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Wyniki wyszukiwania dla: SOLID - PHASE MICROEXTRACTION
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Two-phase optimizing approach to design assessments of long distance heat transportation for CHP systems
PublikacjaCogeneration or Combined Heat and Power (CHP) for power plants is a method of putting to use waste heat which would be otherwise released to the environment. This allows the increase in thermodynamic efficiency of the plant and can be a source of environmental friendly heat for District Heating (DH). In the paper CHP for Nuclear Power Plant (NPP) is analyzed with the focus on heat transportation. A method for effectivity and feasibility...
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Preparation and evaluation of 1,3-alternate 25,27-bis-(pentafluorobenzyloxy)-26,28-bis-(3-propyloxy)-calix[4]arene-bonded silics gel high performance liquid chromatography stationary phase
PublikacjaA 1,3-alternate 25,27-bis-(pentafluorobenzyloxy)-26,28-bis-(3-propyloxy)-calix[4]arene-bonded silica gel stationary phase (CalixBzF10) was synthesized, structurally characterized, and used as a selector in liquid chromatography. The selectivity study of this phase was done by using fluorine-containing compounds (fluorobenzenes, fluoro-pyrimidine bases), as well as non-fluorinated analytes (non-steroidal anti-inflammatory drugs,...
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SiC-based phase-shift dual half bridge DC-DC converter as a key component of multilevel cascaded MV converters
PublikacjaThe paper describes SiC-based dual half bridge (DHB) DC-DC converter considered as a key component of high frequency isolated multilevel cascaded medium voltage converters. Two topologies of bi-directional DC-DC converters: the resonant half-bridge DC-DC converter and the phase-shift DHB converter are compared in the paper. Experimental results of SiC-based 50 kHz DHB DC-DC converter are presented in the paper.
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High Efficiency Dual-Active-Bridge Converter with Triple-Phase-Shift Control for Battery Charger of Electric Vehicles
PublikacjaAn optimal modulation scheme with triple-phase-shift (TPS) control could increase the efficiency in the entire load range for a dual-active-bridge (DAB) converter under wide output voltage range conditions. Therefore, this study proposes a convergent approach to TPS mode selection, coupled with an optimal modulation scheme, ensuring the circuit’s efficiency over the entire range in the realm of a high-power and high-efficiency...
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The influence of synthesis method on the microstructure and catalytic performance of Y 0.07 Sr 0.93 Ti 0.8 Fe 0.2 O 3-δ in synthetic biogas operated solid oxide fuel cells
PublikacjaThe Y0.07Sr0.93Ti0.8Fe0.2O3-δ (YSTF) material was fabricated using three different synthesis methods: modified polymer precursor method (MPP), Pechini method and a solid state reaction method. It was applied as an anode catalytic material for biogas reforming in solid oxide fuel cells. Clear differences in the microstructure of fabricated catalytic layers were found, mainly with respect to a grain size and distribution of grains....
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The pulse width modulation strategy for a five-phase three-level NPC voltage source inverter with DC-link voltage balancing ability
PublikacjaThe doctoral dissertation is all about the development of the space vector modulation algorithm for controlling the generation of output voltage vectors in a three-level, five-phase NPC inverter. The developed algorithm can be used to control five-phase motors, where it will be possible to increase the motor torque by 15%; by appropriate injection of 3rd harmonic current. The proposed control approach also opens up the possibility...
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Balancing energy consumption in limited power grid with active front-end and three phase dual active bridge system
PublikacjaPaper deals with simulation analysis of bidirectional power converters system for charging station of electric vehicle in condition of limited power source in city infrastructure. In case of incapability to provide additional power supply through the grid by virtue of historical, architectural and economic reasons it is possible to solve this issue by implementation of mobile battery-powered supply source. The proposed bidirectional...
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Functional phase bistability in a nanocrystalline RbMn[Fe(CN)6] thin film fabricated by matrix-assisted laser evaporation
PublikacjaOne of the main barriers hindering applications of Prussian blue metal assemblies is their poor processability, which makes the fabrication of intact thin films very difficult. In this work, a nanocrystalline RbMn[Fe(CN)6]·xH2O film on silicon substrate was obtained for the first time via laser-stimulated deposition and investigated. Temperature-induced phase transition and bistability within broad hysteresis loop (120 K), along...
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Characteristics of La0.8Sr0.2Ga0.8Mg0.2O3-delta -supported micro-tubular solid oxide fuel cells with bi-layer and tri-layer electrolytes
PublikacjaIn this study, La0.8Sr0.2Ga0.8Mg0.2O3−δ (LSGM)-supported micro tubular solid oxide fuel cells (T-SOFCs) with two different configurations, one containing an LSGM–Ce0.6La0.4O2−δ (LDC) bi-layer electrolyte (Cell A) and one containing an LDC–LSGM–LDC tri-layer electrolyte (Cell B), were fabricated using extrusion and dip-coating. After optimizing the paste formulation for extrusion, the flexural strength of the dense and uniform LSGM...
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Solid-Contact Ion-Selective Electrodes with Highly SelectiveThioamide Derivatives of p-tert-Butylcalix[4]arene for theDetermination of Lead(II) in Environmental Samples
PublikacjaThioamide derivatives of p-tert-butylcalix[4]arene were used as ionophores in the development of solid-contact ion-selective electrodes based on conducting polymer poly(3,4-ethylenedioxythiophene)/polystyrene sulfonate (PEDOT/PSS) which was synthesized by electrodeposition on the glassy carbon electrodes. The typical ion-selective membranes with optionally two different plasticizers [bis(2-ethylhexyl)sebacate (DOS) and 2-nitrophenyl...
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Analysis of IMS/NGN Call Processing Performance Using Phase-Type Distributions Based on Experimental Histograms
PublikacjaThe paper describes our further research done with the proposed analytical and simulation traffic models of the Next Generation Network (NGN), which is standardized for delivering multimedia services with strict quality and includes elements of the IP Multimedia Subsystem (IMS). The aim of our models of a single IMS/NGN domain is to evaluate two standardized call processing performance parameters, which appropriate values are very...
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Effect of lipid phase composition on autoxidation of water - in - oil emulsion
PublikacjaW pracy przedstawiono ocenę procesu autooksydacji emulsji W/O ze szczególnym uwzględnieniem składu fazy olejowej emulsji na postęp reakcji. Zbadano również wpływ wybranych antyoksydantów i emulgatorów na stabilność sporządzonych układów emulsyjnych.
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Phase Transitions in Pores: Experimental and Simulation Studies of Melting and Freezing
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Sensorless predictive control of three-phase parallel active filter
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36-pulse rectifier with a system of coupled three-phase reactors
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Interconnection of the Customer-Side Resources Using Single Phase VAPF
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Rich magnetic phase diagram in the Kagome-staircase compound Mn3V2O8
PublikacjaNa podstawie pomiarów podatności magnetycznej i ciepła właściwego monokryształu Mn3V2O8 skonstruowano diagram fazowy. Właściwości magnetyczne związku są silnie anizotropowe.
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Ifluence of geometrical and thermophysical parameters on two-phase thermosiphon performance
PublikacjaW pracy przedstawiono wyniki badań eksperymentalnych dotyczących wpływu geometrii pęku rur, rodzaju powierzni przejmowania ciepła parownika oraz płynu pośredniego na całkowitą wydajność dwufazowego termosyfonowego wymiennika ciepła (DTWC).
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The first order phase transition and superconductivity in BaNi2As2 single crystals
PublikacjaDyskutowane są synteza i właściwości fizyczne monokryształów BaNi2As2. BaNi2As2 krystalizuje w strukturze ThCr2Si2, a stałe sieciowe wynoszą odpowiednio: a = 4.112(4) A i c = 11.54(2) A. Pomiar oporu elektrycznego, zmiennopolowej podatności magnetycznej, ciepła właściwego, pokazują objętościowy efekt nadprzewodzący z Tc = 0.7 K.
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A study on application of Smoothed Particle Hydrodynamics to multi-phase flows
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Low-energy positron scattering from gas-phase uracil
PublikacjaQuantum scattering calculations are presented for the interaction of low energy positrons with the uracil molecule, an important component of biological systems. The rotational elastic and inelastic cross sections and vibrational inelastic cross sections are reported and compared with existing experiments, indicating a general trend of the cross sections different from the experimental findings and in line with what should be expected...
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CeIr3: superconductivity in a phase based on tetragonally close packed clusters
PublikacjaWe present the crystallographic analysis, superconducting and spectroscopic characterization, and theoretical modeling of CeIr3. Lattice parameters a = 5.2945(1) Å and c = 26.219(1) Å are found for the R-3m symmetry crystal structure, which are close to the literature values. CeIr3 is a moderate type-II superconductor (κ GL = 17, λ e–p = 0.65) below 2.5 K. Ce ions exhibit a strongly intermediate valence character as evidenced by...
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A study on application of Smoothed Particle Hydrodynamics to multi-phase flows
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Heat transfer characteristics of a two-phase thermosyphon heat exchanger
PublikacjaPrzedstawiono wyniki badań wpływu geometrii parownika, rodzaju rur użytych do budowy parownika, rodzaju cieczy pośredniej oraz poziomu cieczy nad najwyższym rzędem rur na działanie dwufazowego, termosyfonowego wymiennika ciepła. Zaprezentowano algorytm obliczeń przedstawionego wymiennika.
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Strong-coupling character of superconducting phase in compressed selenium hydride
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Charge Loss in Gas-Phase Multiply Negatively Charged Oligonucleotides
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Gradient reversed-phase high-performance chromatography of ionogenic analytes
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pH/Organic Solvent Double-Gradient Reversed-Phase HPLC
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Five-Phase EV Drive with Switched-Autotransformer (LCCAt) Inverter
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Cooperation of a Non-Linear Receiver with a Three-Phase Power Grid
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Pressure- and temperature-driven phase transitions in HgTe quantum wells
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The magnesium-palladium-silver system: Thermodynamic properties of the liquid phase
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Hydration phase diagram for sodium cobalt oxide Na0.3CoO2·yH2O
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Phase-locking of 19-core Yb3+ - doped optical fibre
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Phase-locking of 7-core Yb3+-doped optical fiber
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Phase Centre Corrections of GNSS Antennas and Their Consistency with ATX Catalogues
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A review on energy and cost effective phase separated pretreatment of biosolids
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Sensorless predictive control of three-phase parallel active filter
PublikacjaThe paper presents the control system of parallel active power filter (APF) with predictive reference current calculation and model based predictive current control. The novel estimator and predictor of grid emf is proposed for AC voltage sensorless operation of APF, regardless of distortion of this voltage. Proposed control system provides control of APF current with high precision and dynamics limited only by filter circuit parameters....
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Hydration phase diagram for sodium cobalt oxide NaxCoO2*yH2O
PublikacjaPrzedstawiony został diagram fazowy uwodnionego, sodowo kobaltowego związku tlenkowego Na0.3CoO2*yH2O. Diagram powstał w oparciu o zależność stopnia uwodnienia (y) od wilgotności względnej w temperaturze pokojowej. Zaobserwowano trzy fazy: y = 0, 0.6 i 0.13. Zauważono histerezę przy zamianie kierunku procesu uwadniania.
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Convective momentum and heat transfer in single and two-phase flows
PublikacjaW pracy przedstawiono dorobek autora w zakresie modeowania wymiany pędu i ciepław w przepływach jedno i dwufazowych.
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Computational analysis of substituent effects on proton affinity and gas-phase basicity of TEMPO derivatives and their hydrogen bonding interactions with water molecules
PublikacjaThe study investigates the molecular structure of 2,2,6,6-tetramethylpiperidine-1-oxyl (TEMPO) and its derivatives in the gas phase using B3LYP and M06-2X functional methods. Intermolecular interactions are analyzed using natural bond orbital (NBO) and atoms in molecules (AIM) techniques. NO2-substituted TEMPO displays high reactivity, less stability, and softer properties. The study reveals that the stability of TEMPO derivatives...
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Application of Potentiometric Taste Sensor with All Solid State Electrodes for Distinguishing of Red Dry Wines from Polish and French Vineyards
PublikacjaOpracowano nowy potencjometryczny czujnik smaku z sześcioma różnymi elektrodami typu All Solid State Electrode (ASSE). Każda z elektrod zawiera dwie warstwy: polimer przewodzący i membranę lipidowo-polimerową, w której rozpuszczone są poszczególne związki lipidowe. Potencjometryczny sensor smaku charakteryzuje się globalną selektywnością. Zastosowano go w celu odróżnienia próbek wytrawnych czerwonych win pochodzących z różnych...
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Corrosion degradation monitoring of ship stiffened plates using guided wave phase velocity and constrained convex optimization method
PublikacjaThe study presents an experimental investigation on the corrosion degradation level assessment using nondestructive wave-based methods. The degradation level of ship structural elements has been assessed in two different ways. The first one is based on the spectral decomposition and zero-crossing incorporated reconstruction of the dispersion curve approach of the antisymmetric Lamb wave mode and the best matching of the theoretical...
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Application of normal-phase high-performance liquid chromatography followed by gas chromatography for analytics of diesel fuel additives
PublikacjaThe paper presents the results of investigations on new procedures of determination of selected cleaning additives in diesel fuel. Two procedures: one-step analysis using gas chromatography with flame ionization detection (GC-FID) or mass spectrometry (GC-MS) and a two-step procedure in which normal-phase high-performance liquid chromatography (NP-HPLC) was used for preliminary separation of the additives, were compared. The additive...
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Emissions and toxic units of solvent, monomer and additive residues released to gaseous phase from latex balloons
PublikacjaThis study describes the VOCs emissions from commercially available latex balloons. Nine compounds are determined to be emitted from 13 types of balloons of different colors and imprints in 30 and 60°C. The average values of total volatile organic compounds (TVOCs) emitted from studied samples ranged from 0.054 up to 7.18 μg∙g-1 and from 0.27 up to 36.13 μg∙g-1 for 30oC and 60oC, respectively. The dataset is treated with principal...
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Numerical and experimental investigation of guided ultrasonic wave propagation in non-uniform plates with structural phase variations
PublikacjaThe article presents the results of numerical and experimental investigations of guided wave propagation in aluminum plates with variable thickness. The shapes of plate surfaces have been specially designed and manufactured using a CNC milling machine. The shapes of the plates were defined by sinusoidal functions varying in phase shift, which forced the changes in thickness variability alongside the propagation path. The main aim...
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Salt saturated single drop microextraction of gold from water samples and its determination by graphite furnace atomic absorption spectrometry
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Ultrasound-Assisted Dispersive Liquid-Liquid Microextraction Using Deep Eutectic Solvents (DESs) for Neutral Red Dye Spectrophotometric Determination
PublikacjaDeep eutectic solvents (DES), which have low toxicity and are low cost, biodegradable, and easily synthesized, were used for the extraction of neutral red (NR) dye before its spectrophotometric analysis. DES, containing choline chloride as a hydrogen bond acceptor and phenol as a hydrogen bond donor with a molar ratio of 1:2, was used for the extraction of NR dye from aqueous media. The possible interaction of different DESs with...
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Composite materials for Solid Oxide Fuel Cells - various ways of preparation and application
PublikacjaWykonano przeglad mozliwosci zastosowania materialow kompozytowych w wysokotemperaturowych tlenkowych ogniwach paliwowych oraz scharakeryzowano najbardziej popularne metody wytwarzania i nakladania tego typu materialow.
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Solid electrolyte gas sensors based on cyclic voltammetry with one active electrode
PublikacjaW artykule przedstawiono wyniki badań elektrokatalitycznego czujnika gazów toksycznych z jedną elektrodą aktywną.