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Search results for: FREEZE-CASTING
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Usuwanie hydrofobowych zanieczyszczeń ropopochodnych z gleby metodą odmywania za pomocą roztworów związków powierzchniowo czynnych = Washing out of hydrophobic organic pollutants from soil using surfactants solutions
PublicationBadano efektywność oczyszczania gleby zanieczyszczonej substancjami ropopochodnymi. W badaniach wykorzystano surfaktanty niejonowe z grupy oksyetylenowanych alkoholi tłuszczowych i alkilopoliglukozydów oraz biosurfaktant z grupy ramnolipidów. Efektywność odmycia gleby w zależności od rodzaju surfaktantów wahała się od 67 do 78% przy stężeniu surfaktantu 3 g/L. Wraz ze wzrostem stężenia surfaktantu w roztworze obserwowano wzrost...
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Application of Headspace Solid-phase Microextraction with Poly(1-vinyl-3- Hexylimidazolium Chloride) Polymeric Ionic Liquid Coating using GC - MS to Determine Volatile Fatty Acids in Dairy Wastewater
PublicationVolatile fatty acids were determined in this study using headspace solid-phase microextraction (HS-SPME) with a poly(1-vinyl-3-hexylimidazolium chloride) polymeric ionic liquid coated fiber followed by gas chromatography - mass spectrometry. Experimental parameters such as extraction time and temperature, sample volume as well as desorption time and temperature were optimized. Detection limits of the method were in the range of...
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Analysis of free vibrations of cantilever bars with parabolically variable cross-sections using the Rayleigh’s method
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Polymer-free cubosomes for simultaneous bioimaging and photodynamic action of photosensitizers in melanoma skin cancer cells
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PARTIAL WHEAT FLOUR REPLACEMENT WITH GLUTEN-FREE FLOURS IN BREAD - QUALITY, TEXTURE AND ANTIOXIDANT ACTIVITY
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The anion [Mg6Cl8Cp*5]-: a final intermediate on the way to the molecular donor-free Grignard compound MgClCp*?
PublicationOtrzymano i scharakteryzowano strukturalnie rzadki przypadek związku Grignarda pozbawionego donora. Struktura krystaliczna [Mg6Cl8Cp*5][AlCp*2] C6H6 zawiera zarówno metallocen (Cp*AlCp*) jak i odwrócony metallocen (MgCp*Mg).
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A comparison of three solvent-free techniques coupled with gas chromatography for determining trihalomethanes in urine samples
PublicationDążenie do oznaczania lotnych analitów organicznych w próbkach płynów biologicznych charakteryzujących się złożonym, a często zmiennym składem matrycy, stanowi siłę napędową do działań analityków w zakresie poszukiwania nowych rozwiązań metodycznych i aparaturowych. Publikacja ta przedstawia porównanie trzech technik zastosowanych do tych celów: technikę analizy fazy nadpowierzchniowej z generacją strumienia ciekłego sorbentu...
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Role of nitrogen in optical and electrical band gaps of hydrogenated/hydrogen free carbon nitride film
PublicationWe report the optical and electrical band gap energy of amorphous hydrogenated carbon nitride (a-HCNx) and carbon nitride (a-CNx) as a function of nitrogen concentration (N/C). The optical band gap of a-HCNx and a-CNx films has been determined by means of Ellipsometry and UV-VIS. Both optical and electrical band gaps increase with elevated nitrogen concentration. Experimentally obtained electrical band gap is compared with the...
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Hunting for the Magnesium(I) Species: Formation, Structure, andReactivity of some Donor-Free Grignard Compounds
PublicationMagnesium bromide radicals have to be prepared as high-temperature molecules and trapped as a metastable solution because a seemingly simple reduction of donor-free Grignard compounds failed. However, the essential role of magnesium(I) species during the formation of Grignard compounds could be demonstrated experimentally.
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A chromatography-free total synthesis of a ferrocene-containing dendrimer exhibiting the property of recognizing 9,10-diphenylanthracene
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Role of biochar-based free radicals in immobilization and speciation of metals in the contaminated soil-plant environment
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FeCl3-Modified Carbonaceous Catalysts from Orange Peel for Solvent-Free Alpha-Pinene Oxidation
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Microstructural and Mechanical Properties of Novel Co-Free Maraging Steel M789 Prepared by Additive Manufacturing
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Free volume in physical absorption of carbon dioxide in ionic liquids: Molecular dynamics supported modeling
PublicationUnderstanding the mechanisms underlying the carbon dioxide (CO2) absorption in ionic liquids (ILs) is the key to their efficient utilization in industrial flue gas treatment. One of the parameters considered substantially important in the process is the Free Volume. In this study, the Fractional Free Volume (FFV) of 73 ILs was calculated using Molecular Dynamics (MD). A quantitative Structure-Property Relationship (QSPR) study...
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Separation of surfactant functionalized single-walled carbon nanotubes via free solution electrophoresis method
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Waste-free synthesis of silica nanospheres and silica nanocoatings from recycled ethanol–ammonium solution
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Fe local structure in Pt-free nitrogen-modified carbon based electrocatalysts: XAFS study
PublicationThe paper presents a new results on the bonding environment (coordination number and geometry) and on oxidation states of Fe in nitrogen-modified Fe/C composites used as Pt-free catalysts for oxygen reduction in Direct Hydrogen Fuel Cells. Starting from glucose or fructose, two catalysts displaying different electrochemical performance were prepared and studied in the form of pristine powder and thin catalytic layer of electrode...
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Quantitative study of free convective heat losses from thermodynamic partitions using Thermal Imaging
PublicationThe following paper presents a simple method of determining the presence, distribution and values of heat losses from external building walls as thermodynamic partitions using a Thermal Imaging Camera (TIC). According to Fourier's equation, the value of heat loss is proportional to the temperature gradient ∂t/∂y|y=0 in air in the y direction perpendicular to the heated surface. Unfortunately, air temperature cannot be measured...
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The Effect of Sterols on Amphotericin B Self-Aggregation in a Lipid Bilayer as Revealed by Free Energy Simulations
PublicationAmphotericin B (AmB) is an effective but toxic antifungal drug, known to increase the permeability of the cell membrane, presumably by assembling into transmembrane pores in a sterol-dependent manner. The aggregation of AmB molecules in a phospholipid bilayer is, thus, crucial for the drug’s activity. To provide an insight into the molecular nature of this process, here, we report an atomistic molecular dynamics simulation study...
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Helium-assisted, solvent-free electro-activation of 3D printed conductive carbon-polylactide electrodes
PublicationFused filament fabrication is one of the most rapidly developing 3D printing techniques, with numerous applications, including in the field of applied electrochemistry. Here, the utilisation of conductive carbon black polylactic acid (CB-PLA) for 3D printouts is the most promising. To use CB-PLA as an electrode material, an activation process must be performed, removing the polymer matrix and uncovering the electrically conductive...
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A general isogeometric finite element formulation for rotation‐free shells with in‐plane bending of embedded fibers
PublicationThis article presents a general, nonlinear isogeometric finite element formulation for rotation-free shells with embedded fibers that captures anisotropy in stretching, shearing, twisting, and bending - both in-plane and out-of-plane. These capabilities allow for the simulation of large sheets of heterogeneous and fibrous materials either with or without matrix, such as textiles, composites, and pantographic structures. The work...
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What matters most to patients? On the Core Determinants of Patient Experience from Free Text Feedback
PublicationFree-text feedback from patients is increasingly used for improving the quality of healthcare services and systems. A major reason for the growing interest in harnessing free-text feedback is the belief that it provides richer information about what patients want and care about. The use of computational approaches such as structural topic modelling for analysing large unstructured textual data such as free-text feedback from patients...
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Convenient and efficient N-methylation of secondary amines under solvent-free ball milling conditions
PublicationIn the present work, we report the development of a rapid, efcient, and solvent-free procedure for the N-methylation of secondary amines under mechanochemical conditions. After optimization of the milling parameters, a vibrational ball mill was used to synthesize 26 tertiary N-methylated amine derivatives in a short time of 20 min (30 Hz frequency) and high yields ranging from 78 to 95%. An exception was compounds having a hydroxyl...
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Reference-free determination of debonding length in reinforced concrete beams using guided wave propagation
PublicationThis paper presents theoretical and experimental investigations of guided wave propagation in reinforced concrete beams, with pre-existing debonding between steel rebars and concrete blocks, for the purpose of damage detection. The primary aim of these investigations was a detailed analysis of the possible applications of wave propagation in single and multiple debonding detection in reinforced concrete structures and reference-free...
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General, Mild, and Metal-Free Functionalization of Indole and Its Derivatives Through Direct C3-Selenylation
PublicationA very mild method for the introduction of functionalized alkylselenyl group at C-3 position of the indole ring was developed. The proposed procedure consists of an electrophilic substitution of indole and its derivatives with bis(O,O-diisopropoxyphosphorothioyl) diselenide and subsequent cleavage of the P–Se bond with tetrabutylammonium fluoride in the presence of various electrophilic reagents. This method can be successfully...
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Simultaneous optical and electrochemical label-free biosensing with ITO-coated lossy-mode resonance sensor
PublicationIn this work we discuss a new label-free biosensing device based on indium tin oxide (ITO) overlaid section of a multimode optical fiber fused silica core. The sensor has been used to optical measurements also simultaneously interrogated electrochemically (EC). Due to optimized thickness and optical properties of ITO film, a lossy-mode resonance (LMR) could be observed in the optical domain, where electrical properties of the film...
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A Flexible Nafion Coated Enzyme‐free Glucose Sensor Based on Au‐dimpled Ti Structures
PublicationThe detection of glucose at low concentrations using electrochemical sensors is of great importance due to the possibility of using different human body fluids than blood, such as e.g. urine, saliva, sweat or tears. The interest behind those biofluids is related to their utility in non-invasive sugar determination. In this work, we present flexible, fully biocompatible electrode material based on Au nanoparticles immobilized onto...
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Implicit versus explicit finite volume schemes for extreme, free surface water flow modelling.
PublicationPrzedstawiono jeden jawny i trzy niejawne schematy metody objętości skończonych. Porównano własności tych schematów oraz oceniono możliwości ich stosowania do modelowania gwałtownych przepływów w kanałach otwartych. Zaproponowano modyfikację schematu niejawnego. Poprawiony schemat może być stosowany do obliczeń przepływu szybkozmiennego w kanałach otwartych i w sieciach kanalizacyjnych.
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Inter-rater reliability of the Brief Psychiatric Rating Scale and the Groningen Social Disabilities Schedule in a European multi-site randomized controlled trial on the effectiveness of acute psychiatric day hospitals
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The Influence of PEG on Morphology of Polyurethane Tissue Scaffold
PublicationIn this study, polyurethanes (PU) were synthesized from oligomeric dihydroxy(etylene-butylene adipate), poly(ethylene glycol) (PEG), hexamethylene diisocyanate (HDI), 1,4-butanediol (BDO) as chain extender and stannous octoate as catalyst. PEG due to its hydrophilic character influences physical and chemical properties of PU. For testing were used PU having the following weigh contents of PEG: 0%, 7%, and 14%. Porous scaffolds...
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Justyna Płotka-Wasylka dr hab. inż.
PeopleUrodziła się w Słupsku (24.03.1986).W 2005 roku ukończyła I Liceum Ogólnokształcące im. Jana II Sobieskiego w Wejherowie i rozpoczęła studia na Wydziale Chemicznym Politechniki Gdańskiej. Po ich ukończeniu w 2010 rozpoczęła pracę naukową na tej uczelni, uzyskując w 2014 roku stopień doktora nauk chemicznych. Tematem jej rozprawy doktorskiej, wykonywanej pod kierunkiem prof. Marka Biziuka oraz dr Caluma Morrisona (Uniwersytet w...
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DLC coating doped with W in ring-on-ring sliding with water lubrication 20MPa/0.1m/s
Open Research DataWear tests in sliding friction of 1% W (tungsten) doped DLC coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, DLC-W over DLC-W. Mean contact stress: 20MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: WATER. Tribometer: PT-3. Overall test time >15h. The test was...
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DLC coating doped with W in ring-on-ring sliding with water lubrication 10MPa/0.1m/s
Open Research DataWear tests in sliding friction of 1% W (tungsten) doped DLC coating on 1.4021 (EN 10088-1) heat treated stainless steel. Ring - on - ring contact in unidirectional sliding, DLC-W over DLC-W. Mean contact stress: 10MPa. Sliding velocity: 0,1 m/s. Mean friction radius: 9.5mm. Lubricant: WATER. Tribometer: PT-3. Overall test time >15h. The test was...
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PULSE and ECG measurement from the hand with standing - hands resting on the device - Man 29 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with standing - hands resting on the device - Woman 27 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with standing - hands resting on the device - Woman 28 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows resting on the armrests of the chair - Woman 28 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows resting on the table top - Man 29 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows resting on the table top - Woman 28 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows resting on the armrests of the chair - Man 29 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows resting on the table top - Woman 27 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows resting on the armrests of the chair - Woman 27 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows resting on the armrests of the chair - Woman 30 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows resting on the table top - Man 30 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows resting on the table top - Woman 30 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with standing - hands resting on the device - Woman 24 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows resting on the table top - Woman 24 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows resting on the armrests of the chair - Man 53 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with standing - hands resting on the device - Man 53 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...
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PULSE and ECG measurement from the hand with elbows resting on the armrests of the chair - Woman 24 age
Open Research DataThe data set presents the measurements of the pulse and the ECG signal from the hand made with the use of a proprietary measuring system based on the AD8232 chip, a set of green diode and a phototransistor made on the STM32 microcontroller. Thanks to such a constructed device, it is possible to measure the ECG signal in a non-standard way - from the...