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Wyniki wyszukiwania dla: BINBO4 CERAMICS, PRESSURELESS SINTERING, X-RAY DIFFRACTION, PHASE ANALYSIS, CRYSTAL STRUCTURE
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Properties of LiMnBO3 glasses and nanostructured glass-ceramics
PublikacjaPolycrystalline LiMnBO3 is a promising cathode material for Li-ion batteries. In this work, we investigated the thermal, structural and electrical properties of glassy and nanocrystallized materials having the same chemical composition. The original glass was obtained via a standard melt-quenching method. SEM and 7Li solid-state NMR indicate that it contains a mixture of two distinct glassy phases. The results suggest that the...
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The study of structure and surface morphology of lithium titanate sol-gel derived thin films
PublikacjaIn this paper the structure and the surface morphology of lithium titanate (LTO) thin films are presented. Nanocrystalline thin films were prepared by sol–gel method. To examine the influence of the annealing time on as-prepared films crystallization, the coatings were heated at different temperatures in the range of 500 °C–600 °C for 10, 20, 40 and 80 h. The structure of the obtained material was investigated using the X-ray diffraction...
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Testing Stability of Digital Filters Using Optimization Methods with Phase Analysis
PublikacjaIn this paper, novel methods for the evaluation of digital-filter stability are investigated. The methods are based on phase analysis of a complex function in the characteristic equation of a digital filter. It allows for evaluating stability when a characteristic equation is not based on a polynomial. The operation of these methods relies on sampling the unit circle on the complex plane and extracting the phase quadrant of a function...
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The effect of morphology and crystalline structure of Mo/MoO3 layers on photocatalytic degradation of water organic pollutants
PublikacjaMolybdenum oxide layers were formed by anodization of the Mo metallic foil in a water/ethylene glycol-based electrolyte containing fluoride ions. The as-prepared, amorphous samples were annealed in air at different temperatures in a range from 100 �C to 700 �C. The crystal phase and morphology of anodized and annealed MoO3 layers were investigated using X-ray diffraction, Raman spectroscopy, and scanning electron microscopy. The...
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Journal of Surface Investigation-X-Ray Synchrotron and Neutron Techniques
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The XRD diffraction patterns of reduced LSCNT prepared using two methods and two sintering temperatures
Dane BadawczeThe dataset includes XRD diffraction patterns of La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s produced using two methods, namely organic (citrate assisted) and Pechini sintered at 1000 or 1200oC under air atmosphere and reduced at 900 for 12 h in wet H2.
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Design advantages and analysis of a novel five-phase doubly-fed induction generator
PublikacjaPurpose – The purpose of this paper is to provide an analysis of the performance of a new five-phase doubly fed induction generator (DFIG). Design/methodology/approach – This paper presents the results of a research work related to fivephase DFIG framing, including the development of an analytical model, FEM analysis as well as the results of laboratory tests of the prototype. The proposed behavioral level analytical model is based...
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Structure, luminescent properties and FDTD simulation of TeO2-BaO-Bi2O3-Ag:Ln3+ glass-ceramics system
PublikacjaTeO2-BaO-Bi2O3-Ag glass systems (TBB) co-doped with terbium and europium ions have been successfully synthesized through conventional melt-quenching technique. Heat treatment procedure at 350 °C has been conducted in order to synthesize silver nanoparticles embedded in TBB glass matrix. Structural measurements involved XRD studies that revealed no crystallization of glass structure after heat treatment at elevated temperatures....
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15th Conference on Calorimetry and Thermal Analysis
WydarzeniaRegistration for the workshops with Sponsors, which will take place during the free time on Tuesday, September 10, 2024, from 2:30 PM, will be conducted by signing up on a list at the registration desk. We kindly inform you that posters should be prepared in size B1 (707 x 1000 mm). Templates:pptx, pdf Please submit your presentations...
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Imaging polarimeter with high-accuracy measuring principles in crystal optics
PublikacjaAn imaging polarimeter based on the principles of high-accuracy polarimetry well known in crystal optics is proposed. The application of scientific digital cameras for performance light measurements leads to precise data on polarizers quality, i.e., maps of extinction ratio and transmission axis. Processing of numerous images, acquired at various settings in the polarizer-sample-analyser system, allows to determine the two-dimensional...
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Tomasz Wąsowicz dr hab.
OsobyAbsolwent Technikum Elektrycznego w Słupsku (1997 rok) oraz Wydziału Matematyki, Fizyki i Informatyki Uniwersytetu Gdańskiego (2002 rok). W 2006 roku obronił dysertację doktorską z fizyki na WMFiI UG. Pracując już w PG, w 2018 roku uzyskał habilitację. W pierwszym okresie prace badawcze Tomasza Wąsowicza miały związek ze spektroskopią atomową wysokiej zdolności rozdzielczej i koncentrowały się na pomiarze i analizie prawdopodobieństw...
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Lanthanum investigations in ceramics annealed in a dry and wet atmosphere
Dane BadawczeCeramics based on Barium, Lanthanum, Gadolinium and Cobaltium were produced by standard solid state reaction from oxides and carbonate powders. After sintring, samples were annealed for 2 hours or 72 hours at 300 Celsius degree in a both: wet and dry atmosphere. Results of annealing on a chemical composition and valence state of lanthanum were observed...
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Jarosław Guziński prof. dr hab. inż.
OsobySTOPNIE NAUKOWE 2021 Tytuł profesora nauk inżynieryjno-technicznych. 2012 Stopień doktora habilitowanego nauk technicznych – Wydział Elektrotechniki i Automatyki PG. Rozprawa habilitacyjna „Układy napędowe z silnikami indukcyjnymi i filtrami wyjściowymi falowników. Zagadnienia wybrane”. Kolokwium i nadanie stopnia doktora habilitowanego 29 maja 2012 r. Monografia uzyskała nagrodę naukową Wydziału IV Nauk Technicznych Polskiej...
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Assessment of the cryoprotectant concentration inside a bulky organ for cryopreservation using X-ray computed tomography
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The X-ray photoelectron spectroscopy of surface composition of aged mixed copper manganese oxide catalysts
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Modeling of the L and M x-ray line structures for tungsten in high-temperature tokamak plasmas
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Modelling of the soft X-ray tungsten spectra expected to be registered by GEM detection system for WEST
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Fracture evolution in concrete compressive fatigue experiments based on X-ray micro-CT images
PublikacjaArtykuł omawia ewolucje pękania w betonie podczas cyklicznego ściskania betonu. Przestrzenną ewolucję pękania zobrazowano stosując mikro-tomograf rentgenowski. Zdjęcia wykonano dla różnych cykli zmęczeniowych. Wyniki porównano z testami monotonicznymi. Jakościowa ewolucja objętości pękania ze wzrostem zmęczeniowego zniszczenia pokazała silnie nieliniowy kształt.
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Crystal and molecular structure of bis(O,O'-diethyldithiophosphato-S,S')nickel(II): A redetermination
PublikacjaDoniesienie przedstawia ponownie wyznaczoną strukturę tytułowego, centrosymetrycznego kompleksu, [Ni{S2P(OC2H5)2}2]. Centralny rdzeń (S2P)2 jest płaski, co potwierdza wcześniejsze wyniki uzyskane przez McConnell'a i Kastalsky'ego, przy czym odchylenia standardowe są około siedmiokrotnie mniejsze oraz wyznaczono wszystkie pozycje atomów wodoru. W strukturze krystalicznej zaobserwowano róznież parę krótkich kontaktów HH (2.33 Å).
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PbGa2GeS6 crystal as a novel nonlinear optical material: Band structure aspects
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Crystal structure and physical properties of a novel ternary compound La15Mo Ge9
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Conformation-family Monte Carlo: A new method for crystal structure prediction
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Silver complexes stabilized by large silanethiolate ligands – crystal structures and luminescence properties
PublikacjaBulky silanethiolate and disiladithiolate ligands were applied to synthesize one mononuclear and three trinuclear silver complexes including two cyclic “microclusters” and a linear tri-nuclear silanethiolate complex. All obtained compounds are characterized by X-ray diffraction and FT-IR. NMR and emission spectroscopies were used where possible. The first trinuclear anionic silver thiolate is structurally characterized. The influence...
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Lower rim substituted p-tert-Butylcalix[4]arenes: Part XI. New ester derivatives of calix[4]arene, their ionophoric properties and x-ray structure studies
PublikacjaPrzedstawiono syntezę 6-ciu nowych estrowych pochodnych kaliks[4]arenuw konformacji stożkowej. Pierwsze badania kompleksowania jonów metali przeprowadzone w membranach elektrod jonoselektywnych (ISE) potwierdziły kompleksowanie jonów sodu w sposób selektywny. Zaprezentowano strukturę rentgenowską monokryształów związku 6.
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XPS (X-ray photoelectron spectroscopy) survey spectra of CPMD and CPMH
Dane BadawczeXPS (X-ray photoelectron spectroscopy) survey spectra of CPMD and CPMH. XPS spectra were obtained using Al Kɑ (hv=1486.6 eV) radiation with a Prevac system equipped with a Scienta SES 2002 electron energy analyzer operating at constant transmission energy (Ep=50 eV). Sample abbreviations (CPMD, CPMH) are in agreement with the markings used in the linked...
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Paenibacillus alvei MP1 as a Producer of the Proteinaceous Compound with Activity against Important Human Pathogens, Including Staphylococcus aureus and Listeria monocytogenes
PublikacjaAn emerging need for new classes of antibiotics is, on the one hand, evident as antimicrobial resistance continues to rise. On the other hand, the awareness of the pros and cons of chemically synthesized compounds’ extensive use leads to a search for new metabolites in already known reservoirs. Previous research showed that Paenibacillus strain (P. alvei MP1) recovered from a buckwheat honey sample presented a wide spectrum of...
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Crystal Facet Engineering of TiO2 from Theory to Application
PublikacjaRecently, the surface structure effect on photocatalytic activity has gathered increasing attention due to its reported influence on the charge carrier trapping and separation. Detailed control over the surface structure can be achieved by exposing the specific crystal facets. As a result, the photogenerated electrons and holes can be effectively separated between the different facets of semiconductor crystals. TiO2 is the most...
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Chemical composition of La-Sr-Ce-Ni-Ti ceramics material measured by XPS method
Dane BadawczeLa-Sr-Ce-Ni-Ti (LSCNT) based ceramics sample was manufactured by standard solid state reaction.Prepared powder was pressed into pilled and sintered in a furnace in air atmosphere for 10h. Annealing temperature was 1200 Celsius degree. To calculate chemical composition and determine valence states of the elements, X-Ray photoemission spectroscopy (XPS)...
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EFFECTS OF DOPING ON STRUCTURE AND PHASE TRANSITION OF HIGH TEMPERATURE PROTON CONDUCTOR LaNb1-xMxO4-σ (M=As, Sb, V, Ta AND X=0,05 TO 0,3)
PublikacjaIn this work synthesis of lanthanum orthoniobate has been done. Doping by arsenic, antimony, vanadium or tantalum in 5% to 30% have been introduced. The relationship between doping type and percentage and structural properties of the material have been investigated.
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Ray-tracing analysis of uniaxial birefringent optical components
PublikacjaW artykule przedstawiono elgorytm pozwalający na wyznaczenie kierunków i natężeń promieni propagowanych w układach optycznych zawierających elemennty wykonane z jednoosiowych materiałów dwójłomnych. Obliczenia w prezentowanym algorytmie są wykonywane na wektorach w globalnym układzie współprzędnych, eliminując konieczność częstych zmian ukłądu współprzędnych. Jako przykład obliczeniowy przedstawiono pełną analizę propagacji promieni...
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Novel 1,2,3-Triazole Derivatives as Mimics of Steroidal System—Synthesis, Crystal Structures Determination, Hirshfeld Surfaces Analysis and Molecular Docking
PublikacjaHerein, we present the synthesis and crystal structures determination of five 4-(1-phenyl-1H-1,2,3-triazol-4-yl)phenol derivatives containing halogen atoms, 6a–e, which may be used as an excellent mimic of steroids in the drug development process. Good quality crystals obtained for all of the synthesized compounds allowed the analysis of their molecular structures. Subsequently, the determined crystal structures were used to calculate...
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X-ray Photoelectron Spectroscopy studies of salivary gland stones
Dane BadawczeThis dataset contains the high-resolution XPS studies for 23 cross-sections of salivary gland stones. The sialoliths were cut to determine the differences in composition between various regions: core (labeled as R), interlayer (labeled as P) and sialolith surface (labeled as Z).
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Influence of Antimony Substitution on Spontaneous Strain and Thermodynamic Stability of Lanthanum Orthoniobate
PublikacjaThe analysis of the antimony substitution influence on temperature dependence of unit cell distortion has been done. The values of spontaneous strain and Landau order parameter for three different antimony contents varied had been calculated. The phase transition occurring for antimony substituted lanthanum orthoniobate was found to be second order. The high temperature solution calorimetry method has been used to investigate...
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Improvement of microstructure and mechanical properties of high dense sic ceramics manufactured by high-speed hot pressing
PublikacjaNon-oxide ceramics possess high physical-mechanical properties, corrosion and radiation resistance, which can be used as a protective materials for radioactive wastes disposal. The aim of the present study was the manufacturing of high density SiC ceramics with advanced physical and mechanical parameters. The high performance on the properties of produced ceramics was determined by the dense and monolithic structure. The densified...
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Atomic resolution crystal structure of HV-BBI protease inhibitor from amphibian skin in complex with bovine trypsin
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Third order nonlinear optical effects of ZnO–ZrO2–B2O3 glass ceramics embedded with ZnZrO3 perovskite crystal phases
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Structure and optical parameters of Eu doped tellurium oxide thin films prepared by reactive magnetron sputtering method
PublikacjaIn this work the structural properties and photoluminescence of tellurium dioxide thin films doped by europium were described. Thin films were deposited by magnetron sputtering method and simultaneously heated at 200 °C. Presence of Eu ions and their valence states was confirmed by X-ray photoemission spectroscopy measurements. The structure of the films as well as the influence of europium dopant on crystalline structure of the...
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An Analysis of Elliptical-Rectangular Patch Structure on Multilayer Elliptic Cylinders
PublikacjaThe resonance frequency problem of an ellipticalrectangular patch mounted on multilayered dielectric coated elliptic conducting cylinder, is investigated in this paper. A fullwave analysis and a moment-method calculation are employed. The analysis is carried out considering the expansion of the field as a series of Mathieu functions. An additional theorem for Mathieu functions is utilized to investigate the non-confocal ellipse...
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Electrochemical Characterization of Gelatine Derived Ceramics
PublikacjaNew materials obtained by pyrolysis of gelatine (G) and poly(1,2-dimethylsilazane) (PSN) (weight ratio: G/PSN 70/30) at temperatures 700 and 900 °C were characterized by SEM and Raman spectroscopy. The presence of ceramics influences on the cluster size of the materials. Electrochemical tests were performed by cyclic voltammetry and galvanostatic cyclic polarization. The capacity of G/PSN was 464 and 527 mAh/g for materials pyrolysed...
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Response to David Steigmann’s discussion of our paper
PublikacjaWe respond to David Steigmann's discussion of our paper "A general theory for anisotropic Kirchhoff-Love shells with in-plane bending of embedded fibers, Math. Mech. Solids, 28(5):1274-1317" (arXiv:2101.03122). His discussion allows us to clarify two misleading statements in our original paper, and confirm that its formulation is fully consistent with the formulation of Steigmann. We also demonstrate that some of our original statements...
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A general isogeometric finite element formulation for rotation‐free shells with in‐plane bending of embedded fibers
PublikacjaThis article presents a general, nonlinear isogeometric finite element formulation for rotation-free shells with embedded fibers that captures anisotropy in stretching, shearing, twisting, and bending - both in-plane and out-of-plane. These capabilities allow for the simulation of large sheets of heterogeneous and fibrous materials either with or without matrix, such as textiles, composites, and pantographic structures. The work...
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The topography of strontium–borate glasses and glass-ceramics containing nanocrystallites of Bi2VO5.5. measured with SEM method
Dane BadawczeThe topography of strontium–borate glasses and glass-ceramics containing nanocrystallites of Bi2VO5.5. was measured by SEM.
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Detection of Cystic Fibrosis Symptoms Based on X-Ray Images Using Machine Learning- Pilot Study
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FPGA-based LLRF control module for x-ray free electron laser and TESLA feedback system
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Inelastic X-Ray Scattering Studies of Phonon Dispersion in PbTe and (Pb,Cd)Te Solid Solution
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Diagnostics of the plasma parameters based on the K X-ray line positions for various 4d and 4f metals
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Quantitative estimation of volume changes of granular materials during silo flow using X-ray tomography.
PublikacjaW artykule przedstawiono wyniki badań doświadczalnych nad zmianami objętościowymi materiału granulowanego podczas przepływu silosowego. Badania wykonano przy zastosowaniu tomografii rentgenowskiej. Wyniki porównano z wynikami doświadczalnymi przy zastosowaniu cyfrowej obróbki zdjęć płynącego materiału.
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Karol Flisikowski dr inż.
OsobyKarol Flisikowski jest profesorem uczelni w Katedrze Statystyki i Ekonometrii, Wydziału Zarządzania i Ekonomii Politechniki Gdańskiej. Jest odpowiedzialny jest za prowadzenie zajęć ze statystyki opisowej i matematycznej (w języku polskim i angielskim), a także badań naukowych w zakresie statystyki społecznej. Był uczestnikiem wielu konferencji o zasięgu krajowym, jak i międzynarodowym, gdzie prezentował wyniki prowadzonych przez...
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Polish Conference on Crystal Growth 2022
WydarzeniaWelcome to the webpage of the Polish Conference on Crystal Growth 2022! The conference will be held in Gdańsk, Poland on June 19-24, 2022. The event is organized by the Polish Society for Crystal Growth (PTWK) in collaboration with Gdańsk University of Technology and the ENSEMBLE 3 Centre...
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On the origin of surfaces-dependent growth of benzoic acid crystal inferred through the droplet evaporation method
PublikacjaCrystal growth behavior of benzoic acid crystals on different surfaces was examined. The performed experiments documented the existence of very strong influence introduced by polar surfaces as glass, gelatin, and polyvinyl alcohol (PVA) on the growth of benzoic acid crystals. These surfaces impose strong orientation effect resulting in a dramatic reduction of number of faces seen with x-ray powder diffractions (XPRD). However,...