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Search results for: PHOSPHONIUM CALIX[4]ARENES
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Recent trends in prevalence of neoplasia in the Baltic clam Macoma balthica (L.) from the Gulf of Gdańsk (Baltic Sea).
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Tmscl as a rate accelerating additive in acylations of amines with 5-(α-amino- α'-hydroxy)methylene meldrum's acids
PublicationAspects are presented of the acylation of amines, alcohols and thiols with 5-(α-amino- α'-hydroxy)methylene Meldrum's acids. We placed special emphasis on the acylation reaction of secondary amines with 5-(α-amino- α'-hydroxy)methylene Meldrum's acids, which, due to their basicity, caused problems concerning salt formation with a Meldrum acid derivative. We found that secondary amines, which react at the slowest rate and with a...
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N-Substituted piperazine derivatives as potential multitarget agents acting on histamine H3 receptor and cancer resistance proteins
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The hydration of the protein stabilizing agents: trimethylamine-N-oxide, glycine and its N-methylderivatives - the volumetric and compressibility studies
PublicationThe densities at T = (288.15, 293.15, 298.15, 303.15, and 308.15) K and sound velocities at T = 298.15 K have been measured for aqueous solutions of trimethylamine-N-oxide, glycine, N-methylglycine (sarcosine), N,N-dimethylglycine, N,N,N-trimethylglycine (betaine). From these data the apparent molar volumes, VΦ, the apparent molar isentropic compressions, KS,Φ, and the solvation numbers of solutes have been determined. The concentration...
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Electrochemical simulation of metabolic reduction and conjugation reactions of unsymmetrical bisacridine antitumor agents, C-2028 and C-2053
PublicationElectrochemistry (EC) coupled with analysis techniques such as liquid chromatography (LC) and mass spectrometry (MS) has been developed as a powerful tool for drug metabolism simulation. The application of EC in metabolic studies is particularly favourable due to the low matrix contribution compared to in vitro or in vivo biological models. In this paper, the EC(/LC)/MS system was applied to simulate phase I metabolism of the representative...
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Polymeric metal‐containing ionic liquid sorbent coating for the determination of amines using headspace solid‐phase microextraction
PublicationThis study describes the design, synthesis, and application of polymeric ionic liquid sorbent coatings featuring nickel metal centers for the determination of volatile and semivolatile amines from water samples using headspace solidphase microextraction. The examined polymeric ionic liquid sorbent coatings were composed of two ionic liquid monomers (tetra(3-vinylimidazolium)nickel bis[(trifluoromethyl)sulfonyl]imide [Ni2+(VIM)4]...
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Unexpected Z/E isomerism of N-methyl-O-phosphothioyl benzohydroxamic acids, their oxyphilic reactivity and inertness to amines
PublicationThiophosphinoylation of N-methyl p-substituted benzohydroxamic acids using disulfanes (method A) or diphenylphosphinothioyl chloride (method B) provides only one conformer of the respective O-phosphothioyl derivative (Xray and NMR analysis). Undergoing the P-transamidoxylation reaction is an evidence of the reversibility of thiophosphinoylation. Only those products containing strong EWG substituents in the aroyl residue or bulky...
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Absence of 6-Hydroxydopamine in the Rat Brain After Treatment with Stimulants and Other Dopaminergic Agents: A Mass Fragmentographic Study
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Pd-catalysed general access to 7-membered N/O-heterocyclic compounds as potential agents against inflammation
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Trends in biomedical analysis of red blood cells – Raman spectroscopy against other spectroscopic, microscopic and classical techniques
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Silicon polypodands: powerful metal cation complexing agents and solid–liquid phase-transfer catalysts of new generation
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DNA methylation in cancer development, diagnosis and therapy-multiple opportunities for genotoxic agents to act as methylome disruptors or remediators
PublicationThe role of DNA methylation and recently discovered hydroxymethylation in the function of the human epigenome is currently one of the hottest topics in the life sciences. Progress in this field of research has been further accelerated by the discovery that alterations in the methylome are not only associated with key functions of cells and organisms, such as development, differentiation and gene expression, but may underlie a number...
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The influence of ammonia and selcted amines on the characteristics of calcium carbonate precipitated from calcium chloride solutions via carbonation
PublicationThe precipitation of calcium carbonate was carried out by passing a gasous mixture of carbon dioxide and air into a calcium chloride solution. The selected compounds enhancing carbon dioxide absorption were used as additives which promote the formation of carbonate ions in the solution. The additives were ammonia, monoethanolamine, triethylamine and triethanolamine. The resulting calcium carbonate particles varied in polymorphic...
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What is the future of digital education in the higher education sector? An overview of trends with example applications at Gdańsk Tech, Poland
PublicationUniversities worldwide recognise the need to adapt to changes in society, the economy and the way young people prefer to learn. Additionally, the impetus to improve the digital approach in higher education intensifies as educational institutions have to remain competitive with commercial providers of education. Following the latest technological trends and implementing strategies to develop new digital solutions helps to improve...
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Synthesis and characterization of ruthenium and rhenium dyes with phosphonate anchoring groups
PublicationRe(L1)–Re(L3), a series of rhenium(I) tricarbonyl chloride complexes with bpy-R2 derivatives L1–L3 (bpy = 2,2′-bipyridine, R represents the substitution at the 4- and 4′-positions), and their corresponding trishomoleptic Ru(L1)3–Ru(L3)3 as well as heteroleptic ruthenium(II) complexes Ru(tbbpy)2(L1) and Ru(tbbpy)2(L2) have been synthesized and characterized. Their applicability as immobilizable metal–organic chromophores in solar...
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The Reactivity of Phosphanylphosphinidene Complexes of Transition Metals Toward Terminal Dihaloalkanes
PublicationThe reactivities of phosphanylphosphinidene complexes [(DippN)2W(Cl)(η2-P−PtBu2)]− (1), [(pTol3P)2Pt(η2- P=PtBu2)] (2), and [(dppe)Pt(η2-P=PtBu2)] (3) toward dihaloalkanes and methyl iodide were investigated. The reactions of the anionic tungsten complex (1) with stochiometric Br(CH2)nBr (n = 3, 4, 6) led to the formation of neutral complexes with a tBu2PP(CH2)3Br ligand or neutral dinuclear complexes with unusual tetradentate...
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Ekspertyza techniczna dotycząca stanu technicznego budynku zlokalizowanego w gdańsku przy ul. Podwale Grodzkie 4 w aspekcie określenia zakresu prac zabezpieczających układ konstrukcyjny obiektu
PublicationCelem ekspertyzy jest ocena stanu technicznego układu konstrukcyjnego budynku przy ulicy Podwale Grodzkie 4. Ponadto celem opracowania jest udzielenie odpowiedzi na pytanie czy możliwa jest zmiana sposobu użytkowania obiektu bez przeprowadzenia istotnych zmian układu konstrukcyjnego i jego docelowa eksploatacja jako budynku użyteczności publicznej. Zakres opracowania obejmuje również wskazanie ramowego programu prac związanych...
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Synthesis and molecular structure of novel 2-(alkylthio)-4-chloro-N-(4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-yl)-5-methylbenzenesulfonamideswith potential anticancer activity
PublicationOtrzymano 15 nowych związków: 2-(alkilotio)-4-chloro-N-(4,5-dihydro-5-oxo-1H-1,2,4-triazol-3-yl)-5-metylobenzenosulfonamidów, dla których opracowano nową metodę syntezy. Dla jednej pochodnej wyznaczono strukturę rentgenowską. Związek nr 36 wykazuje wysoką aktywność przeciwnowotworową w stosunku do 13 linii komórek nowotworowych o poziomie GI_50 w zakresie stężeń 1,9-3,0 μM.
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Influence of synthesis conditions on glass formation, structure and thermal properties in the Na 2 O-CaO-P 2 O 5 system doped with Si 3 N 4 and Mg
PublicationOxynitride phosphate glasses and glass-ceramics were prepared using new synthesis routes for phosphate glasses. Materials were melted from pre-prepared glass samples in the system Na-Ca-P-O with addition of Mg and/or Si3N4 powders under different preparation conditions. The melting process was conducted at 1000–1500 °C either under air or nitrogen atmosphere to obtain materials with different nitrogen content. Their topography...
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Ekspertyza techniczna dotycząca stanu technicznego drewnianej konstrukcji stropu nad salą balową w budynku dawnej przychodni PKP w Gdańsku przy ul. Podwale Grodzkie 4
PublicationPrzedmiotem ekspertyzy była ocena stanu technicznego stropu drewnianego nad salą balową z uwzględnieniem analizy statyczno-wytrzymałościowej i oceny szkodliwości grzybów występujących na drewnianych krążynach sklepienia kolebkowego.
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PRZEJMOWANIE CIEPŁA PRZY WRZENIU NANOCIECZY W DUŻEJ OBJĘTOŚCI. Cz. 4. Wyniki badań eksperymentalnych wrzenia nanocieczy woda-Al2O3 i woda-Cu na poziomych rurkach
PublicationPrzedstawiono wyniki badań eksperymentalnych wrzenia nanocieczy woda-Al2O3 i woda-Cu o koncentracji nanocząstek 0.01%, 0.1% i 1% na stalowych rurkach gładkich i pokrytych powłoką porowatą.
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Synthesis of 3-(2-Alkylthio-4-chloro-5-methylbenzenesulfonyl)-2-(1-phenyl-3-arylprop-2-enylideneamino)guanidine Derivatives with Pro-Apoptotic Activity against Cancer Cells
PublicationThe untypical course of reaction between chalcones and benzenesulfonylaminoguanidines led to the new 3-(2-alkylthio-4-chloro-5-methylbenzenesulfonyl)-2-(1-phenyl-3-arylprop-2- enylideneamino)guanidine derivatives 8–33. The new compounds were tested in vitro for their impact on the growth of breast cancer cells MCF-7, cervical cancer cells HeLa and colon cancer cells HCT-116 by MTT assay. The results revealed that the activity of...
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On trees with double domination number equal to 2-outer-independent domination number plus one
PublicationA vertex of a graph is said to dominate itself and all of its neighbors. A double dominating set of a graph G is a set D of vertices of G such that every vertex of G is dominated by at least two vertices of D. The double domination number of a graph G is the minimum cardinality of a double dominating set of G. For a graph G=(V,E), a subset D subseteq V(G) is a 2-dominating set if every vertex of V(G)D has at least two neighbors...
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Ochrona odgromowa dużych obiektów sportowych na przykładzie stadionu PGE ARENA w Gdańsku
PublicationW artykule przedstawiono specyfikę ochrony dużych obiektów sportowych przed skutkami wyładowań atmosferycznych. Omówiono zasady ochrony tych obiektów przed bezpośrednim uderzeniem pioruna oraz sposoby ograniczenia przepięć powstających w instalacjach elektroenergetycznych oraz sterujących i pomiarowych zainstalowanych w takich obiektach. Wskazano konieczność indywidualnego rozwiązywania systemów ochronnych.
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Water Needs of Sweet Cherry Trees in the Light of Predicted Climate Warming in the Bydgoszcz Region, Poland
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Predictive Capacity of Rainfall Data to Estimate the Water Needs of Fruit Plants in Water Deficit Areas
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Human Health Risk Assessment on the Consumption of Apples Growing in Urbanized Areas: Case of Kharkiv, Ukraine
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Low Frequency Electromagnetic Interferences Impact on Transport Security Systems Used in Wide Transport Areas
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Hyponastic Leaves 1 Interacts with RNA Pol II to Ensure Proper Transcription of MicroRNA Genes
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Military Training Areas and Vegetation – the Effect of Explosion Craters on Species Diversity along a Moisture Gradient
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The use of terrestrial laser scanning in monitoring and analyses of erosion phenomena in natural and anthropogenically transformed areas
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Haloperidol, but not olanzapine, may affect expression of PER1 and CRY1 genes in human glioblastoma cell line
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A role for accessory genes rI.-1 and rI.1 in the regulation of lysis inhibition by bacteriophage T4
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Coexistence of HFE and rare UGT1A1 genes mutations in patients with iron overload related liver injury
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Altered Expression of ESR1, ESR2, PELP1 and c-SRC Genes Is Associated with Ovarian Cancer Manifestation
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Enterococci isolated from plant-derived food - Analysis of antibiotic resistance and the occurrence of resistance genes
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Effects of flavonoids on expression of genes involved in cell cycle regulation and DNA replication in human fibroblasts
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The Risk Indicators of Construction Projects’ Cost Overruns Assessed with PCA, Decision Trees, and Pearson’s Correlations
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Comparison of Absorbed and Intercepted Fractions of PAR for Individual Trees Based on Radiative Transfer Model Simulations
PublicationThe fraction of absorbed photosynthetically active radiation (fAPAR) is a key parameter for estimating the gross primary production (GPP) of trees. For continuous, dense forest canopies, fAPAR, is often equated with the intercepted fraction, fIPAR. This assumption is not valid for individual trees in urban environments or parkland settings where the canopy is sparse and there are well-defined tree crown boundaries. Here, the distinction...
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A different methylation profile of circadian genes promoter in breast cancer patients according to clinicopathological features
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P.238 Lithium treatment modulates the expression of inflammation involved genes in major depressive disorder
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Increased Expression of Several Collagen Genes is Associated with Drug Resistance in Ovarian Cancer Cell Lines
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Expression Changes in Fatty acid Metabolic Processrelated Genes in Porcine Oocytes During in Vitro Maturation
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Analysis of loading history influence on fatigue and fracture surface parameters using the method of induction trees
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Acoustic imaging of selected areas of Gdansk Bay with the aid of parametric echosounder and side-scan sonar
PublicationThe article presents and analyses the data recorded during sounding of the Gdansk Bay seabed with the aid of a parametric echosounder and a side-scan sonar. The accuracy of seabed structure examination, as a condition for obtaining valuable results, requires correct configuration of echolocation devices and proper calibration of peripheral devices, such as the survey unit geographical position sensor – GPS, the navigation unit,...
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Providing Public Space Continuities in Post-Industrial Areas through Remodelling Land/Water Connections
PublicationThis article examines the problem of urban transformation strategies applied in recent years which are based on the creation of new water areas and modification of existing ones. The research is an attempt to prove that modifications of plans of water areas and forms of their borders may play an important role in achieving the best quality public spaces in post-industrial territories. The basis for demonstrating the importance...
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Analyzing sets of phylogenetic trees obtained from bayesian MCMC process using topology metrics
PublicationThe reconstruction of evolutionary trees is one of the primary objectives in phylogenetics. Such a tree represents historical evolutionary relationship between different species or organisms. Tree comparisons are used for multiple purposes, from unveiling the history of species to deciphering evolutionary associations amongorganisms and geographical areas.In the paper, we describe a general method for comparing hylogenetic trees....
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The Application Of A Noise Mapping Tool Deployed In Grid Infrastructure For Creating Noise Maps Of Urban Areas
PublicationThe concept and implementation of the system for creating dynamic noise maps in PL-Grid infrastructure are presented. The methodology of dynamic acoustical maps creating is introduced. The concept of noise mapping, based on noise source and propagation models, was developed and employed in the system. The details of incorporation of the system to the PL-Grid infrastructure are presented. The results of simulations performed by...
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Endangerments of Aesthetical and Composition Values of the Landscape in Suburban Areas UZUPEŁNIĆ TŁUMACZENIE TYTUŁU : POLSKI TYTUŁ
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Fracture Areas Quantitative Investigating of Bending-Torsion Fatigued Low-Alloy High-Strength Steel
PublicationIn this study, the impact of pseudo-random non-proportional bending-torsion fatigue loadings proportion on the fatigue life and the fracture surface topography was analyzed. Investigation was carried out for 24 specimens made of S355J2 steel with 11 different ratios of maximum stresses λ. For these cases, after the fatigue tests, the surface topography measurements were carried out using an optical profilometer, using the focus...