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Modern trends in solid phase extraction: New sorbent media
PublikacjaBased on the recently published literature, this review provides an update of the most important features and application of formats and devices employed in solid phase extraction (SPE). Special attention was paid on new trapping media proposed in SPE prior the chromatography analysis, based on the use of nanostructured materials, including carbon nanomaterials, electrospun nanofibers, dendrimes and magnetic nanoparticles, molecular...
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Extraction with environmentally friendly solvents
PublikacjaThe ever-increasing demand for determining compounds at low concentration levels in complex matrices requires a preliminary step of analytes isolation/enrichment in order to employ a detection technique characterized by high sensitivity at low LOQ. Sample preparation is considered as crucial part of analytical procedures. Previously the parameter of “greenness” is as important as selectivity in order to avoid using harmful organic...
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Determination of Selected Metals in Fruit Wines by Spectroscopic Techniques
PublikacjaThe determination of metals in different types of food and beverages samples has drawn significant attention due to several reasons with the most important one being the nutritional and toxic effects of these elements or their compounds. The knowledge of certain elements content in wines/fruit wines is of special interest due to their toxicity in case of excessive intake and also the effect they seem to have on the organoleptic...
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Direct solid phase microextraction combined with gas chromatography – Mass spectrometry for the determination of biogenic amines in wine
PublikacjaA direct method based on immersion solid phase microextraction (DI-SPME) gas chromatography mass-spectrometry (GC-MS) was optimized and validated for the determination of 16 biogenic amines in Polish wines. In the analysis two internal standards were used: 1,7-diaminoheptane and bis-3-aminopropylamine. The method allows for simultaneous extraction and derivatization, providing a simple and fast mode of extraction and enrichment....
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Main complications connected with detection, identification and determination of trace organic constituents in complex matrix samples
PublikacjaIt is well known that some problems with the determination of organic analytes at trace level can occur. This issue is connected with contamination during each stage of the analytical procedure from sampling to sample preparation up to chromatographic analysis, which often leads to false-positive or overestimated results. Another problem associated with determination of analytes occurs at trace- and ultra-trace level is a background...
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An analytical hierarchy process for selection of the optimal procedure for resveratrol determination in wine samples
PublikacjaThe study shows the application of analytical hierarchy process (AHP) in ranking the analytical procedures, that are applied for resveratrol determination in wine samples. 19 different analytical methodologies are described by metrological, economic and environmental criteria, that are further divided into 10 subcriteria. Before AHP application, the amount of input data is decreased with cluster analysis. The first run of AHP is...
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Determination of Metals Content in Wine Samples by Inductively Coupled Plasma-Mass Spectrometry
PublikacjaKnowledge about the metal content of wine is very important, for many reasons. Depending on the element, its quantity varies in wine from ng/L to mg/L. Despite the fact that metals are not directly connected to the taste and aroma of the wine, their content should be determined and controlled, because excess is undesirable, and in some cases prohibited, due to potential toxicity. Several analytical procedures for metal determination...
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Prenatal exposure to substance of abuse: A worldwide problem
PublikacjaSubstance abuse during pregnancy is an important public health issue affecting the mother and the growing infant. Preterm labor, miscarriage, abruption and postpartum hemorrhage are obstetric complications which have been associated with women who are dependent on abused substances. Moreover, women are also at an increased risk of medical problems such as poor nutrition, anemia, urinary tract infections as well as sexually transmitted...
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Deep eutectic solvents vs ionic liquids: Similarities and differences
PublikacjaDeep eutectic solvents (DES) were introduced as an alternative to ionic liquids (IL) to overcome the drawbacks of IL solvents. However, some authors consider them to be a subclass of ILs. In contrast, other authors emphasize that these are by their nature independent, different groups of substances. Thus, the question arises: Which solvent group should DESs belong to? Maybe a new class should be added to the existing ones. The...
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Green, simple analytical method for biogenic amines determination in fruit juice samples using salting-out assisted liquid-liquid microextraction and gas chromatography-mass spectrometry
PublikacjaSalting-out assisted liquid-liquid microextraction (SALLME) was integrated with the derivatization procedure to establish a one-step sample pre-treatment approach for rapid analysis of 14 biogenic amines (BAs) in fruit juices. The methodology consists of salting-out of analytes, derivatization with ethyl chloroformate (ECF), extraction with ethyl acetate (EtAc), and the analysis of the derivatized BAs using gas chromatography-mass...
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Solid Phase Microextraction: Apparatus, Sorbent Materials, and Application.
Publikacjahe primary objective of this review article is to strategically screen and highlight the advancements in the area of solid phase microextraction (SPME). The plenty of review articles have been written on different aspects of SPME, this review is dedicated to provide the brief but clear overview of the research footprints so produced from SPME. Some of the key advancements in types and designs, coating materials, coating strategies,...
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Prediction of the Biogenic Amines Index of Poultry Meat Using an Electronic Nose
PublikacjaThe biogenic amines index of fresh chicken meat samples during refrigerated storage was predicted based on the headspace analysis using an electronic nose equipped with an array of electrochemical sensors. The reference biogenic amines index values were obtained using dispersive liquid–liquid microextraction–gas chromatography–mass spectrometry. A prototype electronic nose with modular construction and a dedicated sample chamber...
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Application of deep eutectic solvents in bioanalysis
PublikacjaThe application of deep eutectic solvents (DESs) is sharply surging as a green alternative to conventional solvents due to their unique properties in terms of simplicity of preparation, designability and low cost. A great deal of attention has been paid to the application of these green solvents in analytical chemistry in recent years, and a lot of interesting work has been reported. This review summarizes the most relevant applications...
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Multivariate Statistical Analysis for Mutual Dependence Assessment of Selected Polyphenols, Organic Acids and Metals in Cool-Climate Wines
PublikacjaPolyphenols, organic acids and metal ions are an important group of compounds that affect the human health and quality of food and beverage products, including wines. It is known that a specific correlation between these groups exist. While wines coming from the New World and the Old World countries are extensively studied, wines coming from cool-climate countries are rarely discussed in the literature. One of the goals of this...
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Ultrasound assisted solvent extraction of porous membrane-packed samples followed by liquid chromatography-tandem mass spectrometry for determination of BADGE, BFDGE and their derivatives in packed vegetables
PublikacjaThe problem of the presence of trace organic pollutants in food is of growing importance due to increasing awareness about their impact on newborns, infants and adults of reproductive age. Despite the fact that packaged food products offer many advantages, packaging can be a source of contamination for stored food. Thus, monitoring such pollution in food is of high importance. In this work, a novel methodology based on the solvent...
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Thermal Imaging in Wound Healing Diagnostics
PublikacjaOpisano wyniki projektu badawczego poświęconego opracowaniu metody obiektywnej diagnostyki ran pooperacyjnych w kardiochirurgii. Sprawdzono możliwość połączenia oceny obrazów RGB z obrazami termograficznymi oraz nową w medycynie metodą aktywnej termografii dynamicznej ADT. W projekcie zastosowano chłodzenie obszaru zainteresowania wykorzystując kriostat na dwutlenku węgla. W okresie powrotu do stanu równowagi termodynamicznej rejestrowane...
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25 years of research and experiences about the application of constructed wetlands in southeastern Poland
PublikacjaThis paper is a review of research and experiences related to the application of constructed wetland systems (CWs) in southeastern Poland in 1992–2016. On the basis of literature data, a comparison between pollutant removal efficiencies of one-stage and hybrid CWs was made. Some problems regarding the operation of these treatment plants were also presented. Data from various facilities indicate that one-stage CWs with horizontal...
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Szkolenie CNE: Niezwykła moc zadawania pytań w nauczaniu
Wydarzenia„Dydaktyczne Piątki” w CNE: Szkolenie dla nauczycieli akademickich „Niezwykła moc zadawania pytań w nauczaniu”
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Green Chemistry in Higher Education: State of the Art, Challenges, and Future Trends
PublikacjaNowadays, there is increasing interest in global sustainability, and thus, university students would like to know how human actions affect the health status of our planet. This is mainly due to their basic knowledge of problems such as global warming and greenhouse gases. Students would like to gain knowledge on how to safeguard the earth for future generations. This must involve changes in education programs at interested institutions...
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Magnetic deep eutectic solvents – Fundamentals and applications
PublikacjaMagnetic deep eutectic solvents (MDES), a relatively new subclass of conventional deep eutectic solvents (DES) containing additional paramagnetic components in their structure. MDES exhibit a strong response toward external magnetic fields, thus they can improve many industrial and analytical applications. In addition, this new group of solvents present unique physicochemical properties that can be easily tuned by selecting the...
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Dispersive Micro‐Solid Phase Extraction of Selected Metals in Water and Food Samples Followed by ICP‐OES Analysis: Method Development, Analysis of Real Samples and Greenness Evaluation
PublikacjaMultiwalled carbon nanotubes (MWCNTs) are well-known adsorbents because of their high surface area, layered and hollow architecture, hydrophobicity, and multiple and easily accessible adsorption sites. In this study, MWCNTs were used for dispersive micro-solid-phase extraction of various metal chelates in environmental and food samples. Different parameters such as concentration of the chelating reagent, the sorbent dosage, the...
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Novel Lytic Enzyme of Prophage Origin from Clostridium botulinum E3 Strain Alaska E43 with Bactericidal Activity against Clostridial Cells
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Changes in Nuclear Gene Expression Related to Mitochondrial Function Affect Extracellular Matrix, Collagens, and Focal Adhesion in Keratoconus
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NOWOCZESNE TECHNIKI ANALITYCZNE Wykład
Kursy OnlineStudenci zostaną zapoznani z nowoczesnymi technikami analitycznymi wykorzystywanymi do celów analizy i monitoringu zanieczyszczeń środowiska.
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Grywalizacja w dydaktyce akademickiej
WydarzeniaPowstające Centrum Nowoczesnej Edukacji PG zaprasza na ostatnie w tym roku seminarium z cyklu "Dydaktyczne piątki".
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Określenie jakości wyrobów winiarskich domowej produkcji pod względem zawartości amin biogennych
ProjektyProjekt realizowany w Katedra Chemii Analitycznej zgodnie z porozumieniem 0375/IP3/2015/73 z dnia 2015-03-19
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Opracowanie nowej metodyki rozdzielania enancjomerów oraz oznaczania jakościowego i ilościowego metamfetaminy otrzymanej metodą Emde oraz jej zanieczyszczeń i półproduktów w celu sporządzenia charakterystyki próbek metamfetaminy otrzymanej tą metodą
ProjektyProjekt realizowany w Wydział Chemiczny z dnia 2013-03-25
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PAMPERS Jednorazowe pieluchy dziecięce: monitorowanie wybranych związków toksycznych poprzez zastosowanie nowych metod analitycznych
ProjektyProjekt realizowany w Katedra Chemii Analitycznej zgodnie z porozumieniem UMO-2020/37/B/ST4/02886 z dnia 2021-02-01
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New method for personalization of avatar animation
PublikacjaThe paper presents a method for creating a personalized animation of avatar utilizing fuzzy inference. First the user designs a prototype version of animation, with keyframes only for important poses, roughly describing the action. Then animation is enriched with new motion phases calculated by the fuzzy inference system using descriptors given by the user. Various degrees of motion fluency and naturalness are possible to achieve....
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Remote task submission and publishing in BeesyCluster: security and efficiency of Web Service interface
PublikacjaPrezentujemy nowy system BeesyCluster, który stanowi łatwy w użyciu portal dostępowy do rozszerzalnej sieci usług wdrożonych i opublikowanych na klastrach/komputerach PC z wirtualnymi płatnościami za wykorzystanie usług. Administratorzy/użytkownicy mogą dołączać klastry/komputery PC dostępne poprzez SSH kliknięciem myszy bez konieczności dalszej konfiguracji na klastrze/komputerze PC udostępniającego. Ponadto, użytkownicy mogą...
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Microextraction by packed sorbent: Uncommon detection techniques, sorbents, samples and analytes
PublikacjaAmong sample preparation approaches, the most desirable are procedures that ensure high efficiency and reproducibility, that are cheap, fast and simple, that minimize the number of operational steps and that require a small amount of sample and solvent and are thus environmentally friendly. Microextraction by packed sorbent (MEPS) is a miniaturized form of solid-phase extraction, the use of which has been continuously expanding...
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Metal-Organic Frameworks in Green Analytical Chemistry
PublikacjaTaking into consideration the rapid expansion of MOFs applications in the analytical chemistry area, it is important to evaluate the existing and future analytical MOF-based methods according to GAC principles. From this point of view, eco-friendly MOFs-based methods should include features such as: green design and synthesis of MOF, evaluation of toxicity issues of MOFs, and incorporation of MOFs in GAC methods. This Chapter will...
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Application of additional factors supporting the microextraction process
PublikacjaDue to the fact that green analytical chemistry is of high importance, the past two decades have witnessed a rapid growth in the sample preparation area with special emphasis on simplification, miniaturization and automation of extraction procedures. In addition, to accelerate the extraction processes and to improve the separation of analytes, several enhanced parameters are applied. These factors include, ultrasounds, microwaves,...
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Ciecze głęboko eutektyczne pochodzenia naturalnego jako nowe medium ekstrakcji
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Literature update of analytical methods for biogenic amines determination in food and beverages
PublikacjaBiogenic amines (BAs) have been reported in a variety of foods, such as fish, meat, cheese, and wines. The formation of BAs in food by the microbial decarboxylation of amino acids can result in human allergic reactions, characterized by difficulty in breathing, rash, vomiting, and hypertension. Control measures to prevent biogenic amine formation in foods and/or reduce their levels should be considered. Therefore, monitoring of...
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CE-MS and GC-MS as “Green” and Complementary Methods for the Analysis of Biogenic Amines in Wine
PublikacjaTwo novel complementary analytical methods, namely an extraction-free capillary electrophoresis coupled to mass spectrometry (CE-MS) and direct immersion-solid-phase microextraction combined with gas chromatography-mass spectrometry (DI-SPME-GC-MS), have been developed and successfully applied for the determination of biogenic amines (BAs) in wine and fruit wine. They have been rigorously compared to each other in terms of various...
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Detection, identification and determination of chiral pharmaceutical residues in wastewater: Problems and challenges
PublikacjaChiral pharmaceuticals (CPs) are widely used in different areas of human life, thus they are frequentlydetected in different ecosystems. However, before CPs reach the environment, wastewater is subjected todifferent treatment processes in order to remove them. Nevertheless, such processes may affect thechirality of CPs, thus it is very important to monitor CP levels during the wastewater treatment.This review addresses the present...
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Chemiczne Źródła Prądu 2023
Kursy OnlinePzedmiot dla studentów WFTiMS , specjalność Konwersja Energii Zajęcia odbywają się zgodnie z planem w poniedziałki od 10 do 13, Prowadzący mgr inż. Zuzanna Zarach Pliki instrukcji dostępne na enauczaniu sprawozdania przesyłać należy na platformę enauczaniae w zakładce "Zadanie"
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Szkolenie CNE: English sounds in technology
Wydarzenia„Dydaktyczne Piątki” w CNE: „English sounds in technology – pronunciation workshop”
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Preliminary evaluation of selected mineral adsorbents used to remove phosphorus from domestic wastewater = Wstępna ocena przydatności wybranych adsorbentów mineralnych do usuwania fosforu ze ścieków bytowych
PublikacjaFour grinded mineral materials were studied for their ability of P sorption from the aq. phosphate solns. in 24-h tests by using equations of Langmuir and Freundlich isotherms. The particular sorbents contained mainly SiO254,5% Ca) 29.6%, Fe2O3 69,4% and showed the sorption capacities 56, 159, 285 or 2.4 mg/g resp.
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Influence of the particle size of carbonate-siliceous rock on the efficiency of phosphorous removal from domestic wastewater
PublikacjatThe aim of the study was to determine the influence of the particle size of carbonate–silica rock (opoka)used in rock filters on the efficiency of phosphorus removal from domestic wastewater. The investigationswere carried out in a laboratory using a model consisting of three vertical flow filters with carbonate–silicarock of different particle sizes (G1= 1–2 mm; G2= 2–5 mm; G3= 5–10 mm). The tested rock was subjectedto decarbonising...
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Projekt wnętrza IV sem 22/23 (gr. 3)
Kursy OnlineProjekt wnętrza, semestr 4, grupa 2 prowadzące: prof. ASP dr hab. Anna Wejkowska- Lipska, anna.wejkowska-lipska@asp.gda.pl dr Natalia Sokół, natalia.sokol@pg.edu.pl zajęcia: piątki 11:15 do 14:00, sala 352
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Komunikacyjne Konstrukcje Geotechniczne - 2023/2024
Kursy OnlineCelem przedmiotu jest zapoznanie studentów z zagadnieniami dotyczącymi konstrukcji na stałe związanych z gruntem, a co do których w przyszłości inżynierowie po specjalizacji mostowej i po otrzymaniu uprawnień budowlanych będą mieli prawo je projektować i budować.Należą do niech:przyczółki mostowe, filary mostowe, skrzydła przy przyczółkowe, ściany oporowe.tunele płytkie (drogowe, przejścia dla pieszych) , tunele głębokie, przepusty,...
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Szkolenie CNE: Wykładowca na tropie niewiedzy studenta
Wydarzenia„Dydaktyczne Piątki” w CNE: „Wykładowca na tropie niewiedzy studenta. Podstawy neurobiologiczne wpływu strachu na przywoływanie śladów pamięciowych”
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Association between Age at Diagnosis of Graves' Disease and Variants in Genes Involved in Immune Response
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Mechatronika II - Laboratorium
Kursy OnlineKurs umożliwia dokończenie laboratoriów z programowania sterowników Siemens na stanowisku MAS200 na Wydziale Mechanicznym. W ramach kursu zostaną podane informacje niezbędne do samodzielnego zrealizowania Laboratorium. Dodatkowo prowadzący w wyznaczonych godzinach będzie na bieżąco odpowiadał na pytania studentów. Wśród materiałów dostępne będą filmy z laboratorium, zdjęcia, pliki wsadowe i instrukcje.
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Szkolenie CNE: Kiedy student się uczy?
Wydarzenia„Dydaktyczne Piątki” w CNE: Szkolenie dla nauczycieli akademickich „Kiedy student się uczy? Techniki i narzędzia wspomagające proces efektywnej nauki studentów (w oparciu o wiedzę neurobiologiczną)”
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Angażujące formy zadań: 20 sposobów na wzbudzenie motywacji
WydarzeniaPowstające Centrum Nowoczesnej Edukacji Politechniki Gdańskiej zaprasza na kolejne seminarium z cyklu "Dydaktyczne piątki"
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Development of thin film SPME sorbents based on deep eutectic solvents and their application for isolation and preconcentration of endocrine-disrupting compounds leaching from diapers to urine
PublikacjaIn this study, the thin film solid phase microextraction (TF-SPME) based on a novel sorbent composed of deep eutectic solvent (DES) is proposed. Among several synthesized sorbents the most efficient was DES containing trihexyl(tetradecyl)phosphonium chloride and docosanol mixed with polydimethylsiloxane (PDMS) in a molar ratio 1:3:0.25 to achieve a more stable structure. The proposed sorbent was applied on a fiberglass mesh and...
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Greening procedures and analytical parameters. The polychlorinated naphthalenes analysis in complex matrices as proof of concept
PublikacjaDue to the complexity of analytical procedures employed for the determination of wide spectrum of persistent organic pollutants (POPs), it is important to consider the green character of the applied protocols and propose the greenest solutions. In this review, the green aspects of several analytical procedures used for the determination of polychlorinated naphthalenes (PCNs) (as a representatives of POPs) in different types of...