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Wyniki wyszukiwania dla: PHASE CHANGE MATERIALS
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Investigations on mixture preparation for two phase adiabatic pressure drop of R134a flowing in 5 mm diameter channel
PublikacjaThe article presents detailed two-phase adiabatic pressure drops data for refrigerant R134a. Study cases have been set for a mass flux varying from 200 to 400 kg/m2 s, at the saturation temperature of 19.4 ◦C. Obtained experimental data was compared with the available correlations from the literature for the frictional pressure drop during adiabatic flow. Influence of mixture preparation on pressure drop was investigated, for...
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Determination of volatile organic compounds in water samples using membrane-solid phase microextraction (M-SPME) (headspace version)
PublikacjaThe results of a study on the use of membrane-solid phase microextraction (M-SPME) for sampling volatile organic compounds (VOCs) from the headspace above the liquid medium are presented. The sampled VOCs were subsequently quantified by gas chromatography (GC). Two systems were compared in this study, i.e. a novel two-phase sorption system (M-SPME), and a commercial fibre. Headspace sampling using SPME was optimized with respect...
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Powering the Future by Iron Sulfide Type Material (FexSy) Based Electrochemical Materials for Water Splitting and Energy Storage Applications: A Review
PublikacjaWater electrolysis is among the recent alternatives for generating clean fuels (hydrogen). It is an efficient way to produce pure hydrogen at a rapid pace with no unwanted by-products. Effective and cheap water-splitting electrocatalysts with enhanced activity, specificity, and stability are currently widely studied. In this regard, noble metal-free transition metal-based catalysts are of high interest. Iron sulfide (FeS) is one...
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First deep eutectic solvent-based (DES) stationary phase for gas chromatography and future perspectives for DES application in separation techniques
PublikacjaThe paper presents the first application of deep eutectic solvents (DES) as stationary phases for gas chromatography. DES obtained by mixing tetrabutylammonium chloride (TBAC) as a hydrogen bond acceptor (HBA) with heptadecanoic acid being a hydrogen bond donor (HBD) in a mole ratio of HBA:HBD equal to 1:2 was characterized by its ability to separate volatile organic compounds (VOCs). The Rohrschneider – McReynolds constants determined...
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Coupled evolution of preferential paths for force and damage in the pre-failure regime in disordered and heterogeneous, quasi-brittle granular materials.
PublikacjaMetoda elementów dyskretnych (DEM) została wykorzystana do symulacji betonu poddanego jednoosiowemu rozciąganiu. Beton modelowano jako materiał losową heterogeniczy 2/3-fazowy, złożony z cząstek kruszywa, matrycy cementowej i stref przejściowych międzyfazowej. Odkryto dowody na zoptymalizowaną transmisję siły, scharakteryzowaną przez dwa nowe wzorce, które przewidują i wyjaśniają sprzężoną ewolucję ścieżki siły i uszkodzenia od...
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A nontargeted approach to determine the authenticity of Ginkgo biloba L. plant materials and dried leaf extracts by liquid chromatography-high-resolution mass spectrometry (LC-HRMS) and chemometrics
PublikacjaThe lack of stringent regulations regarding raw materials for herbal supplements used for medicinal purposes has been a constant challenge in the industry. Ginkgo biloba L. leaf extracts attract consumers because of the supposed positive effect on mental performance and memory. Supplements are produced using dried leaf materials and standardized leaf extracts such as EGb 761. Adulteration of Ginkgo biloba L. plants and extracts...
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Induction Assisted Hybrid Friction Stir Welding of Dissimilar Materials AA5052 Aluminium Alloy and X12Cr13 Stainless Steel
PublikacjaThis research aimed to study the induction in-situ heated hybrid friction stir welding (IAFSW) method to join AA5052 aluminium alloy with X12Cr13 stainless steel (SS) to enhance joint strength. The potency of this method on the mechanical properties and microstructural characterizations were also investigated. The results show that the transverse tensile strength gained was 94% of the AA5052 base metal that is 229.5 MPa. This superior...
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Low-Cost Unattended Design of Miniaturized 4 × 4 Butler Matrices with Nonstandard Phase Differences
PublikacjaDesign of Butler matrices dedicated to Internet of Things and 5th generation (5G) mobile systems—where small size and high performance are of primary concern—is a challenging task that often exceeds capabilities of conventional techniques. Lack of appropriate, unified design approaches is a serious bottleneck for the development of Butler structures for contemporary applications. In this work, a low-cost bottom-up procedure for...
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Polymeric metal‐containing ionic liquid sorbent coating for the determination of amines using headspace solid‐phase microextraction
PublikacjaThis study describes the design, synthesis, and application of polymeric ionic liquid sorbent coatings featuring nickel metal centers for the determination of volatile and semivolatile amines from water samples using headspace solidphase microextraction. The examined polymeric ionic liquid sorbent coatings were composed of two ionic liquid monomers (tetra(3-vinylimidazolium)nickel bis[(trifluoromethyl)sulfonyl]imide [Ni2+(VIM)4]...
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Quantitative structure—retention relationships of some steroid and phenanthrene derivatives on cyano-, reversed-phase, and normal-phase thin-layer chromatography stationary phases
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The valance state of vanadium-key factor in the flexibility of potassium vanadates structure as cathode materials in Li-ion batteries
PublikacjaPotassium hexavanadate (K2V6O16·nH2O) nanobelts have been synthesized by the LPE-IonEx method, which is dedicated to synthesis of transition metal oxide bronzes with controlled morphology and structure. The electrochemical performance of K2V6O16·nH2O as a cathode material for lithium-ion batteries has been evaluated. The KVO nanobelts demonstrated a high discharge capacity of 260 mAh g−1, and long-term cyclic stability up to 100...
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Physical properties of homogeneous TiO2 films prepared by high power impulse magnetron sputtering as a function of crystallographic phase and nanostructure
PublikacjaOptical, photo-electrochemical, crystallographic and morphological properties of TiO2 thin films prepared by high power impulse magnetron sputtering at low substrate temperatures (<65 ◦C) without post-deposition thermal annealing are studied. The film composition-anatase, rutile or amorphous TiO2-is adjusted by the pressure (p ∼ 0.75-15 Pa) in the deposition chamber. The different crystallographic phases were determined with grazing...
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Enhanced formability and forming efficiency for two-phase titanium alloys by Fast light Alloys Stamping Technology (FAST)
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Evaluation of Linkers’ Influence on Peptide-Based Piezoelectric Biosensors’ Sensitivity to Aldehydes in the Gas Phase
PublikacjaRecent findings qualified aldehydes as potential biomarkers for disease diagnosis. One of the possibilities is to use electrochemical biosensors in point-of-care (PoC), but these need further development to overcome some limitations. Currently, the primary goal is to enhance their metrological parameters in terms of sensitivity and selectivity. Previous findings indicate that peptide OBPP4 (KLLFDSLTDLKKKMSEC-NH2) is a promising...
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Experimental study on single phase operation of microjet augmented heat exchanger with enhanced heat transfer surface
PublikacjaThe article presents experimental investigations on a prototype heat exchanger. Presented research is focused on combined active and passive enhancement techniques of surface modification and microjet impingement. The results were compared to reference plate heat exchanger without microjet impingement. The Wilson plot method was applied to determine the heat transfer coefficients in the single phase operation. The heat exchanger...
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Energy-based fatigue failure characteristics of materials under random bending loading in elastic-plastic range
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Effect of Nitrogen Ion Implantation on the Cavitation Erosion Resistance and Cobalt-Based Solid Solution Phase Transformations of HIPed Stellite 6
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Sensitive simultaneous determination of 19 fluorobenzoic acids in saline waters by solid-phase extraction and liquid chromatography–tandem mass spectrometry
PublikacjaA solid-phase extraction (SPE) procedure using C18 stationary phase was optimized for the preconcentration of 19 fluorinated derivatives of benzoic acid (FBA): mono-, di-, tri-, and tetrafluorosubstituted in the ring, trifluoromethylbenzoic acid and 3,5-bistrifluoromethyl benzoic acid from undiluted salt-rich (>20%) reservoir waters. Quantitative (>90%) retention/elution of 16 out of 19 analyte compounds was achieved allowing a...
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Two-phase optimizing approach to design assessments of long distance heat transportation for CHP systems
PublikacjaCogeneration or Combined Heat and Power (CHP) for power plants is a method of putting to use waste heat which would be otherwise released to the environment. This allows the increase in thermodynamic efficiency of the plant and can be a source of environmental friendly heat for District Heating (DH). In the paper CHP for Nuclear Power Plant (NPP) is analyzed with the focus on heat transportation. A method for effectivity and feasibility...
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Preparation and evaluation of 1,3-alternate 25,27-bis-(pentafluorobenzyloxy)-26,28-bis-(3-propyloxy)-calix[4]arene-bonded silics gel high performance liquid chromatography stationary phase
PublikacjaA 1,3-alternate 25,27-bis-(pentafluorobenzyloxy)-26,28-bis-(3-propyloxy)-calix[4]arene-bonded silica gel stationary phase (CalixBzF10) was synthesized, structurally characterized, and used as a selector in liquid chromatography. The selectivity study of this phase was done by using fluorine-containing compounds (fluorobenzenes, fluoro-pyrimidine bases), as well as non-fluorinated analytes (non-steroidal anti-inflammatory drugs,...
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Towards the Application of Structure-Property Relationship Modeling in Materials Science: Predicting the Seebeck Coefficient for Ionic Liquid/Redox Couple Systems
PublikacjaThis work focuses on determining the influence of both ionic liquid (IL) type and redox couple concentration on Seebeck coefficient values of such a system. The quantitative structure property relationship (QSPR) and read-across techniques are proposed as methods to identify structural features of ILs (mixed with LiI/I2 redox couple), which have the most influence on the Seebeck coefficient (Se) values of the system. ILs consisting...
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SiC-based phase-shift dual half bridge DC-DC converter as a key component of multilevel cascaded MV converters
PublikacjaThe paper describes SiC-based dual half bridge (DHB) DC-DC converter considered as a key component of high frequency isolated multilevel cascaded medium voltage converters. Two topologies of bi-directional DC-DC converters: the resonant half-bridge DC-DC converter and the phase-shift DHB converter are compared in the paper. Experimental results of SiC-based 50 kHz DHB DC-DC converter are presented in the paper.
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Electrode materials for electrochemical capacitors based on poly(3,4-ethylenedioxythiophene) and functionalized multi-walled carbon nanotubes characterized in aqueous and aprotic electrolytes
PublikacjaWithin this work, we report a facile one-stage synthesis of nanocomposites based on functionalized carbon nanotubes (CNTs) and electroactive polymer poly(3,4-ethylenedioxythiophene). Three different composites are investigated as potential electrode materials for the electrochemical capacitors. Two of the composites contain carbon nanotubes (ox-CNTs), functionalized by acid oxidation process (65% HNO3, 120 °C). The third composite...
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High Efficiency Dual-Active-Bridge Converter with Triple-Phase-Shift Control for Battery Charger of Electric Vehicles
PublikacjaAn optimal modulation scheme with triple-phase-shift (TPS) control could increase the efficiency in the entire load range for a dual-active-bridge (DAB) converter under wide output voltage range conditions. Therefore, this study proposes a convergent approach to TPS mode selection, coupled with an optimal modulation scheme, ensuring the circuit’s efficiency over the entire range in the realm of a high-power and high-efficiency...
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Microstructure and nanomechanical properties of single stalks from diatom Didymosphenia geminata and their change due to adsorption of selected metal ions
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Effects of Flywheel vs. Free-Weight Squats and Split Squats on Jumping Performance and Change of Direction Speed in Soccer Players
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Ti-doped Sr2Fe1.4-xTixMo0.6O6-δ double perovskites with improved stability as anode materials for Solid Oxide Fuel Cells
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Selective Laser Sintering And Melting Of Pristine Titanium And Titanium Ti6Al4V Alloy Powders And Selection Of Chemical Environment For Etching Of Such Materials
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Deep insight into the pore size distribution of N-doped porous carbon materials on electrochemical energy storage and CO2 sorption
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Balancing energy consumption in limited power grid with active front-end and three phase dual active bridge system
PublikacjaPaper deals with simulation analysis of bidirectional power converters system for charging station of electric vehicle in condition of limited power source in city infrastructure. In case of incapability to provide additional power supply through the grid by virtue of historical, architectural and economic reasons it is possible to solve this issue by implementation of mobile battery-powered supply source. The proposed bidirectional...
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Tuning Cu-Content La1−xSrxNi1−yCuyO3−δ with Strontium Doping as Cobalt-Free Cathode Materials for High-Performance Anode-Supported IT-SOFCs
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Design and Utility of Specialist Comminution Set-Up for Plastics and Organic Materials
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Wear measurements of self-lubricating bearing materials in small oscillatory movement
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Production of gaseous matrix-free reference materials. Application of thermoanalytical techniques
PublikacjaMateriały odniesienia są wykorzystywane w każdym laboratorium w celu zapewnienia jakości wyników pomiarów analitycznych. Produkcja materiałów odniesienia nie jest zadaniem łatwym, szczególnie w przypadku składników gazowych, toksycznych i o nieprzyjemnym zapachu. Termiczny rozkład związków powierzchniowych jest bardzo dogodnym sposobem sporządzania właśnie tego rodzaju mieszanin. Ważną rolę w procesie termicznego rozkładu związków...
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Functionalized azobenzocrown ethers as sensor materials—The synthesis and ion binding properties
PublikacjaNew 13- and 16-membered azobenzocrown ethers with aromatic amino, amide, ether–ester or ether–amide residue in para position to an azo moiety were obtained. Acid–base properties and ion binding ability of the colored compounds were studied by spectroscopic methods: UV–vis, fluorimetry and 1H NMR spectroscopy. Selected azobenzocrowns were tested as ionophores in ion-selective membrane electrodes (ISEs) – classic and miniature all...
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Emulsifi ers from renewable materials: an eco-friendly synthesis and properties
PublikacjaThe focus of this study was the preparation of novel bio based polyglycerol emulsifiers characterized by a one pot synthesis, thus by modified properties with respect to interfacial activity and effectiveness as emulsion stabilizers. The final products of the esterification process, carried out in the presence of carboxylates were used directly as emulsifiers (without purification or fractionation). Polyglycerol emulsifiers obtained...
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Standard gas mixtures – indispensable reference materials in the analysis of gaseous media
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Porous Selective Laser Melted Ti and Ti6Al4V Materials for Medical Applications
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Structural, thermal and photocatalytic properties of composite materials SiO2/TiO2/C
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Wear measurements of self lubricating bearing materials in small oscillatory movement
PublikacjaRosnące wymagania ekologiczne powodują wzrost tendencji wymiany klasycznych materiałów łożyskowych, wymagających dodatkowego czynnika smarnego, na materiały nie wymagające smarowania. Zamianie takiej może towarzyszyć obniżenie trwałości zmodernizowanego łożyska. Ten niekorzystny efekt nierzadko obserwuje się w węzłach łożyskowych kierownic turbin wodnych. Autorzy podjęli próbę wyjaśnienia zjawisk występujących w tego typu łożyskach....
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Effect of starch fillers on the dynamic mechanical properties of rubber biocomposite materials
PublikacjaIn the paper the results of dynamic mechanical study of the biocomposites containing one of two types of (potato or corn) strach used as fillers in different amount were discussed. The composites were obtained from rubbery mixture containing natural rubber (NR) as a main component. Thermomechanical analyses (by DMA) showed that the used quantity of strach fillers only slightly influence on the glass transition temperature of vulcanizates.
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Recent developments in the synthesis and applications of graphene-family materials functionalized with cyclodextrins
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Is Dialdehyde Chitosan a Good Substance to Modify Physicochemical Properties of Biopolymeric Materials?
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The Impact of the Quality of Tap Water and the Properties of Installation Materials on the Formation of Biofilms
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Absorbable sutures in general surgery – review, available materials, and optimum choices
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The Application of Phenolic Acids in The Obtainment of Packaging Materials Based on Polymers—A Review
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New Thiophene Imines Acting as Hole Transporting Materials in Photovoltaic Devices
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Theoretical analysis of current induced by high-energetic radiation in dielectric materials
PublikacjaW pracy poddano analizie mechanizmy generacji i rekombinacji nośników ładunku w obecności wysokoenergetycznego promieniowania. Przedstawiono zależności gęstości prądu elektrycznego od natężenia promieniowania i napięcia polaryzujacego próbkę.
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Explicit accumulation model for granular materials under multiaxial cyclic loading.
PublikacjaPróba korelacji parametrów modelu akumulacyjnego piasku z wynikami badań dynamicznych piasku.
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Estimation of optical parameters of highly scattering materials by time-of-flight spectroscopy.
PublikacjaPrzedstawiono metody wyznaczania podstawowych parametrów materiałów silnie rozpraszających światło na podstawie pomierzonego rozkładu czasu przelotu krótkich impulsów laserowych. W algorytmie wykorzystano metodę Monte Carlo i metodę dyfuzji do opisu propagacji światła. Oszacowano dokładność oszacowywania tych parametrów.