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Search results for: synthetic benchmarking
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Application of multicriteria decision analysis to assess the greenness of molecularly imprinted polymers synthesis components
PublicationThe study applies multicriteria decision analysis (MCDA) to rank the components of molecularly imprinted polymers (MIPs) synthesis according to their greenness. The components are taken from papers that are describing synthesis of MIPs for persistent organic pollutants (POPs) sorbents. Functional monomers (n = 14), target/surrogate molecules (n = 10), porogens (n = 8), cross-linking agents (n = 8) and initiators (n = 4) are described...
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Optimizing Medical Personnel Speech Recognition Models Using Speech Synthesis and Reinforcement Learning
PublicationText-to-Speech synthesis (TTS) can be used to generate training data for building Automatic Speech Recognition models (ASR). Access to medical speech data is because it is sensitive data that is difficult to obtain for privacy reasons; TTS can help expand the data set. Speech can be synthesized by mimicking different accents, dialects, and speaking styles that may occur in a medical language. Reinforcement Learning (RL), in the...
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Efficient method for octahedral NH2-MIL-125 (Ti) synthesis: Fast and mild conditions
PublicationA new hot injection method for preparing octahedral NH2-MIL-125 (Ti) was developed. This method is six times faster and conducted under milder conditions, i.e., at 120°C in a flask, and exhibits higher crystal formation efficiency than the commonly used solvothermal method while maintaining comparable structural, optical, and photocatalytic properties.
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Practical Method for the Preparation of 2,2-Dimethyl-5- {aryl[(hetero)aryl]methyl}-1,3-dioxane-4,6-diones: Synthesis and Mechanistic Study
PublicationAn efficient practical synthetic procedure has been developed for the synthesis of 2,2-dimethyl-5-{aryl[(hetero)aryl]methyl}- 1,3-dioxane-4,6-diones through Friedel–Crafts alkylation. The scope and limitation of the reaction of 2,2-dimethyl-5-arylidene-1,3-dioxane- 4,6-diones with π-excess aromatic systems have been delineated.
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Bibliometric data for a research study on scientific productivity of Polish technical universities (AGH University of Science & Technology 2016-2020) retrieved by InCites benchmarking tool.
Open Research DataThis dataset was created for the purpose of research on scientific productivity at Polish technical universities.The raw data was retrieved in July 2021 by the InCites benchmarking tool in xlsx format and will be used to create the research profiles of the universities and underlying data of journals articles. The most common definition of research...
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Bibliometric data for a research study on scientific productivity of Polish technical universities (West Pomeranian University of Technology 2016-2020) retrieved by InCites benchmarking tool.
Open Research DataThis dataset was created for the purpose of research on scientific productivity at Polish technical universities.The raw data was retrieved in July 2021 by the InCites benchmarking tool in xlsx format and will be used to create the research profiles of the universities and underlying data of journals articles. The most common definition of research...
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Dataset of bibliometric data for a research study on scientific productivity of Polish economic universities (Warsaw School of Economics 2016-2020) retrieved by InCites benchmarking tool.
Open Research DataThis dataset was created for the purpose of research on scientific productivity at Polish economic universities. The raw data was retrieved in July 2021 by the InCites benchmarking tool in xlsx format and will be used to create the research profiles of the universities and underlying data of journals articles. The most common definition of research...
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Dataset of bibliometric data for a research study on scientific productivity of Polish economic universities (University of Economics in Katowice 2016-2020) retrieved by InCites benchmarking tool.
Open Research DataThis dataset was created for the purpose of research on scientific productivity at Polish economic universities. The raw data was retrieved in July 2021 by the InCites benchmarking tool in xlsx format and will be used to create the research profiles of the universities and underlying data of journals articles. The most common definition of research...
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Dataset of bibliometric data for a research study on scientific productivity of Polish economic universities (Cracow University of Economics 2016-2020) retrieved by InCites benchmarking tool.
Open Research DataThis dataset was created for the purpose of research on scientific productivity at Polish economic universities. The raw data was retrieved in July 2021 by the InCites benchmarking tool in xlsx format and will be used to create the research profiles of the universities and underlying data of journals articles. The most common definition of research...
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A heterotrimetallic synthetic approach in versatile functionalization of nanosized {MxCu13–xW7}3+ and {M1Cu8W6} (M = Co, Ni, Mn, Fe) metal–cyanide magnetic clusters
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XRD patterns of V2O5 thin films deposited on isotropic etching silicon substrates (111)
Open Research DataThe DataSet contains the XRD patterns of V2O5 thin films deposited on isotropic etching silicon substrates (111). The silicon wafers were etched in a mixture of nitric acid, hydrofluoric acid, and acetic acid in the ratio of 40:1:15. The soaking time for the substrates was from 30 to 90 seconds. The thin films were obtained by the sol-gel method. ...
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Nowe monomery pochodzenia roślinnego w syntezie termoplastycznych elastomerów poliuretanowych
PublicationJak dotychczas w syntezie termoplastycznych elastomerów poliuretanowych (TPU) są powszechnie wykorzystywane surowce pochodzenia petrochemicznego. Sytuacja jednak zmienia się dynamicznie i w wielu gospodarkach świata widoczne są już trendy, polegające na coraz większym wykorzystaniu substancji pochodzenia roślinnego w produkcji surowców, np. glikoli, izocyjanianów czy polioli, jako zamienników analogów syntetycznych. Praca obejmuje...
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Synthesis and photocatalytic performance of TiO2 nanospheres–graphene nanocomposite under visible and UV light irradiation
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Synthesis, characterization, and photocatalytic properties of core/shell mesoporous silica nanospheres supporting nanocrystalline titania
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A chromatography-free total synthesis of a ferrocene-containing dendrimer exhibiting the property of recognizing 9,10-diphenylanthracene
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Tris(ferrocenylmethidene)sumanene: synthesis, photophysical properties and applications for efficient caesium cation recognition in water
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Novel and effective synthesis protocol of AgNPs functionalized using L-cysteine as a potential drug carrier
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New Insight into the Synthesis and Biological Activity of the Polymeric Materials Consisting of Folic Acid and β‐Cyclodextrin
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Sulfonated carbon-encapsulated iron nanoparticles as an efficient magnetic nanocatalyst for highly selective synthesis of benzimidazoles
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Synthesis and structural properties of carbon/alumina composites: Practical application in solid phase extraction of explosives
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Synthesis, biological activity and conformational analysis of head-to-tail cyclic analogues of LL37 and histatin 5
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Synthesis and Modification by Carbonization of Styrene–Ethylene Glycol Dimethacrylate–Lignin Sorbents and their Sorption of Acetylsalicylic Acid
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Diosgenyl 2-amino-2-deoxy-β-D-galactopyranoside: synthesis, derivatives and antimicrobial activity
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Synthesis and luminescence characteristics of Dy3+ ions in silica xerogels doped with Ln2−xDyx(WO4)3
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Fischer–Tropsch synthesis: Studies effect of reduction variables on the performance of Fe–Ni–Co catalyst
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A novel green one-step synthesis of gold nanoparticles using crocin and their anti-cancer activities
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Synthesis and characterization of mechanically alloyed nanostructured ternary titanium based alloy for bio-medical applications
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Studies on Aminoanthraquinone-Modified Glassy Carbon Electrode: Synthesis and Electrochemical Performance toward Oxygen Reduction
PublicationIn this paper, 9,10-anthraquinone (AQ) derivative-modified glassy carbon (GC) electrodes werestudied towards the electrochemical reduction of oxygen in aqueous and non-aqueous solutions. The reaction of 1-chloro-9,10-anthraquinone with aliphatic diamines was applied for the synthesis of amino-9,10-anthraquinone derivatives. The obtained AQ derivatives were grafted onto the surface of glassy carbon electrodes by electropolymerisation...
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Electrochemical properties and bioactivity of hydroxyapatite coatings prepared by MEA/EDTA double-regulated hydrothermal synthesis
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Structural and Magnetic Properties of Co‒Mn Codoped ZnO Nanoparticles Obtained by Microwave Solvothermal Synthesis
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Silica-Polyethylene Glycol Matrix Synthesis by Sol-Gel Method and Evaluation for Diclofenac Diethyloammonium Release
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The mechanical properties and conduction of solid polyurethane electrolytes depending on the methods of synthesis and LiClO4 content as addition
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Tetraalkylammonium acetates and tetraalkylammonium tetrafluoroborates as new templates for room-temperature synthesis of mesoporous silica spheres
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Sulforaphane, a cruciferous vegetable-derived isothiocyanate, inhibits protein synthesis in human prostate cancer cells
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Synthesis of new polycyclic anthracenodione analogs with hetero- or carbocyclic ring(s) fused to the chromophore system
PublicationZsyntezowano serię nowych analogów antracenodionów z różnymi pierścieniami hetero- lub karbocyklicznymi sprzężonymi z układem chromoforowym. Związki te mogą stanowić nową klasę pochodnych antracenodionów o potencjalnej zdolności pokonywania oporności wielolekowej komórek nowotworowych.
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New amino acid propyl ester ibuprofenates from synthesis to use in drug delivery systems
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Novel method of expression and purification of hirudin based on pBAD TOPO, pTYB12 vectors and gene synthesis
PublicationW pracy przedstawiono nową, szybką i tanią metodę otrzymywania, ekspresji i oczyszczania białka hirudyny naturalnie izolowanego z ślinianek pijawki lekarskiej. Hirudyna pełni funkcje bezpośredniego inhibitora trombiny, głównego białka biorącego udział w tworzeniu skrzepów krwi. Właściwości te wykorzystywane są od wielu lat w klinice. Opracowana metoda pozwoliła uzyskać 17 mg/l hodowli E. coli białka o wysokiej czystości i aktywności...
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Ag modified ZnO microsphere synthesis for efficient sonophotocatalytic degradation of organic pollutants and CO2 conversion
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Trichrome Mallory's stain may indicate differential rates of RNA synthesis in eutopic and ectopic endometrium.
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Synthesis and SAR-study for novel arylpiperazine derivatives of 5-arylidenehydantoin with α1-adrenoceptor antagonistic properties
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Synthesis and Comprehensive Structural and Chiroptical Characterization of Enones Derived from (−)-α-Santonin by Experiment and Theory
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Poly(amidoamine) Dendrimer/Camptothecin Complex: From Synthesis to In Vitro Cancer Cell Line Studies
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Synthesis and Testing of BCZY/LNZ Mixed Proton–electron Conducting Composites for Fuel Cell Applications
PublicationA composite of BaCe0.6Zr0.2Y0.2O3–δ and Li2O:NiO:ZnO was investigated for fuel cell applications. The composite was successfully synthesized and its phase stability was confirmed at temperatures up to 900 °C. The influence of sintering and pressing aids on density was also investigated. Electrical properties were measured. DC electrical conductivity was about 8•10-4 S/m at 845 K. Open circuit voltage measurements in wet hydrogen...
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The ILs-assisted solvothermal synthesis of TiO2 spheres: the effect of ionic liquids on morphology and photoactivity of TiO2
PublicationEffect of the ionic liquid (IL) structure (chain length in the imidazolium cation) on morphology and photoactivity of TiO2 particles has been systematically investigated. The TiO2 microspheres have been successfully synthesized via facile solvothermal method assisted by ionic liquids, such as 1-butyl-3-methylimidazolium chloride [BMIM][Cl] and 1-decyl-3-methylimidazolium chloride [DMIM][Cl] using tetra-tert-butyl orthotitanate...
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New Method for the Synthesis of Azocrown Compounds Containing Oxygen, Nitrogen and Oxygen, or Sulfur Atoms in the Macroring.
PublicationW publikacji opisano nową metodę syntezy azokoron z różnymi heteroatomami w makrocyklu i o różnej wielkości molekularnej wnęki. Metoda ta polega na reakcji 2,2´-difluoroazobenzenu z diolami, diaminami, aminodiolami i ditiolamiw obecności zasady.
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Silica nanospheres as a key process element in the Green engineering for the synthesis of carbon nanotubes as a supercapacitors additives
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Waste-free synthesis of silica nanospheres and silica nanocoatings from recycled ethanol–ammonium solution
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Kinetics study of the fully bio-based poly(propylene succinate) synthesis. Functional group approach
PublicationCurrently, the increasing importance of the bio-based chemical compounds development is visible in the polymer chemistry, chemical engineering and materials science. It is well-known that the various purity level and different contaminants characterize petrochemical-based compounds compared to their biobased counterparts. Therefore, it is necessary to find out the contaminants impact on the bio-based monomers synthesis. One of...
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Synthesis of 3-Carbamoyl b-Lactams via Manganese(III)-Promoted Cyclization of N-Alkenylmalonamides
PublicationManganese(III)-promoted cyclization of N-alkenylmalonamides (¼N-alkenylpropanediamides) gave 3-(aryl/(alkylamino)carbonyl) b-lactams as well as 3-(aryl/(alkylamino)thiocarbonyl) b-lactams. The relative configuration of the obtained products was unambiguously determined by X-ray crystallography. The proposed method is very useful for the one-pot synthesis of a number of 3-(aryl/ (alkylamino)carbonyl) b-lactams, especially those...
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Fluorescent analogs of trypsin inhibitor SFTI-1 isolated from sunflower seeds-synthesis and applications
PublicationThis article describes the synthesis and enzymatic study of newly synthesized analogs of trypsin inhibitors SFTI-1 that were fluorescent labeled on their N-terminal amino groups. Two fluorescent derivatives of benzoxazole (3-[2-(4-diphenylaminophenyl) benzoxazol-5-yl]-L-alanine[(4NPh(2)) Ph] Box-Ala and 3-[2-(2', 4', 5'-trimethoxyphenyl) benzoxazol-5-yl]-l-alanine-[2,4,5-(OMe)3Ph] Box-Ala) were used as efficient fluorescent labels....