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Wyniki wyszukiwania dla: MICROEXTRACTION TEHCNIQUES
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A hybrid speech codec employing parametric and perceptual coding techniques
PublikacjaW referacie przedstawiono hybrydowy kodek mowy dla zastosowan w komunikacji VoIP wykorzystujący kodowanie parametryczne i percetualne. Sygnał mowy jest dzielony na składowe dźwięczne, które podlegają kodowania perceptualnemu, składowe bezdźwięczne, które kodowane są metodą parametryczną oraz transjenty, które nie są kodowane żadną stratną metodą. Dodatkowo przedstawiono architekturę kodeka, w której perceptualnie kodowana i przesyłana...
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Sample preparation techniques for determination of pesticide residues in food samples
PublikacjaPesticides are very important in increasing the efficiency and quality of agricultural production. They are applied in many spheres of life, not only in agriculture, and their applications are expanding. Despite their numerous merits, pesticides are some of the most toxic substances contaminating our environment and have a negative impact on the human health. Properties of pesticides such as stability, ability to bioaccumulation...
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Selecting Requirements Documentation Techniques for Software Projects: a Survey Study
PublikacjaA significant number of techniques dedicated to requirements specification and documentation is described in the available sources. As there is no purpose to use all of them, a selection has to be made, taking into consideration the context of a given software project, for example its size, usage of agile approach or stakeholders' technical competency. This paper is intended to provide guidelines for such selection. We reviewed...
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Usability Techniques Possible to Use in Diagnostic Tools Interface Improvement
PublikacjaThe development of diagnostic tools has caused a rapid increase in the amount of information generated and presented, necessitating the use of computer displays as an interface to data presentation and the use of modern diagnostic tools. The paper presents methods for testing usability that can be used in designing and improving the quality of interfaces of modern diagnostic tools that use communication through graphical user interfaces.
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Techniques of acquiring additional features of the responses of individual gas sensors
PublikacjaGas sensors usually exhibit lack of selectivity, require fre quent calibration, exhibit drift of the response and a lot of factors, such as humidity or ambient temperature, influen ce their performance. Different approaches can be used to overcome this shortcomings. Building arrays of different sensors and usage of pattern recognition methods to analyze responses of elements...
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Evaluation of Selected UX Techniques by Product Managers - A Preliminary Survey
PublikacjaIn this paper we present the results of an opinion survey among 28 IT product managers who evaluated the subjective usefulness of 24 selected UX techniques to 6 IT product management tasks derived from ProdBOK®. We selected the UX techniques based on the literature review and 6 interviews with experienced IT product managers. Based on the survey results, we propose our recommendation of useful techniques for 5 of the 6 studied...
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Using wavelet techniques for multibeam sonar bathymetry data compression
PublikacjaMultibeam sonars are widely used in applications like high resolution bathymetry measurements or underwater object imaging. One of the significant problems in multibeam sensing of the marine environment is large amount of data which must be transmitted from the sonar processing unit to an operator station using a limited bit rate channel. For instance, such a situation would be in the case when the multibeam sonar was mounted on...
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Study on applicability of two modal identification techniques in irrelevant cases
PublikacjaStudy on applicability of two modal identification techniques in irrelevant cases is made in this paper. The following techniques are considered: Peak Picking based on correlation analysis (PP-CA), dedicated for ambient vibrations and Eigensystem Realization Algorithm (ERA), formulated for free decay vibrations investigation. Irrelevant cases are found when analyzed signals are different than recommended to a given technique. The...
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Cognitive Systems, Concepts, Processes, and Techniques for the Age of Industry 4.0
PublikacjaThe aim of this Guest Edition of Cybernetics and Systems is to present a wide-ranging scale of concepts and processes being currently researched, developed, and evaluated in real life settings in anticipation of incoming Industry 4.0 era. With the fourth industrial revolution expectation, the broad spectrum of cognitive approaches have emerged as an attempt to mimic and augment, in some way, human intelligence. Intelligence, in...
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Comparative analysis of various transformation techniques for voiceless consonants modeling
PublikacjaIn this paper, a comparison of various transformation techniques, namely Discrete Fourier Transform (DFT), Discrete Cosine Transform (DCT) and Discrete Walsh Hadamard Transform (DWHT) are performed in the context of their application to voiceless consonant modeling. Speech features based on these transformation techniques are extracted. These features are mean and derivative values of cepstrum coefficients, derived from each transformation....
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Methods of Assessing Degradation of Supercapacitors by Using Various Measurement Techniques
PublikacjaThis article presents the qualitative analyses of the construction of supercapacitor samples. The analyses are based on the suggested thermographic measurements as well as the technique of testing the inherent noise of the investigated element. The indicated assessment methods have been referred to the currently used parameters for the qualitative evaluation of supercapacitors. The approach described in this paper, which introduces...
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Molecularly imprinted polymers applied in capillary electrochromatography and electrophoresis techniques
PublikacjaMolecularly imprinted polymers (MIPs) are synthetic materials with predetermined selectivity for a particular analyte or group of structure-linked chemicals which make them an ideal separation component. The process of developing and applying new types of MIPs in the field of environmental analytical chemistry has been broadly discussedi n many scientific studies in recent years. The use of new types of MIP sorbents as unique sorption...
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Preparation and evaluation of solid-phase microextraction fibres based on functionalized latex nanoparticle coatings for trace analysis of inorganic anions
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Room temperature ionic liquid-based dispersive liquid–liquid microextraction of uranium in water samples before spectrophotometric determination
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APPLICATION OF RESPONSE SURFACE MODELING FOR OPTIMIZATION AND DETERMINATION OF MALONDIALDIALDEHYDE BY VORTEX-ASSISTED DISPERSIVE LIQUID-LIQUID MICROEXTRACTION AND GC-FID
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In-Syringe Dispersive Liquid-Liquid Microextraction Coupled with High- Performance Liquid Chromatography for Trace Analysis of Naphthalene Sulfonates in Seawater
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Application of response surface methodology to optimize solid-phase microextraction procedure for chromatographic determination of aroma-active monoterpenes in berries
PublikacjaMost of scientific papers concern the qualitative or semi-quantitative analysis of aroma-active terpenes in liquid food matrices. Therefore, the procedure based on solid-phase microextraction and comprehensive two-dimensional gas chromatography-time-of-flight mass spectrometry for determination of monoterpenes in fresh berries was developed. The optimal extraction conditions using divinylbenzene-carboxen-polydimethylsiloxane fiber...
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Optimization of vortex-assisted supramolecular solvent-based liquid liquid microextraction for the determination of mercury in real water and food samples
PublikacjaA novel method was developed for sample preparation for spectrophotometric determination of Hg(II) in water and food samples. The method was based on vortex-assisted supramolecular solvent-assisted liquid-liquid microextraction (VA-SUPRASs-LLME). Analytical parameters such as pH, chelating agent, solvent type and volume, vortex time and salting out effect were optimized. Surface and normal probability plots were drawn for the variables...
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Determination of volatile organic compounds in water samples using membrane-solid phase microextraction (M-SPME) (headspace version)
PublikacjaThe results of a study on the use of membrane-solid phase microextraction (M-SPME) for sampling volatile organic compounds (VOCs) from the headspace above the liquid medium are presented. The sampled VOCs were subsequently quantified by gas chromatography (GC). Two systems were compared in this study, i.e. a novel two-phase sorption system (M-SPME), and a commercial fibre. Headspace sampling using SPME was optimized with respect...
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Monolithic capsule phase microextraction prior to gas chromatography-mass spectrometry for the determination of organochlorine pesticides in environmental water samples
PublikacjaIn this study, a capsule phase microextraction (CPME) protocol followed by gas chromatography-mass spectrometry is proposed for the accurate and sensitive monitoring of organochlorine pesticides (OCPs) in environmental water samples. Different monolithic sol–gel encapsulated sorbents were compared and monolithic sol–gel poly(ethylene glycol)-based sorbent incorporated into porous microextraction capsules resulted in the highest...
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Ionogel sorbent coatings for determining organophosphorus and pyrethroid insecticides in water and fresh juice samples by headspace-solid phase microextraction
PublikacjaThe sol–gel method yielded three different ionogel sorbent coatings that were obtained based on a silica material containing ionic liquids (ILs) immobilized in its pores. Two ILs, triethylsulfonium bis(trifluoromethylsulfonyl) imide [Set3][TFSI] and 1-butyl-1-methylpiperidinium bis(trifluoromethylsulfonyl)imide [C4C1Pip][TFSI], as well as their equimolar mixture [Set3/C4C1Pip], were used to obtain ionogel fibers. The developed...
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Sciences et Techniques en Perspective
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IEE PROCEEDINGS-COMPUTERS AND DIGITAL TECHNIQUES
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CLINICAL TECHNIQUES IN SMALL ANIMAL PRACTICE
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International Journal of Computational Intelligence Techniques
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Operative Techniques in Thoracic and Cardiovascular Surgery
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Techniques in Hand and Upper Extremity Surgery
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Current Protocols in Essential Laboratory Techniques
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U.S. Geological Survey Techniques and Methods
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Journal of Laparoendoscopic & Advanced Surgical Techniques
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Rapid and sensitive determination of acrylamide in potato crisps using reversed-phase direct immersion single drop microextraction-gas chromatography
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Salt saturated single drop microextraction of gold from water samples and its determination by graphite furnace atomic absorption spectrometry
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Determination of selenium by X-ray fluorescence spectrometry using dispersive solid-phase microextraction with multiwalled carbon nanotubes as solid sorbent
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Ionogel fibres of bis(trifluoromethanesulfonyl)imide anion-based ionic liquids for the headspace solid-phase microextraction of chlorinated organic pollutants
PublikacjaIonogels, a family of hybrid materials in which ionic liquids (ILs) are confined in a sol–gel network, are receiving much attention in a variety of scientific and technological fields. In this work, ionogels derived from three different ILs based on the anion bis(trifluoromethanesulfonyl)imide (TFSI), namely 1-butyl- 3-methylpyridinium bis(trifluoromethanesulfonyl)imide ([C4C1Py][TFSI]), 1-butyl-1-methylpyrrolidinium bis(trifluoromethanesulfonyl)imide...
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Rapid Characterization of the Human Breast Milk Lipidome Using a Solid-Phase Microextraction and Liquid Chromatography-Mass Spectrometry-Based Approach.
PublikacjaHuman breast milk (HBM) is a biofluid consisting of various biomolecules such as proteins, lipids, carbohydrates, minerals and bioactive substances. Due to its unique and complex composition, HBM provides not only nutritional components required for the growth of the infant, but also additional protection against infections. Global insight into the composition of HBM is crucial to understanding the health benefits infants receive...
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A rapid dispersive liquid–liquid microextraction of antimicrobial onion organosulfur compounds in animal feed coupled to gas chromatography-mass spectrometry
PublikacjaA rapid analytical procedure is proposed for determining two antimicrobial onion organosulfur compounds, propyl disulfide (PDS) and propyl propane thiosulfonate (PTSO), in animal feed. The use of PTSO as a natural ingredient in animal feed is allowed due to its antimicrobial activity against pathogenic organisms. Two analytical methodologies using gas chromatography coupled to mass spectrometry (GC-MS) are compared. After the extraction...
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Method for the simultaneous determination of monoaromatic and polycyclic aromatic hydrocarbons in industrial effluents using dispersive liquid-liquid microextraction with GC-MS
PublikacjaWe present a new method for simultaneous determination of 22 monoaromatic and polycyclic aromatic hydrocarbons in postoxidative effluents from the production of petroleum bitumen using dispersive liquid-liquid microextraction coupled to gas chromatography and mass spectrometry. The eight extraction parameters including the type and volume of extraction and disperser solvent, pH, salting out effect, extraction and centrifugation...
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Miniaturized, green salting-out liquid–liquid microextraction coupled with GC–MS used to evaluate biogenic amines in wine samples
PublikacjaMonitoring of the biogenic amines (BAs) content in food products, including wine, is important due to the health and safety of consumers and from the quality control point of view. In a given study, simultaneous derivatization and salting-out liquid–liquid microextraction (SALLME) coupled with GC–MS for BAs determination from wine samples was developed. For the optimization the Box-Behnken design was applied, where three independent...
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Ultrasound-Assisted Dispersive Liquid-Liquid Microextraction Using Deep Eutectic Solvents (DESs) for Neutral Red Dye Spectrophotometric Determination
PublikacjaDeep eutectic solvents (DES), which have low toxicity and are low cost, biodegradable, and easily synthesized, were used for the extraction of neutral red (NR) dye before its spectrophotometric analysis. DES, containing choline chloride as a hydrogen bond acceptor and phenol as a hydrogen bond donor with a molar ratio of 1:2, was used for the extraction of NR dye from aqueous media. The possible interaction of different DESs with...
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Chapter 6 : Non-intrusive measurement techniques in bubble dynamics investigation
PublikacjaPrzedstawiono wyniki badań dynamiki pęcherzyków parowych i gazowych przy użyciu nieinwazyjnych metod optycznych i akustycznych.
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Assessment of river water quality in the South Baltic coast by multivariate techniques
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Shaping coherence function of sources used in low-coherent measurement techniques
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Shaping coherence function of sources used in low-coherent measurement techniques
PublikacjaW niskokoherencyjnych technikach pomiarowych kształt funkcji koherencji wykorzystywanego źródła ma bezpośredni wpływ na parametry metrologiczne układu pomiarowego. Z tego względu, w wielu aplikacjach niezbędne jest użycie metod pozwalających na zmianę kształtu tej funkcji. W artykule przeanalizowano możliwości kształtowania funkcji koherencji, a przedstawione analizy teoretyczne i wyniki symulacji komputerowych wskazują, że kształtowanie...
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Modern techniques of sample preparation for determination of organic analytes by gas chromatography
PublikacjaW pracy dokonano przeglądu szerokiego spektrum technik przygotowania próbki, ze szczególnym uwzględnieniem technik o charakterze prośrodowiskowym. Opisu technik dokonano pod kątem wykorzystywanych mechanizmów izolacji analitów oraz stosowanych rozwiązań aparaturowych. Przegląd rozwiązań aparaturowych uzupełniono o podstawy teoretyczne izolacji bazującej na zjawisku podziału analitów.
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Analytical techniques in studies of the environmental fate of pharmaceuticals and personal-care products
PublikacjaW pracy przedstawiono dane literaturowe odnośnie źródeł emisji, dróg transportu, przemian i metabolizmu, pomiomu stężeń ksenobiotyków z grupy farmaceutyków i środków higieny osobistej w próbkach pobranych z różnych elementów środowiska (woda, gleba, osady denne) oraz próbek bioty. Szczególną uwagę zwrócono na techniki analityczne wykorzystywane w badaniach losu środowiskowego w/w zanieczyszczeń.
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Recent Trends in the Application of Chromatographic Techniques in the Analysis of Luteolin and Its Derivatives
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Ultrahigh-resolution detection techniques for biomedical applications of optical coherent tomography.
PublikacjaOptyczne metody pomiarowe odgrywają w ostatnich latach coraz większą rolę w badaniach i diagnostyce medycznej. Mają one szereg zalet, do których zaliczyć można odporność na promieniowanie elektromagnetyczne, bezinwazyjność, bezpieczeństwo pomiaru oraz wysoką rozdzielczość. Jedną z najważniejszych technik stosowanych w diagnostyce medycznej jest koherentna tomografia optyczna (OCT). Jest to wysokorozdzielcza metoda obrazowania wewnętrznych...
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Comparison of the measurement techniques employed for evaluation of ambient air odour quality
PublikacjaThe paper presents the results of investigation on ambient air odour quality in a vicinity of the industrial sewage treatment plant being a part of the crude oil processing plant. The investigation was performed during spring-winter season using a prototype of electronic nose and the Nasal Ranger field olfactometers. The prototype was equipped with a set of six semiconductor sensors by FIGARO Co. and one PID-type sensor. The field...
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Talents, Competencies and Techniques of Business Analyst: A Balanced Professional Development Program
PublikacjaThis paper presents preliminary results of action research in which we search for fundamentals of an universal theory of balanced approaches to software process. It is developed on the basis of balanced approach for professional development program for business analysts which integrates approaches oriented on talents, competencies and techniques. This paper includes the description of key concepts in background approaches, components...
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Using Continuous Integration Techniques in Open Source Projects – An Exploratory Study
PublikacjaFor a growing number of software projects, continuous integration (CI) techniques are becoming an essential part of the process. However, the maturity of their adoption in open source projects varies. In this paper, we present an empirical study on GitHub repositories to explore the use of continuous integration techniques in open source projects. Following the Goal-Question-Metric (GQM) approach, 3 research questions and 7 metrics...