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Search results for: CALCIUM DOPED CERIA (CDC) SPARK PLASMA SINTERING NANOSTRUCTURES IONIC CONDUCTIVITY ELECTROSTRICTION
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Thermally induced formation of zinc oxide nanostructures with tailoring morphology during metal organic framework (MOF-5) carbonization process
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Opposite pressure impact on electron-phonon coupling in Eu2+ and Ce3+ doped AlN
Open Research DataThis data analyzes the influence of pressure on electron–lattice interactions in the 5d excited states of Ce3+ and Eu2+ in the AlN host based on pressure-dependent photoluminescence and photoluminescence excitation spectra. High-pressure measurements on AlN samples doped with Eu2+ and Ce3+ ions reveal that the Stokes shift increases with pressure for...
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Low-temperature spectroscopic and scintillation characterisation of Ti-doped Al2O3
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High pressure studies of Eu2+ and Mn2+ doped NaScSi2O6 clinopyroxenes
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Breakdown of Adiabatic Superconductivity in Ca-Doped h-BN Monolayer
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Oxide nanoparticle exsolution in Lu-doped (Ba,La)CoO3
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Luminescence and energy-storage properties of Pr3+-doped YAlO3 crystals
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OSL and RL of LiMgPO4 crystals doped with rare earth elements
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Photocatalytic activity and surface properties of carbon-doped titanium dioxide
PublicationTiO2 domieszkowany węglem otrzymano poprzez hydrolizę izopropanolanu tytanu(IV) i kalcynację w 350ºC w atmosferze powietrza przez 2h. Przeprowadzone badania wykazały, że fenol (0.21 mM) jest efektywnie degradowany w fazie wodnej, w obecności otrzymanego fotokatalizatora oraz światła z zakresu widzialnego (λ>400 nm). Pole powierzchni właściwej otrzymanego C-TiO2 wynosiło około 127 m2/g, fotokatalizator absorbuje światło z zakresu...
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Microwave solvothermal synthesis and characterization of manganese-doped ZnO nanoparticles
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Structural and thermal characteristics of Ni-doped carbosils prepared by mechanochemistry
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Boron-doped TiO2: Characteristics and photoactivity under visible light
PublicationOtrzymano TiO2 domieszkowany borem aktywny w reakcjach fotodegradacji pod wpływem światła widzialnego (λ>400 nm). Fotokatalizatory otrzymano poprzez hydrolizę tytanianu(IV) izopropylu w obecności związków boru lub poprzez ucieranie TiO2 (ST-01, P25 i A11) z prekursorami B i następnie kalcynację w zakresie temperatur 200-600oC. Jako źródło boru zastosowano kwas borowy lub ester trietylowy kwasu borowego. Najwyższą aktywność pod...
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Chemical characteristics of new nanopowder of titania doped with nitrogen atoms
PublicationW pracy zaprezentowano charakterystykę domieszkowanego azotem ditlenku tytanu otrzymanego na drodze jednoetapowej syntezy z kompleksu tytanu (IV) z ligandami zawierającymi atomy azotu. ikrostruktura i morfologia nowego materiału została określony za pomocą badań XRD, AFM, UV-VIS i FT-IR. Raport przedstawia również badania elektrochemiczne, które pozowliły na wyznaczenie potencjału pasma płaskiego na podstawie wykresu Mott
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Visible light activity and photoelectrochemical properties of nitrogen-doped TiO2.
PublicationFotokatalizatory TiO2 domieszkowane azotem zostały zsyntetyzowane z propanolanu tytanu (IV) lub chlorku tytanu (IV) i tiomocznika. Żółte proszki otrzymane po ogrzewaniu w temperaturach 400-600 st.C fotokatalizowały mineralizację 4-chlorofenolu w zakresie światła widzialnego (delta większe lub równe 455nm. W odróżnieniu od uprzednio opublikowanych wyników, zsyntetyzowane fotokatalizatory nie zawierały siarki, lecz zamiast tego azot...
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Oxide nanoparticle exsolution in Lu-doped (Ba,La)CoO3
PublicationThis study investigated Lu doping of Ba0.5La0.5CoO3 and its influence on the exsolution of oxide nanoparticles (NPs). As a result of Lu doping, we observed the phase segregation into the main Ba0.4La0.6Co0.85Lu0.15O3 (BLCO–Lu) phase and the secondary Ba0.85La0.15Co0.75Lu0.25O3 (BCO–Lu) phase. We noticed the exsolution of BCO–Lu nanoparticles on the main BLCO–Lu phase. Moreover, the BLCO–Lu phase exsolved in the form of nanoparticles...
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Synthesis of acceptor-doped Ba-Ce-Zr-O perovskites
PublicationPublikacja przedstawia wyniki badań stukturalnych i elektrycznych domieszkowanego akceptorow cerianu baru.
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Valence and Ionic Lowest-Lying Electronic States of Isobutyl Formate Studied by High-Resolution Vacuum Ultraviolet Photoabsorption, Photoelectron Spectroscopy, and Ab Initio Calculations
PublicationThe highest resolution vacuum ultraviolet photoabsorption spectrum of isobutyl formate, C5H10O2, yet reported is presented over the energy range 4.5−10.7 eV (275.5−118.0 nm) revealing several new spectral features. Valence and Rydberg transitions and their associated vibronic series observed in the photoabsorption spectrum have been assigned in accordance with new ab initio calculations of the vertical excitation energies and oscillator...
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Chromatographic behaviour of ionic liquid cations in view of quantitative structure-retention relationship
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Ionic liquids for the passive sampling of sulfonamides from water—applicability and selectivity study
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Review of the applicability of ionic liquid matrices for the quantification of small molecules by MALDI MS
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Comparison of different advanced oxidation processes for the degradation of room temperature ionic liquids
PublicationZbadano możliwość zastosowania wybranych zaawansowanych technologii utleniania (UV, UV/H2O2, UV/TiO2) do degradacji cieczy jonowych. Do degradacji wytypowano pięć związków: HHiM, BMiM, MiM, OMiM oraz EEiM.
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Use of imidazolium ionic liquids for carbon dioxide separation from gas mixtures
PublicationNowoczesnym podejściem do separacji tlenku węgla (IV) z mieszanin gazowych jest zastosowanie cieczy jonowych jako materiału absorpcyjnego. Niemierzalna prężność par i możliwość modyfikacji budowy kationu i wyboru anionu cieczy jonowych sprawiają, że związki te mogą zastąpić obecnie stosowane aminy. Przedstawiono wpływ struktury chemicznej cieczy jonowych, ciśnienia oraz temperatury na efektywność absorpcji CO2 i innych gazów w...
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Investigation of the distribution of imidazolium ionic liquids in the environment - aggregation in water and sorption on minerals
PublicationWpływ cieczy jonowych na środowisko, a w szczególności: migracja do wód powierzchniowych i gruntowych, jak również transport/retencja w gruntach jest determinowany przede wszystkim przez właściwości fizykochemiczne cieczy jonowej jak i właściwości matrycy środowiskowej. Znajomość zjawisk zachodzących w wyniku kontaktu cieczy jonowych z wodą oraz glebą jest jednym z podstawowych warunków oceny ryzyka chemicznego. W pracy wykazano,...
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Volatile organic compound separation from gas phase using ionic liquids
PublicationZanieczyszczenie powietrza lotnymi związkami organicznymi staje się światowym problemem ochrony środowiska w związku z ich toksycznymi właściwościami. W związku z tym poszukuje się nowych, efektywnych technologii oczyszczania strumieni gazowych. Powszechnie stosowaną metodą jest utlenianie termiczne. Wiąże się ono jednak z Wysokiem zużyciem energii i efektami ubocznymi w postaci emisji dwutlenku węgla i tlenków azotu. Alternatywą...
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XPS data of deuterium and hydrogen grown boron-doped diamond
Open Research DataThe high-resolution C1s X-ray absorption spectra of BDD@H and BDD@D samples were measured using the facilities of the HE-SGM beamline (HE-SGM) at the BESSY II synchrotron radiation source of Helmholtz–Zentrum Berlin (HZB).[90] The measurements were carried out under ultra-high vacuum conditions: P ≈ 2×10−9 Torr at T = 300 K. The NEXAFS spectra were...
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SEM images of 8YSZ sintered using flash sintering programme
Open Research DataThe dataset contains the SEM images of 8YSZ (8mol% Y2O3-ZrO2) sintered using the flash technique in the muffle furnace. The programme was as follows: 3oC/min to 1000C - 1h hold- 3oC/min 1100C - 1h hold- 3oC/min 1200C - 2h hold- 3oC/min 1400- 30 min hold- 5oC/min 1200C - 15h hold- 4oC/min RT
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Development of novel (BiO)2OHCl/BiOBr enriched with boron doped-carbon nanowalls for photocatalytic cytostatic drug degradation: Assessing photocatalytic process utilization in environmental condition
PublicationIn this work, a series of novel (BiO)2OHCl/BiOBr-x%B:DGNW (x = 0%, 1%, 1.5%, 2%) composites with different content of boron-doped diamond/graphene nanowalls (B:DGNW) were fabricated by simple solvothermal synthesis. A boron-doped diamond/graphene nanowalls (B:DGNW) were prepared by CVD method. A series of analyses: XRD, XPS, SEM, and TEM showed that the photocatalyst (BiO)2OHCl/BiOBr-x%B:DGNW with a “flower-like” morphology was...
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Nanosilver-loaded PMMA bone cement doped with different bioactive glasses – evaluation of cytocompatibility, antibacterial activity, and mechanical properties
PublicationNanosilver-loaded PMMA bone cement (BC-AgNp) is a novel cement developed as a replacement for conventional cements. Despite favorable properties and antibacterial activity, BC-AgNp still lacks biodegradability and bioactivity. Hence, we investigated the doping with bioactive glasses (BGs) to create a new bioactive BC characterized by time-varying porosity and gradual release of nanosilver. The BC Cemex was used as the base material...
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Boron-doped diamond nanosheet volume-enriched screen-printed carbon electrodes: a platform for electroanalytical and impedimetric biosensor applications
PublicationThis paper focuses on the development of a novel electrode based on boron-doped diamond nanosheet full-volume-enriched screen-printed carbon electrodes (BDDPE) for use as an impedimetric biosensor. Impedimetric biosensors offer high sensitivity and selectivity for virus detection, but their use as point-of-care devices is limited by the complexity of nanomaterials’ architecture and the receptor immobilisation procedures. The study...
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Focused ion beam-based microfabrication of boron-doped diamond single-crystal tip cantilevers for electrical and mechanical scanning probe microscopy
PublicationIn this paper, the fabrication process and electromechanical properties of novel atomic force microscopy probes utilising single-crystal boron-doped diamond are presented. The developed probes integrate scanning tips made of chemical vapour deposition-grown, freestanding diamond foil. The fabrication procedure was performed using nanomanipulation techniques combined with scanning electron microscopy and focused ion beam technologies....
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Effective calcium doping at the B-site of BaFeO3−δ perovskite: towards low-cost and high-performance oxygen permeation membranes
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Fuzzy reasoning approach to properties' determination of calcium phosphate coatings processed using ion beam assisted deposition on heated substrates
PublicationPraca przedstawia rozmyty system wnioskowania dla zamodelowania związków pomiędzy temperaturą podłoża oraz stosunkiem molowym Ca/P w gradientowej powłoce hydroxyapatytowej na podłożu tytanowym. Przeprowadzono symulację działania sterownika rozmytego na pomocą oprogramowania Matlab.
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Efficiency of ozonation process with calcium peroxide in removing heavy metals (Pb, Cu, Zn, Ni, Cd) from aqueous solutions
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XRD, DTA and luminescence measurements of B2O3-Bi2O3-AlF3 glasses doped with Eu3+, Tb3+ and Tm3+ ions
Open Research DataThe DataSet contains the XRD,DTA and luminescence measurements for the B2O3-Bi2O3-AlF3 glass system. Samples were prepared by the conventional melt quenching technique. Starting materials were melted in porcelain crucibles at 950 oC for 20 min. XRD and DTA data were collected for 50B2O3-50Bi2O3,45B2O3-45Bi2O3+10AlF3 and 40B2O3-40Bi2O3+20AlF3 glasses....
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Valence and ionic lowest-lying electronic states of ethyl formate as studied by high-resolution vacuum ultraviolet photoabsorption, He(I) photoelectron spectroscopy, and ab initio calculations
PublicationThe highest resolution vacuum ultraviolet photoabsorption spectrum of ethyl formate, C2H5OCHO, yet reported is presented over the wavelength range 115.0–275.5 nm (10.75–4.5 eV) revealing several new spectral features. Valence and Rydberg transitions and their associated vibronic series, observed in the photoabsorption spectrum, have been assigned in accordance with new ab initio calculations of the vertical excitation energies...
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Phospholipidomic Analysis Reveals Changes in Sphingomyelin and Lysophosphatidylcholine Profiles in Plasma from Patients with Neuroborreliosis
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Photon Physics and Plasma Research, Photonics Applications and Web Engineering, Wilga, May 2012
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The K x-ray line structures of the 3d-transition metals in warm dense plasma
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Increase in wear resistance of nickel plasma coatings under traditional and combined treatment conditions
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Plasma micronutrients, trace elements, and breast cancer in BRCA1 mutation carriers: an exploratory study
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A fully validated HPLC–UV method for determination of sulthiame in human serum/plasma samples
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Proteomic-Biostatistic Integrated Approach for Finding the Underlying Molecular Determinants of Hypertension in Human Plasma
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Independent Association Between Plasma Leptin Levels and Heart Rate in Heart Transplant Recipients
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An independent relationship between plasma leptin and heart rate in untreated patients with essential hypertension
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The plasma concentration of advanced oxidation protein products and arterial stiffness in apparently healthy adults
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Chitosan/phospholipid coated polyethylene terephthalate (PET) polymer surfaces activated by air plasma
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Characteristics of hybrid chitosan/phospholipid-sterol, peptide coatings on plasma activated PEEK polymer
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Blood plasma protein and lipid profile changes in calves during the first week of life
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The impact of regular sperm donation on bulls’ seminal plasma hormonal profile and phantom response
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Electrochemical determination of nitroaromatic explosives at boron-doped diamond/graphene nanowall electrodes: 2,4,6-trinitrotoluene and 2,4,6-trinitroanisole in liquid effluents
PublicationThe study is devoted to the electrochemical detection of trace explosives on boron-doped diamond/graphene nanowall electrodes (B:DGNW). The electrodes were fabricated in a one-step growth process using chemical vapour deposition without any additional modifications. The electrochemical investigations were focused on the determination of the important nitroaromatic explosive compounds, 2,4,6-trinitrotoluene (TNT) and 2,4,6-trinitroanisole...