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Wyniki wyszukiwania dla: TOPOLOGICAL PHASES
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Various types of semiconductor photocatalysts modified by CdTe QDs and Pt NPs for toluene photooxidation in the gas phase under visible light
PublikacjaA novel synthesis process was used to prepare TiO2 microspheres, TiO2 P-25, SrTiO3 and KTaO3 decorated by CdTe QDs and/or Pt NPs. The effect of semiconductor matrix, presence of CdTe QDs and/or Pt NPs on the semiconductor surface as well as deposition technique of Pt NPs (photodeposition or radiolysis) on the photocatalytic activity were investigated. The as-prepared samples were characterized by X-ray powder diffractometry (XRD),...
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Fabrication and photoactivity of ionic liquid–TiO2 structures for efficient visible-light-induced photocatalytic decomposition of organic pollutants in aqueous phase
PublikacjaTo investigate the effect of the ionic liquid (IL) chain length on the surface properties and photoactivity of TiO2, a series of TiO2 microspheres have been synthesized via a solvothermal method assisted by 1-methyl-3-octadecylimidazolium chloride ([ODMIM][Cl]) and 1-methyl-3-tetradecylimidazolium chloride ([TDMIM][Cl]). All as-prepared samples were characterized by X-ray powder diffraction (XRD), X-ray photoelectron spectroscopy...
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Rapid and sensitive determination of acrylamide in potato crisps using reversed-phase direct immersion single drop microextraction-gas chromatography
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Comparison of Headspace Solid-phase Microextraction, Headspace Single-drop Microextraction and Hydrodistillation for Chemical Screening of Volatiles in Myrtus Communis L
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Results of acoustic emission tests of corrosion protection degree of ship steel tanks covered by means of protective coatings (Phase I)
PublikacjaThis paper presents methods and results of the 1st series of tests of acoustic emission (AE) signals, aimed at assessing degree of corrosion protection of a tank made of hull structural steel, protected by means of a protective coating combined from polyurethane layer and concrete filler. The tests were carried outin compliance with a method specially elaborated for application to the work in question. In the method were used requirements...
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The efficiency comparison of ramentaceone isolation from Drosera aliciae plants using normal and reversed phase preparative liquid chromatography technique
PublikacjaW pracy zaprezentowano optymalne warunki otrzymywania ramentaceonu z chloroformowego ekstraktu z rośliny D. muscipula. Opracowano i przedstawiono dwie procedury otrzymywania ramantaceonu z wykorzystaniem NP-PLC i RP-PLC. Dla produktu o określonej czystości, porównano maksymalny stopień przeładowania kolumny, efektywność procesu wyrażoną jako ilość substancji otrzymanej w jednostce czasu oraz produktywność kolumny, wyrażoną jako...
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Effective phospholipid removal from plasma samples by solid phase extraction with the use of copper (II) modified silica gel cartridges
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Analytical investigation of phase assemblages of alkali-activated materials in CaO-SiO2-Al2O3 systems: The management of reaction products and designing of precursors
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Solid phase extraction and sequential elution for pre-concentration of traces of Mn and Zn in analysis of honey by flame atomic absorption spectrometry
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Separation of Monovinyl and Divinyl Protochlorophyllides Using C30 Reverse Phase High Performance Liquid Chromatography Column: Analytical and Preparative Applications
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Determination of selenium by X-ray fluorescence spectrometry using dispersive solid-phase microextraction with multiwalled carbon nanotubes as solid sorbent
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Power grid frequency measurement in LabVIEW environment using the least mean squares method to signal phase approximation in the presence of noise
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Molecular biaxiality determines the helical structure – infrared measurements of the molecular order in the nematic twist-bend phase of difluoro terphenyl dimer
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Ionogel fibres of bis(trifluoromethanesulfonyl)imide anion-based ionic liquids for the headspace solid-phase microextraction of chlorinated organic pollutants
PublikacjaIonogels, a family of hybrid materials in which ionic liquids (ILs) are confined in a sol–gel network, are receiving much attention in a variety of scientific and technological fields. In this work, ionogels derived from three different ILs based on the anion bis(trifluoromethanesulfonyl)imide (TFSI), namely 1-butyl- 3-methylpyridinium bis(trifluoromethanesulfonyl)imide ([C4C1Py][TFSI]), 1-butyl-1-methylpyrrolidinium bis(trifluoromethanesulfonyl)imide...
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Sensitive simultaneous determination of 19 fluorobenzoic acids in saline waters by solid-phase extraction and liquid chromatography–tandem mass spectrometry
PublikacjaA solid-phase extraction (SPE) procedure using C18 stationary phase was optimized for the preconcentration of 19 fluorinated derivatives of benzoic acid (FBA): mono-, di-, tri-, and tetrafluorosubstituted in the ring, trifluoromethylbenzoic acid and 3,5-bistrifluoromethyl benzoic acid from undiluted salt-rich (>20%) reservoir waters. Quantitative (>90%) retention/elution of 16 out of 19 analyte compounds was achieved allowing a...
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Simultaneous Determination of Indolic Compounds in Plant Extracts by Solid-Phase Extraction and High-Performance Liquid Chromatography with UV and Fluorescence Detection
PublikacjaA high-performance liquid chromatographic method with UV and fluorescence detection (HPLC-DAD-FLD) was developed for simultaneous determination of indolic compounds in plant material. Indole-3-carbinol (I3C), indole-3-acetic acid (I3AA), indole-3-acetonitrile (I3ACN), and 3,3′-diindolylmethane (DIM) were used as representative compounds that cover a wide spectrum of indole structures occurring in nature. For concentration and purification...
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SiC-based phase-shift dual half bridge DC-DC converter as a key component of multilevel cascaded MV converters
PublikacjaThe paper describes SiC-based dual half bridge (DHB) DC-DC converter considered as a key component of high frequency isolated multilevel cascaded medium voltage converters. Two topologies of bi-directional DC-DC converters: the resonant half-bridge DC-DC converter and the phase-shift DHB converter are compared in the paper. Experimental results of SiC-based 50 kHz DHB DC-DC converter are presented in the paper.
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Experimental verification of the theoretical modelof heat transfer between a liquid layer formed by a two-phase impinging jet and a solid surface
PublikacjaW pracy przedstawiono eksperymentalną weryfikacje modelu teoretycznego wymiany ciepła pomiędzy warstwą wody a stałą powierzchnią. Warstwa cieczy powstała z uderzającej o powierzchnię dwufazowej strugi uderzającej
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Effect of Nitrogen Ion Implantation on the Cavitation Erosion Resistance and Cobalt-Based Solid Solution Phase Transformations of HIPed Stellite 6
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Effect of Nitrogen Ion Implantation on the Cavitation Erosion Resistance and Cobalt-Based Solid Solution Phase Transformations of HIPed Stellite 6
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Application of the MSPD Technique for the HPLC Analysis of Rutin in Sambucus nigra L.: The Linear Correlation of the Matrix Solid-Phase Dispersion Process
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Rapid Characterization of the Human Breast Milk Lipidome Using a Solid-Phase Microextraction and Liquid Chromatography-Mass Spectrometry-Based Approach.
PublikacjaHuman breast milk (HBM) is a biofluid consisting of various biomolecules such as proteins, lipids, carbohydrates, minerals and bioactive substances. Due to its unique and complex composition, HBM provides not only nutritional components required for the growth of the infant, but also additional protection against infections. Global insight into the composition of HBM is crucial to understanding the health benefits infants receive...
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Numerical analysis of the two‐phase steam‐air heat transfer flow induced in smooth and corrugated channel using the VOF model
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First-Phase Left Ventricular Ejection Fraction as an Early Sign of Left Ventricular Dysfunction in Patients with Stable Coronary Artery Disease
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Determination of Butyltin Species in Sea Water Samples Using Solid Phase Extraction Followed by Liquid Chromatography - Tandem Mass Spectrometry
PublikacjaReverse phase liquid chromatography (RP-HPLC)-electrospray ionization-tandem mass spectrometry (ESI-MS-MS) was evaluated for the analysis of TBT using solid phase extraction as sample preparation method. TBT was extracted from acidified water samples (spiked with tripropyltin as internal standard) using reversed phase polymeric Strata-X cartridges. Analytes were eluted from cartridges using acetonitrile-water mixture and the volume...
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Modulation of rat hepatic and kidney phase II enzymes by cabbage juices: comparison with the effects of indole-3-carbinol and phenethyl isothiocyanate
PublikacjaZbadano wpływ soków ze świeżej i kiszonej kapusty na ekspresję i aktywność takich enzymów II fazy jak transferazy S-glutationowe i oksydoreduktaza NQO1 w wątrobie i nerkach szczurów, którym podawano wspomniane soki doustnie. Uzyskane wyniki porównano z oznaczeniami uzyskanymi po doustnym podaniu wyizolowanych produktów degradacji glukozynolanów, indolo-3-karbinolu i izotiocyjanianu fenyloetylu. Wszystkie testowane czynniki powodowały...
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Computational analysis of substituent effects on proton affinity and gas-phase basicity of TEMPO derivatives and their hydrogen bonding interactions with water molecules
PublikacjaThe study investigates the molecular structure of 2,2,6,6-tetramethylpiperidine-1-oxyl (TEMPO) and its derivatives in the gas phase using B3LYP and M06-2X functional methods. Intermolecular interactions are analyzed using natural bond orbital (NBO) and atoms in molecules (AIM) techniques. NO2-substituted TEMPO displays high reactivity, less stability, and softer properties. The study reveals that the stability of TEMPO derivatives...
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Comparative analysis of three‐phase dual active bridge converter with different transformer topology and modern universal control for DC microgrids
PublikacjaThe presented work discusses issues related to the use of modern multiphase topologies of Dual Active Bridge (DAB)-type converters. Converters of this type are widely used in most DC microgrid applications. The introduction emphasizes a comparative analysis between single-phase and multi-phase DAB topologies within high-power DC microgrids, delving into their respective advantages, drawbacks, design procedures, and considerations...
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Discrepancies in determination of biogenic amines in beer samples by reversed phase and hydrophilic interaction liquid chromatography coupled with tandem mass spectrometry
PublikacjaBiogenic amines (BAs) are nitrogenous organic bases occurring mainly in fermented food and beverages as a result of free amino acids bacterial decarboxylation. The reversed phase liquid chromatography (RPLC) and hydrophilic interaction liquid chromatography (HILIC) based methods were compared in terms of usefulness for determination of BAs in beer samples. Analysis of BAs with the use of RPLC method were carried out after their...
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Effective Permeability of Multi Air Gap Ferrite Core 3-Phase Medium Frequency Transformer in Isolated DC-DC Converters
PublikacjaThe magnetizing inductance of the medium frequency transformer (MFT) impacts the performance of the isolated dc-dc power converters. The ferrite material is considered for high power transformers but it requires an assembly of type “I” cores resulting in a multi air gap structure of the magnetic core. The authors claim that the multiple air gaps are randomly distributed and that the average air gap length is unpredictable at the...
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First deep eutectic solvent-based (DES) stationary phase for gas chromatography and future perspectives for DES application in separation techniques
PublikacjaThe paper presents the first application of deep eutectic solvents (DES) as stationary phases for gas chromatography. DES obtained by mixing tetrabutylammonium chloride (TBAC) as a hydrogen bond acceptor (HBA) with heptadecanoic acid being a hydrogen bond donor (HBD) in a mole ratio of HBA:HBD equal to 1:2 was characterized by its ability to separate volatile organic compounds (VOCs). The Rohrschneider – McReynolds constants determined...
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Matrix solid-phase dispersion (MSPD) as simple and useful sample preparation technique for determination of polybrominated diphenyl ethers (PBDEs) in dust
PublikacjaIn the present study a novel analytical procedure for the determination of polybrominated diphenylethers in dust samples was developed.The main aim of the research was the selection of the optimum conditions of the matrix solid-phasedispersion before thefinal determination of polybrominated diphenyl ethers in dust samples. In order toassess the best usefulness of this technique, a favourable ratio of sample amount to the mass ofdispersing...
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Application of a novel deep eutectic solvent modified carbon nanotube for pipette-tip micro solid phase extraction of 6-mercaptopurine
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Belinostat in Patients With Relapsed or Refractory Peripheral T-Cell Lymphoma: Results of the Pivotal Phase II BELIEF (CLN-19) Study
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Ibrutinib as Treatment for Patients With Relapsed/Refractory Follicular Lymphoma: Results From the Open-Label, Multicenter, Phase II DAWN Study
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Efficacy and safety of idelalisib in patients with relapsed, rituximab- and alkylating agent-refractory follicular lymphoma: a subgroup analysis of a phase 2 study
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Ibrutinib versus temsirolimus in patients with relapsed or refractory mantle-cell lymphoma: an international, randomised, open-label, phase 3 study
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Characterization of diatomaceous earth coated with nitrated asphaltenes as superior adsorbent for removal of VOCs from gas phase in fixed bed column
PublikacjaAsphaltenes isolated from bitumen possess unusual adsorption characteristics that can be further enhanced by chemical modifications to promote interactions with VOCs’. Herein, nitrated asphaltenes are used as an active layer coated on a surface of a diatomaceous earth, in order to prepare an efficient adsorbent (AsfNitro). Breakthrough experiments with benzene, pyridine, and 1-nitropropane revealed significant increase in adsorption...
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Nickel phase deposition on V2CTx/V2AlC as catalyst precursors for a dry methane reforming: The effect of the deposition method on the morphology and catalytic activity
PublikacjaDry reforming of methane (DRM) is a promising alternative technology for the production of syngas with simultaneous utilization of two main greenhouse gases (CH4, CO2). However, DRM technology is still an industrially immature process due to the lack of stable and active catalyst. Therefore, the search for new catalytic materials is of great research interest. Recently, MAX and MXenes materials are increasingly being tested as...
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Endometrial nitric oxide production and nitric oxide synthases in the equine endometrium: Relationship with microvascular density during the estrus cycle
PublikacjaNitric oxide (NO) plays an important role in angiogenesis and in the regulation of the blood flow. This study was carried out to investigate (i) the effects of endogenous estrogens and progestins and exogenous progesterone (P(4)) (5 ng/ml or 1 microg/ml) or estradiol 17beta (E(2)beta) (50 pg/ml or 1 microg/ml) on in vitro endometrial NO synthesis; (ii) the presence of different isoforms of NO synthase;...
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Application of continuous wavelet transform in vibration based damage detection method for beams and plates
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Modelling of wave propagation in composite plates using the time domain spectral element method
PublikacjaW pracy przedstawiono wyniki obliczeń propagacji fali sprężystej w płycie kompozytowej modelowanej z wykorzystaniem czasowego sformułowania metody elementów spektralnych
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Optimal Placement of Phasor Measurement Unit in Power System using Meta-Heuristic Algorithms
PublikacjaThe phasor measurement units (PMUs) play an important and vital role in power system monitoring and controlling, since they provide the power system phasors stamped with a common real time reference through a global positioning system (GPS). Indeed, from economical point of view it is not possible to set PMUs in all system buses due to the high cost and the requirement of more complex communication...
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Natural convective heat transfer from isothermal horizontal, vertical and inclined plates - a review
PublikacjaW artykule przedstawiono przegląd otrzymanych przez różnych badaczy korelacji eksperymentalych, teoretycznych i numerycznych, opisujących wymianę ciepła od izotermicznych płyt o różnym kącie pochylenia. Przedstawiono model matematyczny zjawiska. Opisano stosowane metody badawcze i wskazano przyczyny rozbieżności pomiędzy przedstawionymi przez wielu autorów wynikami.
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The influence of applying supplementary web plates on structural joint moment resistance and rotational stiffness
PublikacjaContinual trend to simplify structural elements and find less time-consuming solutions on construction site as well as inevitable increase in labour costs determine for instance elimination of those technological steps that are difficult to automation. Welding additional reinforcements and web stiffeners is a great example of such a step. The method presented in EN 1993-1-8 [8] is a result of long-term studies focused on calculating...
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Effects of traumatic life events, cognitive biases and variation in dopaminergic genes on psychosis proneness
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Dynamics analysis of footbridge mode shapes the s8 expressway on the basis of the results of in situ tests
PublikacjaNon-destructive diagnostics for structure may use dynamic measurements realized during vibrations of a facility induced by dynamic environmental impact, enforced by the use of inductors or impulse impact. Dynamic tests and the analysis were undertaken for a footbridge situated over the expressway S8. The studies in situ allowed for dynamic characteristics to be determined: frequency, shape modes and damping for respective frequency...
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Modern era fortifications as public places = Fortyfikacje nowożytne jako miejskie przestrzenie publiczne
PublikacjaFortyfikacje nowożytne tworzyły systemy budowli ziemnych oraz szerokich fos. Ich powierzchnia przekraczała często powierzchnię otoczonego nimi miasta. Utrata znaczenia obronnego oraz tendencje do wzrostu terytorialnego miast spowodowały konieczność zmiany funkcji fortyfikacji. W XIX i XX wieku były one rozbierane, a ich tereny zabudowywane lub przekształcane w przestrzeń publiczną. Zagospodarowanie i konserwacja tych obiektów...
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Mixed-use buildings as the basic unit that shapes the housing environment of smart cities of the future
PublikacjaThe contemporary approach to creating the residential function is confronted with the trend of increasing the volume of buildings and expectations regarding the future urban environment focused on sustainable development. This paper presents an overview of the residential structure in the context of defined thematic scopes. Namely, it is a systemic approach to the problem of designing mixed-use buildings which create a modern residential...
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Does the Use of Cell Phones and Headphones at the Signalised Pedestrian Crossings Increase the Risk of Accident?
PublikacjaReduction of the number of fatalities among pedestrians remains a topical issue in Poland. For many years, this percentage has remained at around 30% of all those who were killed on the road. At the same time, there is an increase in the use of electronic devices by pedestrians and cyclists that may affect their perception when crossing the road. This can lead to traffic accidents. In order to investigate the problem, field studies...