The Use of Nanocopper
PublikacjaThe aim of the research was to creation an antimicrobial coating on contact lens and examine the ability of copper nanoparticles to decrease microbial adhesion and prevent the growth of bacteria. The creation was based on the immersion method in solution with dispersed nanoparticles of copper at concentration 200 pm. There were evaluated follows factors: time of immersion and base to dispersed nanoparticles. Three solutions: ethyl...
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Ion recognition properties of new pyridine-2,6-dicarboxamide bearing propeller-like pendant residues: multi-spectroscopic approach
PublikacjaThe synthesis and ion binding properties of new amide derived from propeller-like tris(2-pyridyl)amine and 2,6-pyridinedicarboxylic acid chloride were described. Amide binds divalent metal cations: copper(II), nickel(II), zinc(II), and lead(II) in acetonitrile. In acetonitrile:water mixture (9:1 v/v) amide interacts only with copper(II) and nickel(II) cations forming complexes of 1:1 stoichiometry. It was found that the introduction...
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The Effect of Full-Cell Impregnation of Pine Wood (Pinus sylvestris L.) on Changes in Electrical Resistance and on the Accuracy of Moisture Content Measurement Using Resistance Meters
PublikacjaThe impact of the full-cell impregnation of pine wood was investigated with respect to changes in electrical resistance and the accuracy of moisture content measurement. This study compared the resistance of impregnated and untreated pine timber harvested from the northern part of Poland (Pomeranian region). The wood was impregnated by the vacuum-pressure method. The preservative (TANALITH E 3475) and coloring (TANATONE 3950) agents...
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Reliability of acicular grindable thermocouples for transient temperature measurements at sliding contacts
PublikacjaAcicular grindable thermocouples represent an interesting and prospective technique of temperature measurements at sliding contacts. This study aimed at the investigation of their reliability and accuracy as applied to the friction materials of various classes in contact with steel. The tests were conducted on a pin-on-disc tribometer under stationary and transient regimes. The experimental results were validated by comparing the...
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Scanning electron microscopy studies of the weld decay on SS 304 of water supply pipeline
Dane BadawczeThis dataset contains micrographs made with scanning electron microscope (SEM) Hitachi S-3400N, of the weld decay for water supply system pipelines made of AISI 304 stainless steel. Within the dataset one can see the different corrosion mechanisms. The micrographs were made after the Strauss test (excluding pictures labeled as pits_in_HAZ, done without...
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Hydrogen effects in duplex stainless steel welded joints - electrochemical studies
PublikacjaIn this work results on the influence of hydrogen on passivity and corrosion resistance of 2205 duplex stainless steel (DSS) welded joints are described. The results were discussed by taking into account three different areas on the welded joint: weld metal (WM), heat-affected zone (HAZ) and parent metal. The corrosion resistance was qualified with the polarization curves registered in a synthetic sea water. The conclusion is that,...
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Janusz Smulko prof. dr hab. inż.
OsobyUrodził się 25 kwietnia 1964 r. w Kolnie. Ukończył w 1989 r. z wyróżnieniem Wydział Elektroniki Politechniki Gdańskiej, specjalność aparatura pomiarowa. Zajął II miejsce w konkursie Czerwonej Róży na najlepszego studenta Wybrzeża w 1989 r. Od początku kariery związany z Politechniką Gdańską: asystent (1989–1996), adiunkt (1996–2012), profesor nadzwyczajny PG (od 2012). Odbył staże naukowe w Texas A&M University (2003, NATO...
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Heat transfer enhancement of modular thermal energy storage unit for reversible heat pump cooperation
PublikacjaThe following article presents experimental comparison research on a hexagonal shelland-tube latent thermal energy storage (TES). Such shape of a shell was deliberately chosen instead of a cylindrical one due to its high modularity and with intent for future applications in automobiles (EV and PHEV) air conditioning systems (HVAC). Two geometries of helical coils, acting as tubes, were studied in this article. One was a simple...
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Wood Moisture-Content Measurement Accuracy of Impregnated and Nonimpregnated Wood
PublikacjaThe influence of the impregnation process of pine wood (Pinus sylvestris L.) samples on the electrical resistance changes and the moisture-content measurement accuracy is presented in this paper. In this study, the resistances of impregnated and nonimpregnated green pine timber harvested from northern Poland were compared. An impregnation method based on a vacuum-pressure chamber was used. Copper salts were applied as the impregnated...
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Magneto-thermal convection of low concentration nanofluids
PublikacjaThe main aim of this paper was to analyze possible utilization of the low concentration nanofluids and the magnetic field to enhance heat transfer. The studied fluids were based on water with an addition of copper particles (40-60 nm diameter). They belonged to the diamagnetic group of materials. As a first attempt to stated target the analysis of enclosure placed in the maximal value of square magnetic induction gradient was carried...
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Performance‐driven modeling of compact couplers in restricted domains
PublikacjaFast surrogate models can play an important role in reducing the cost of EM-driven design closure of miniaturized microwave components. Unfortunately, construction of such models is challenging due to curse of dimensionality and wide range of geometry parameters that need to be included in order to make it practically useful. In this letter, a novel approach to design-oriented modeling of compact couplers is presented. Our method...
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Preparation of nano-tubular oxide layers on titanium alloy Ti13Nb13Zr
PublikacjaThe article presents results of oxidation tests and corrosion investigations of titanium alloy Ti13Nb13Zr preformed at different conditions. The oxide layers have been formed using electrochemical method in 2M H3PO4 + 0,3% HF solution for 30 min. and 1h at 20V constant voltage. The corrosion tests heve been made with poteniodynamic method in Ringer's solution at pH ranged 3 and 7. It has been shown that the nano-oxide films, which...
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Metal dusting phenomena of 501 AISI furnace tubes in refinery fractional distillation unit
PublikacjaThe purpose of this investigation was to conduct the failure analysis of 501 AISI furnace tubes places before distillation column in fractional distillation unit. The investigated furnace tubes were planned to work for ten years however after just two years of exploitation <30% of the material left. The observed corrosion process had the intense and complex character. The well-adhered shiny black deposits and deep, round pits were...
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Numerical analysis of chip removing system operation in circular sawing machine using CFD software
PublikacjaPaper presents the analysis of the results of numerical simulations of the air flow process of wood chips removing system in the circular sawing machine. The attention is focused on the upper cover and bottom shelter of the chip removing system. Within the framework of the work a systematic numerical modeling of the air flow distribution in the cover and shelter during operation of the selected rotational speed of saw blade with...
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Anna Lisowska-Oleksiak prof. dr hab.
OsobyAnna Lisowska-Oleksiak, born in 1952, has been working at GUT since 1977. Currently is employed at the Faculty of Chemistry as a full professor. She was employed as a research assistant at the University of St Andrews in the group of C. A. Vincent and P.G. Bruce (1991-1994). She completed a two-month research internship in CEA Grenoble (2011). Anna Lisowska-Oleksiak obtained her MSc in chemistry at Nicolaus Copernicus University...
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Influence of sludge treatment processes on heavy metal speciation
PublikacjaSludge composition is depending on sewage quality and also affected by processing methods such as thickening, stabilization and dewatering. During those processes some of sludge's undesirable properties might be reduced or enhanced.The objective of the study is the assessment of the influence of sludge processing on selected heavy metals partitioning between phases (aqueous and particle) and sludge. Sludge from the WWTP in Gdansk...
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Degradation of protective coatings in steel chimneys of flue gas desulfurisation system
PublikacjaThis paper presents problems associated with corrosion of steel stacks and changes in philosophy of corrosion protection when implemented into flue gas desulphurization systems. In-situ tests were taken by means of electrochemical impedance spectroscopy at the stack which discharges flue gas before wet lime/limestone desulphurization. A very quick electrolyte absorption by the spherical infill vinylester coating was found using...
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Jan Hupka prof. dr hab. inż.
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Problemy z powłokami antykorozyjnymi na elementach wyposażenia obiektów mostowych
PublikacjaOpisano problem wadliwości zabezpieczenia antykorozyjnego w zakresie malarskich powłok ochronno-dekoracyjnych wykonywanych na stalowych elementach barier zabezpieczonych uprzednio poprzez ocynkowanie metodą zanurzeniową na gorąco. Wykorzystując przykłady pochodzące z różnych obiektów przedstawiono powtarzający się problem delaminacji powłok malarskich, niezależny od rodzaju zastosowanych wyrobów lakierniczych oraz znacznego rozwoju...
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Problemy z powłokami antykorozyjnymi na elementach wyposażenia obiektów mostowych
PublikacjaPrzedstawiono problem wadliwości zabezpieczenia antykorozyjnego w zakresie malarskich powłok ochronno - dekoracyjnych wykonywanych na stalowych elementach barier zabezpieczonych uprzednio poprzez ocynkowanie metodą zanurzeniową. Wykorzystując przykłady pochodzące z różnych obiektów przedstawiono powtarzający się problem delaminacji powłok malarskich, niezależny od rodzaju zastosowanych wyrobów lakierniczych oraz znacznego rozwoju...
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MINERAL CONTENT OF TREE SAP FROM THE SUBCARPATHIAN REGION
Publikacjabut also as medicinal substance in folk medicine. Traditionally, it was used to treat various conditions, mostly anaemia and chronic fatigue. This study has been designed to establish the content of metallic elements (sodium, potassium, calcium, magnesium, zinc and copper) in sap collected from eight different species (silver birch, downy birch, hornbeam, Norway maple, boxelder maple, black walnut, black alder and white willow)...
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Preparation and structure of nanocrystalline sol-gel derived Cu doped LiTi2O4 powders
PublikacjaAmong the spinel oxides materials, lithium titanate (Li1+xTi2-xO4 where 0 ≤ x ≤ 0.33) could be very interested from pratical applications point of view. Lithium titanate is a II type spinel oxide superconductor with relatively high (~13 K for x = 0) superconducting transition temperature Tc. Above Tc lithium titanate shows metallic behaviour and can be used e.g. as electrodes for rechargeable lithium-ion batteries. Since the discovery...
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Review of titanium and steel welding methods
PublikacjaThe paper presents review of methods of titanium and steel welding. On basis of professional literature it was stated that titanium can be joined with steel by means of explosive welding or brazing.Joining titanium with steel by TIG welding and friction welding methods is possible with the use of copper and tantalum or vanadium interlayer.
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Między spotkaniem a mijaniem. Rahel Varnhagen, Hannah Arendt, Judith Butler
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«Ciało» na wojnie. Wokół Soli ziemi Józefa Wittlina
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Praktyczne kompetencje cyfrowe
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Rest cure – XIX-wieczna terapia nudą Silasa Weira Mitchella w opowiadaniu „Żółta tapeta” Charlotte Perkins Gilman
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