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Search results for: CERAMIC
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Wady powierzchniowe ceramicznych elementów tocznych = Surface cracks of ceramic rolling elements
PublicationMateriały ceramiczne posiadają kombinację optymalnych własności, które są niezbędne w zastosowaniach na wysoko obciążone elementy maszyn. Podstawowym problemem związanym z wytrzymałością zmęczeniową materiałów ceramicznych są wszelkiego rodzaju wady powierzchniowe będące efektem procesu wytwarzania lub wynikające z defektów struktury materiału ceramicznego. W artykule przedstawiono badania doświadczalne dwutlenku cyrkonu ze sztucznie...
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Deposition and growth of thin ceramic films
Publication: Thin ceramic films play an important role in modern technology. One of the more utilized methods of deposition of ceramic films is spin coating. In this paper we investigate optimal deposition parameters for LaNi0.6Fe0.4O3−δ thin layers spin coated from a polymeric precursor. The quality of the obtained layers is checked using scanning electron microscopy. Additionally, we investigate the growth of grains in ceramic films annealed at...
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Manufacturing technology of porous ceramic structure
PublicationW pracy przedstawiono wybrane metody otrzymywania porowatych struktur ceramicznych w oparciu o istniejące dane literaturowe.
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Crack propoagation in MgO-PSZ ceramic materials
PublicationThe properties of ceramic materials such as elevated hardness, high temperature capability, low coefficient of thermal expansion are of interest for rolling element materials. Widely used ceramic materials in engineering applications are silicon nitride, zirconia and alumina. The paper presents an experimental study of the fatigue life of MgO-PSZ ceramic material in lubricated contact with defined types of cracks. A ceramic angular...
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Emergency condition of the ceramic facade of a residential building
PublicationThe paper presents a description of the technical condition of the ceramic cladding of a residential building, the technical condition of which deteriorated significantly after only a few years of operation. The analysis of the influence of the applied design and working solutions on the façade failure frequency was analyzed. The article presents a conceptual solution to bring the building to the proper technical condition in terms...
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Emergency condition of the ceramic facade of a residential building
PublicationThe paper presents a description of the technical condition of the ceramic cladding of a residential building, the technical condition of which deteriorated significantly after only a few years of operation. The analysis of the influence of the applied design and working solutions on the façade failure frequency was analyzed. The article presents a conceptual solution to bring the building to the proper technical condition in terms...
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Hertzian Crack Propagation in Ceramic Rolling Elements
PublicationThe properties of ceramics are of most interest to rolling element manufacturers. The influence of ring crack size on rolling contact fatigue failure has been studied using numerical fracture analysis. Such crack are very often found on ceramic bearing balls and decrease fatigue life rapidly. The numerical calculations are based on a three dimensional model for the ring crack propagation. The stress intensity factors along crack...
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Pore structure of carbons coated on ceramic particles
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Carbon nanotube synthesis via ceramic catalysts
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Review on electrolyte ceramic materials for fuel cells
PublicationPublikacja stanowi przegląd materiałów wykorzystywanych w tlenkowych ogniwach paliwowych ze szczególnym uwzględnieniem materiałów elektrolitowych.
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Voltammetric response of ceramic Nasicon ammonia sensor
PublicationW pracy przedstawiono wyniki badań eksperymentalnych odpowiedzi czujnika w różnych stężeniach amoniaku. Czujnik został wykonany w technologii ceramicznej na bazie elektrolitu stałego - NASICONu.
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Ceramic composites for single-layer fuel cells
PublicationComposite materials consisting of acceptor doped lanthanum orthoniobate electrolyte phase (La0.98Ca0.02NbO4) and Li2O:NiO:ZnO semiconducting phase were synthesized. The precursor powder of La0.98Ca0.02NbO4 was prepared in nanocrystalline (mechanosynthesis) and microcrystalline (solid-state synthesis) form. The composite can be applied in a single-layer fuel cell, because of the presence of two phases acting as an anode and a cathode...
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Protonic Ceramic Fuel Cells as novel electrochemical devices
PublicationProton ceramic conductors are novel materials which are interesting from the application point of view. For example, Protonic Ceramic Fuel Cells (PCFCs) is a type of a solid oxide fuel cell, which uses proton ceramic conductors as an electrolyte. Scientists are looking for the most efficient materials for these devices. In recent years main focus has been put on the search for new proton and mixed proton-electron conductors which...
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Technological Problems in Lapping on Flat Surfaces of Ceramic Parts
PublicationThis paper will present the results of research on single-disc lapping of flat surfaces of small ceramic elements. Machining with the use of different tools such as metallic, two-metallic and abrasive-metallic will be analyzed. The basics and techniques of reinforcement of laps will be discussed. The results of the influence of parameters on the surface quality of ceramic conponents (sealing) for three treatments on lapping machines...
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INFLUENCE OF CERAMIC COATING ON MECHANICAL PROPERTIES OF STAINLESS STEEL
PublicationCrystal structure and phase composition of stainless steel substrates (AISI 304 type) was studied and it was found that they adopted the cubic symmetry. The calculated elementary cell parameter for the mayor Fe-Ni phase (weight fraction 99%) was a = 3.593 Å, whereas the mean grain size was = 2932 Å. Morphology of the stainless steel substrate surface was studied with profilometry. Mechanical properties of the stainless steel...
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<title>Glass-ceramic fiber optic sensors</title>
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Structure and oxygen permeability of BaCo0.7Fe0.3−In O3− ceramic membranes
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Properties of glass-ceramic for solid oxide fuel cells
PublicationW pracy przedstawiono właściwości krystalicznych pyro- i orto- krzemowych szkieł przygotowanych dla tlenkowych ogniw paliwowych. Zbadano rozszerzalnoność, ubytek masy, zmiany widm rentgenograficznych oraz widm impedancyjnych dla szkieł narażonych przez 60 dni na atmosfere ulteniajacą i redukująca w temperaturze 800C.
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Boron doped carbon nanotubes via ceramic catalysts
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Application of ceramic and composite tools in smoothing burnishing process.
PublicationArtykuł zawiera oryginalne konstrukcje narzędzi nagniatających. Elementy nagniatające zostały wykonane z ceramiki i kompozytu ''Karbonado''. Narzędzia te mogą być stosowane na obrabiarkach CNC i centrach obróbkowych, zwłaszcza do obróbki stali hartowanych. Artykuł przedstawia również wyniki badań i przykłady zastosowań tych narzędzi w przemyśle.
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New ceramic and composite tools for smoothing burnishing process
PublicationW pracy przedstawiono nowe konstrukcje narzędzi ceramicznych i z kompozytu karbonado do nagniatania twardych hartowanych stali. Zamieszczono wyniki badań wpływu parametrów technologicznych nagniatania walcowych próbek ze stali 45 o różnej twardości 23-56HRC na chropowatość powierzchni próbek.
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Impact of blending with polystyrene on the microstructural and electrochemical properties of SiOC ceramic
PublicationIn this work, we present the electrochemical behavior and microstructural analysis of silicon oxycarbide (SiOC) ceramics influenced by an addition of polystyrene (PS). Polymer-derived ceramics were obtained by pyrolysis (1000°C, Ar atmosphere) of different polysiloxanes prepared by sol–gel synthesis. This method is very effective to obtain desired composition of final ceramic. Two alkoxysilanes phenylthriethoxysilane and diphenyldimethoxysilane...
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A New Microwave Ceramic – Polymer Composite with 0-3 Connectivity
PublicationGoal of the present research was to fabricate and study two-phase BiNbO4//PVDF composites with 0-3 connectivity. Such composite consists of there-dimensionally connected polymer matrix loaded with dielectric ceramic particles. In the present case BiNbO4 powder acted as an active phase (dispersed phase) whereas polyvinylidene fluoride (PVDF) acted as a non-active (passive) phase (matrix). BiNbO4//PVDF composites with the volume...
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Proton Conducting Ceramic Powder Synthesis by a Low Temperature Method
PublicationMolten salt synthesis (MSS) is a simple method for the preparation of ceramic powders with specific morphology. The main role of the molten salts is to increase the reaction rate and lower the reaction temperature. It occurs because of much higher mobility of reactants in the liquid medium than in the solid state. In this work the molten salt synthesis was applied to produce ceramic powders of La0995Ca0005NbO4 and BaCe09−xZrxY01O3....
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SrCe0.9In0.1O3-δ-based reversible symmetrical Protonic Ceramic Cell
PublicationIn-doped SrCe0.9In0.1O3-δ (SCI) perovskite-type oxide is utilized as the solid electrolyte, as well as a component, together with SrFe0.75Mo0.25O3-δ (SFM) compound, in the composite-type electrodes to construct symmetrical Protonic Ceramic Fuel Cells (PCFC). With good mutual stability of SCI and SFM at high temperatures in water vapor-containing reducing and oxidizing conditions, as well as sufficient ionic conductivity with high...
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Polarization-sensitive optical coherence tomography for ceramic materials inspection
PublicationCeramics production is looking for a fast, reliable and non-destructive method that can be implemented on site for defect detection and analysis. In this paper we present polarization-sensitive optical coherence tomography (PS-OCT) as a method for defect inspection. Proposed extensions to standard OCT provide additional information for complete characterization of tested object. We compare OCT and microscope imaging that can easily...
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Aluminium surface treatment with ceramic phases using diode laser
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Research into properties of wear resistant ceramic metal plasma coatings
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The ultrafiltration ceramic membrane used for broth separation in membrane bioreactor
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Polyaryletherketone polymer nanocomposite engineered with nanolaminated Ti3SiC2 ceramic fillers
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Raman Spectroscopy for Investigation of Sol-Gel Materials and Ceramic Materials.
PublicationPrzedstawiono rezultaty prac nad zastosowanie spektroskopii ramanowskiej do badania polimerów hybrydowych wytwarzanych metodą zol-żel oraz ceramik ferroelektrycznych. Wykonano pomiary dla próbek objętościowych i struktur cienkowarstwowych. Zademonstrowano możliwośc monitorowania procesu syntezy w czasie rzeczywistym.
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Preparation and physicochemical characterization of ceramic supports for supported liquid membranes
PublicationImmobilizowane membrany ciekłe stały się przedmiotem intensywnych badań w ostanich latach, głównie w procesach oczyszczania strumieni gazowych. Kluczowym czynnikiem mającym wpływ na efektywność tych procesów ma czas życia układu membranowego, a zatem odpowiedni dobór nośnika i fazy membranowej. W porównaniu do nośników polimerowych, ceramiczne charakteryzują się większą grubością, jednak są bardziej stabilne termicznie. Praca...
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Thermal and Chemical Expansion in Proton Ceramic Electrolytes and Compatible Electrodes
PublicationThis review paper focuses on the phenomenon of thermochemical expansion of two specific categories of conducting ceramics: Proton Conducting Ceramics (PCC) and Mixed Ionic-Electronic Conductors (MIEC). The theory of thermal expansion of ceramics is underlined from microscopic to macroscopic points of view while the chemical expansion is explained based on crystallography and defect chemistry. Modelling methods are used to predict...
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Metoda badania powłok ceramicznych w ruchu postępowo-zwrotnym = A method for testing of ceramic coatings under reciprocating sliding
PublicationOpracowano metodę badania powłok ceramicznych w warunkach tarcia ślizgowego na próbkach tworzących układ o styku niekonforemnym kula - powierzchnia płaska. Pokryte warstwą ceramiczną kule dociskano do próbek płaskich - prostopadłościennych listew (również pokrytych ceramiką), wykonujących ruch postępowo-zwrotny. Jako stanowisko badawcze zastosowano Tribometr Posuwisto-zwrotny TPZ-1. Przebieg zużywania się powłoki ceramicznej oceniano...
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Silicon Oxycarbide (SiOC) Ceramic Materials as Anodes for Lithium Ion Batteries
PublicationPolymer derived ceramics (PDCs) have attracted attention as alternative anode material for Li-ion batteries. It has been found that ternary SiOC and SiCN ceramics obtained through pyrolysis of various preceramic polymers display high reversible capacities of 500 – 650 mAh/g. In this work we try to correlate the electrochemical performance of polymer derived silicon oxycarbide with its chemical composition and microstructural features....
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Thermal and technological aspects of double face grinding of Al2O3 ceramic materials
PublicationDouble face grinding with planetary kinematics is a process to manufacture workpieces with plan parallel functional surfaces, such as bearing rings or sealing shims. In order to increase the economic efficiency of this process, it has to be advanced permanently. The temperature in the contact zone of most grinding processes has a huge influence on the process efficiency and the workpiece qualities. In contrast to most grinding...
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Analysis of Ceramic Elements with Ring-Crack Defects in Lubricated Rolling Contact
PublicationThe properties of ceramics, specifically low density, high hardness, high temperature capability and low coefficient of thermal expansion are of most interest to rolling element manufacturers. Surface ring cracks on lubricating rolling contact fatigue failure has been studied using numerical fracture analysis. Such cracks are very often found on ceramic bearing balls and decrease fatigue life rapidly. The numerical calculations...
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Surface Texture Analysis of Hardened Shafts after Ceramic Ball Burnishing
PublicationThis article represents the results of testing the surface condition of shafts manufactured by the burnishing process. The shafts with a hardness of approximately 62 HRC (Rockwell C). were burnished with a ceramic ball (Si3N4), where the force range was controlled by the means of a hydraulic system. The machining process consisted of hard turning shafts with cubic boron nitride (CBN) inserts, followed by burnishing with the use...
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Wear of electroplated diamond tools in lap-grinding of Al2O3 ceramic materials
PublicationCurrent development of modern products, together with ever-increasing demands for their operation and usage, necessitate the search for new processing methods. Abrasive machining is widely used in many industrial areas, especially for processing difficult-to-machine materials such as advanced ceramics. Grinding with lapping kinematics, also called lap-grinding, is still one of the innovative methods of abrasive processing being...
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Optimization of the compositions area of radiotransparent ceramic in the SrO-Al2O3-SiO2 system
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Ceramic dispersion effect on composite coating properties after plastic working
PublicationW pracy określono wpływ fazy dyspersyjnej Al2O3 na wybrane potencjalne właściwości powłok kompozytowych o osnowie niklowej. Powłoki Ni-Al-Al2O3 zostały nałożone na próbki stalowe przy użyciu technologii poddźwiękowego płomieniowego natryskiwania cieplnego. Następnie poddane zostały obróbce plastycznej na zimno i na gorąco poprzez walcowanie, a także prasowania na zimno na prasie hydraulicznej. Omówiono wpływ obróbki plastycznej...
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Surface roughness of ceramic parts after lapping by abrasive-metallic tools
PublicationPrzedstawiono konstrukcję narzędzi ścierno-metalowych do obróbki na docierarce jednotarczowej. Wykonano badania docierania elementów z ceramiki tlenowej. Analizowano podstawowe parametry chropowatości powierzchni elementów z Al2O3 po obróbce narzędziami na bazie węglika boru.
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Performance and Stability in H2S of SrFe0.75Mo0.25O3-δ as Electrode in Proton Ceramic Fuel Cells
PublicationThe H2S-tolerance of SrFe0.75Mo0.25O3-δ (SFM) electrodes has been investigated in symmetric proton ceramic fuel cells (PCFC) with BaZr0.8Ce0.1Y0.1O3-δ (BZCY81) electrolyte. The ionic conductivity of the electrolyte under wet reducing conditions was found to be insignificantly affected in the presence of up to 5000 ppm H2S. The fuel cell exhibited an OCV of about 0.9 V at 700 °C, which dropped to about 0.6 V and 0.4 V upon exposure...
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Analysis of ring cracks in ceramic rolling elements using the boundary element method
PublicationCeramic materials have been increasingly used in bearing technology for over a dozen years. This is due to the characteristic properties of ceramic materials such as: high hardness, corrosion resistance, the possibility of use in aggressive chemical environments, as well as due to the lower specific weight compared to steel materials. However, the use of ceramic materials is connected with many limitations. The main disadvantages...
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Structure and magnetic properties of BeO-Fe2O3-Al2O3-TeO2 glass-ceramic composites
PublicationIn this work, glass-ceramics in the xBeO–20Fe2O3–(80-x)TeO2 system with x = 0–25 mol% were synthesized by the traditional melt quenching route and studied by inductively coupled plasma optical emission spectroscopy, X-ray diffraction, confocal microscopy, infrared and Raman spectroscopy. BeO addition was found to support the crystallization process of Fe2O3 during melting, and an increased BeO content was associated with an increased...
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A Multi Rig Screening Test for Thin Ceramic Coatings in Bio - Tribological Applications
PublicationA method is presented for the comparative testing of wear resistance of ceramic coatings made from materials potentially feasible in tribo - medical applications, mainly orthopaedic implants made from ceramics coated metals for low cost, long life and low wear particle emission into the body. The method was devised as the main tool for use in research and is comprised of flat on flat and ball on flat surface (sliding) tests. Seven...
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Sensing properties of a mixed-potential type NOx sensor based on YSZ ceramic
PublicationW pracy przedstawiono wyniki badań czujnika typu ''mixed-potential''. Czujnik zbudowany jest na bazie YSZ z warstwą NiO. Zbadano właściwości czujnika w rożnych stężeniach NO2. Zbadano wpływ grubości warstwy NiO na właściwości czujnika.
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Modular Ceramic-Polymeric Device for Analysis of Selected Elements in Liquid Using Microplasma
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Change of the Phase Composition and Strength of Al2O3–ZrO2-Ceramic After Hydrothermal Aging
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Influence of Firing Temperature on Phase Composition and Color Properties of Ceramic Tile Bodies
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