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Wyniki wyszukiwania dla: transiton metals
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Polymeric metal‐containing ionic liquid sorbent coating for the determination of amines using headspace solid‐phase microextraction
PublikacjaThis study describes the design, synthesis, and application of polymeric ionic liquid sorbent coatings featuring nickel metal centers for the determination of volatile and semivolatile amines from water samples using headspace solidphase microextraction. The examined polymeric ionic liquid sorbent coatings were composed of two ionic liquid monomers (tetra(3-vinylimidazolium)nickel bis[(trifluoromethyl)sulfonyl]imide [Ni2+(VIM)4]...
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Metal (Mo, W, Ti) Carbide Catalysts: Synthesis and Application as Alternative Catalysts for Dry Reforming of Hydrocarbons—A Review
PublikacjaDry reforming of hydrocarbons (DRH) is a pro-environmental method for syngas production. It owes its pro-environmental character to the use of carbon dioxide, which is one of the main greenhouse gases. Currently used nickel catalysts on oxide supports suffer from rapid deactivation due to sintering of active metal particles or the deposition of carbon deposits blocking the flow of gases through the reaction tube. In this view,...
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Silicon polypodands: powerful metal cation complexing agents and solid–liquid phase-transfer catalysts of new generation
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Study on the effect of the metal–support (Fe-MgO and Pt-MgO) interaction in alcohol-CVD synthesis of carbon nanotubes
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Estimation, optimization and analysis based investigation of the energy consumption in machinability of ceramic-based metal matrix composite materials
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Determination of time dependence of coated metal electrical and electrochemical parameters during exposure using principal component analysis
PublikacjaThe use of the principal component analysis (PCA) permits the complex and quantitative analysis of the time dependence of electrical and electrochemical parameters of coated metal obtained by fitting impedance data. So far, changes in electrical and electrochemical parameters during exposure were analyzed independently. In this way, some of the information contained in the relationship between changes in parameters over time are...
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Noble metal modified TiO2 microspheres: Surface properties and photocatalytic activity under UV-vis and visible light
PublikacjaComposite photocatalysts that consist of TiO2and noble metal nanostructures have been considered tobe the promising and pivotal material for accessible enhancement of the efficiency in the photocatalyticprocess carried out in the aqueous and gas phases. In this work we fabricated porous TiO2microspheresthrough a hydrothermal process followed by photochemical reduction of noble metal nanoparticles atthe TiO2surface. The morphology...
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A pilot study to assess an in-process inspection method for small diameter holes produced by Direct Metal Laser Sintering
PublikacjaPurpose The purpose of this research is to evaluate the geometric quality of small diameter holes in parts printed by DMLS technology. An in-process optical inspection method is proposed and assessed during a pilot study. The influence of the theoretical hole diameter assumed in a CAD system and the sample thickness (hole length) on the hole clearance was analysed. Design/methodology/approach The samples made of two different...
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Determination of metal content in sewage sludge and sewage sludge ash to find opportunities to use them in the construction industry
PublikacjaSewage sludge management is becoming an increasing problem in developed and developing countries. Due to their physicochemical properties (mainly high content of heavy metals) a safe method of utilization is sought. Considering environmental protection, energy recycling, reduction in use of the raw materials and the possibility of immobilization hazardous substances, the use of ashes in building materials becomes a very good way...
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Metal ion directed template synthesis using 2-acetyl-1,3-indandione and ethylenediamine: steric and electronic restrictions
PublikacjaA template synthesis using 2-acetyl-1,3-indandione and ethylenediamine results in formation of octahedral Ni complex, whose crystal structure has been resolved using single crystal X-ray diffraction. The structure indicates that only exocyclic enolic oxygen atom of the triketone takes part in the condensation with ethylenediamine.
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The effects of urban vehicle traffic on heavy metal contamination in road sweeping waste and bottom sediments of retention tanks
PublikacjaDiffuse pollution formed during a surface runoff on paved surfaces is a source of heavy metals (HMs) of various origin. This research study indicates the connection between bottom sediments of retention tanks located on urban streams and road sweeping wastes (RSW) that migrate during surface runoff to the stormwater drainage systems with discharge to the retention tanks. Moreover, we test the primary sources of HMs in RSW by analysing...
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Thermal utilization of meat and bone meals. Performance analysis in terms of drying process, pyrolysis and kinetics of volatiles combustion
PublikacjaA development of technology of thermal utilization requires a thorough knowledge of the physicochemical properties, as well as kinetics of combustion of volatiles and char. Due to waste management regulations the meat and bone meal (MBM) is regarded as biofuel constituting one of the alternatives to fossil fuels in the energy market. MBM is a heterogeneous material that may consist of several different fractions. The extensive...
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Fast-SEC coupled to ICP-MS for selected metal determination and its stability over time in polish wine
PublikacjaMetal ions contribute to the wine browning (as reaction catalysts), turbidity (in complexes), and astringency (due to inter- action with tannins). Being aware that bioavailability and metabolism of metal ions in the human body are strictly related with their concentration and the form they occur it is important to monitor not only the total content of metals but also their speciation. Thus, we can obtain more information about...
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Zr‐Based Metal‐Organic Framework UiO‐66/Ultem® 1000 Membranes for Effective CO2/H2 Separation
PublikacjaMixed-matrix membranes (MMMs) using UiO-66 nanofillers as dispersing inorganic phase and polyetherimide (PEI) as continuous polymeric matrix were synthesized. Different UiO-66 loadings of 10, 20, and 30 wt % were applied. The morphology and UiO-66 dispersion over the prepared MMMs were examined. Gas separation measurements were performed for H2/CO2 gas mixture to evaluate the influence of UiO-66 on the separation yield of resulting...
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The effect of metal cluster deposition route on structure and photocatalytic activity of mono- and bimetallic nanoparticles supported on TiO2 by radiolytic method
PublikacjaTiO2 (P25) was modified with small and relatively monodisperse mono- and bimetallic clusters (Ag, Pd, Pt, Ag/Pd, Ag/Pt and Pd/Pt) induced by radiolysis to improve its photocatalytic activity. The as-prepared samples were characterized by X-ray fluorescence spectrometry (XRF), photoluminescence spectrometry (PL), diffuse reflectance spectroscopy (DRS), X-ray powder diffractometry (XRD), scanning transition electron microscopy (STEM)...
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Determination of electrode impedance by means of exponential chirp signal
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Anisakids of seals found on the southern coast of Baltic Sea
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Sleep Apnea Detection by Means of Analyzing Electrocardiographic Signal
PublikacjaObstructive sleep apnea (OSA) is a condition of cyclic, periodic ob-struction (stenosis) of the upper respiratory tract. OSA could be associated with serious cardiovascular problems, such as hypertension, arrhythmias, hearth failure or peripheral vascular disease. Understanding the way of connection between OSA and cardiovascular diseases is important to choose proper treatment strategy. In this paper, we present a method for integrated...
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ECG-based prediction of ventricular fibrillation by means of the PCA
PublikacjaA Sudden Cardiac Death (SCD) is a death resulting from cardiac failure with no significant symptoms earlier than one hour before occurrence. It is the cause of for approximately 400000 deaths per year in United States and millions of deaths worldwide. The proposed system, including two-stage algorithm and wearable diagnostic device allows for SCD risk estimation and continuous monitoring of high risk patients. A single channel...
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Sea bottom structure investigation by means of acoustic methods
PublikacjaThe main aim of the paper is the result of experimental investigations of the seabed in the Gulf of Gdańsk arried out using parametric echosounder as a main measuring tool. Examination of the surface's upper layer of the seabed, especially is acoustic properties, reflecting most often transsmision and reflection properties of the incident elastic wave, could be a valuable material for determination of the stratification, and the...
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Exploiting audio-visual correlation by means of gaze tracking
PublikacjaThis paper presents a novel means for increasing audio-visual correlation analysis reliability. This is done based on gaze tracking technology engineered at the Multimedia Systems Department of the Gdansk University of Technology, Poland. In the paper, the past history and current research in the area of audio-visual perception analysis are shortly reviewed. Then the methodology employing gaze tracking is presented along with the...
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The Examination of the Upper Layers of the Seabed by the Means of the Acoustic Methods
PublikacjaPropagation of acoustic waves in the sea, in particular in shallow sea, depends on several factors. The basic of them are source power and frequency of acoustic waves, spatial distribution inhomogeneous medium in which acoustic wave propagates, and distributions of speed of sound and density of seawater. The coastal conditions, which limit water medium from above (free surface of the sea) and from bottom (the seabed), are no less...
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Explanation of Reduction of Pressure Forces in Turbine Chamber Seals
PublikacjaThe paper describes a chamber seal reducing the aerodynamic forces created in shroud seals. Asymmetrical pressure distribution (due to rotor-stator eccentricity) in the blade tip clearance leads to the creation of pressure forces acting on the blade shroud. By increasing the volume above the shroud, the pressure distribution becomes more uniform on the whole shroud circumference and the effect of rotor eccentricity is reduced....
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A Study of the Roll Motion by Means of a Free Decay Test
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The Assessment of Maternal and Fetal Intima-Media Thickness in Perinatology
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K-means clustering for SAT-AIS data analysis
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Transport undertaking as means of activation of women in rural areas
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Nanostructure characterization of (SmS)1.19TaS2 by means of STM/STS
PublikacjaW publikacji przedstawiono badania za pomocą techniki STM i STS powierzchni kryształów warstwowego związki typu misfit(SmS)1.19TaS2. Badania pozwalają sądzić, że powierzchniową warstwą jest warstwa Sm-S.
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Motor bearing diagnostics performed by means of laser vibrometer
PublikacjaDamage of bearings is the most common cause of failures in squirrel-cage induction motors. That is why the issues connected with diagnostics of bearings are so important. The equipment employed for bearing diagnostics usually makes use of vibrations as the criterion for technical condition of the bearings. This paper presents exemplary results of the research conducted on bearings with artificially introduced damage. A scanning...
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NEW DESIGNS OF MAGNETIC FLUID SEALS FOR RECIPROCATING MOTION
PublikacjaT he operating conditions of magnetic fluid seals during reciprocating motion are so different from those observed in rotating motion that the use of their conventional structures for reciprocating motion seals yields no good results. The analysis of the sealing mechanism of magnetic fluid seals in reciprocating motion shows that the operation of these seals is affected by the carry-over phenomenon and magnetic fluid...
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The methylome and transcriptome of fetal skin: implications for scarless healing
PublikacjaAim: Fetal skin is known to heal without scarring. In mice, the phenomenon is observed until the 16–17 day of gestation – the day of transition from scarless to normal healing. The study aims to identify key methylome and transcriptome changes following the transition. Materials & methods: Methylome and transcriptome profiles were analyzed in murine dorsal skin using microarray approach. Results & conclusion: The genes associated...
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Digital Government as Implementation Means for Sustainable Development Goals
PublikacjaOne of the challenges for implementing Sustainable Development Goals (SDGs) is the measurement of indicators that represent progress towards such goals. Measuring such progress enables data-driven decision-making and management of SDG-relevant projects and strategies. The premise of this research is that measuring such indicators depends on measuring so-called means of implementation, i.e. activities that directly contribute to...
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Influence of lubricating oil improvers on performance of crankshaft seals
PublikacjaThis paper presents an original method for checking influence of lubricating oil improvers on performance of crankshaft seals of combustion piston engine. Crankshaft seals were tested with the use of a modified friction node of T-02 four- ball apparatus in laboratory conditions. The tests were conducted according to a worked-out algorithm. Their results confirmed usefulness of the method for determining „harmful” performance...
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Assessment of Supercapacitor’s Quality by Means of Low Frequency Noise
PublikacjaLow frequency noise is a well-known tool for quality and reliability assessment of electronic devices. This phenomenon is observed in different electrochemical devices as well (e.g., smart windows, electrochemical corrosion processes). Thus, we can assume that the same tool can be used to asses quality of supercapacitors. Their quality is usually determined only by capacitance and/or equivalent series resistance (ESR), or impedance....
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Explanation of Reduction of Pressure Forces in Turbine Chamber Seals
PublikacjaThe paper describes a chamber seal reducing the aerodynamic forces created in shroud seals. Asymmetrical pressure distribution (due to rotor-stator eccentricity) in the blade tip clearance leads to the creation of pressure forces acting on the blade shroud. By increasing the volume above the shroud, the pressure distribution becomes more uniform on the whole shroud circumference and the effect of rotor eccentricity is reduced....
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Diagnostics of induction motors by means of current supplying measurements
PublikacjaSkładowe prądu zasilającego silnik, które związane są z uszkodzeniami łożysk są małe w porównaniu z dominującą składową sieciową. Zaproponowano układ pomiarowy do ich pomiaru i przedstawiono wyniki badań diagnostycznych na obiektach rzeczywistych.
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Determination of electrode impedance by means of exponential chirp signal.
PublikacjaPrzedstawiona została nowa metoda pomiaru impedancji elektrodowej. Jako pobudzenie zastosowany został niestacjonarny sygnał napięciowy, którego częstotliwość jest ekspotencjalną funkcją czasu. Zastosowanie zmodyfikowanej któtko-czasowej transformaty Fouriera (STFT) w analizie napięciowego pobudzenia i odpowiedzi prądowej pozwala na otrzymanie widma impedancyjnego.
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Diagnostics of cvd process by means of optical emission spectroscopy.
PublikacjaZastosowano optyczną spektroskopię emisyjną do badania w trybie in-situ dysocjacji cząsteczek oraz wzbudzenia i jonizacji atomów wodoru podczas procesu syntezy cienkich warstw diamentowych metodą chemicznego osadzania z par gazowych wspomaganego plazmą mikrofalową (mPACVD). Zbudowano tor światłodowy, umożliwiający sprzężenie komory CVD z systemem spektroskopowym i wykonywanie pomiarów bezinwazyjnych. Wykonano pomiary spektralne...
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Detal wielorodzinnej architektury mieszkaniowej Gdańska okresu miedzywojennego
PublikacjaDetal architektury mieszkaniowej w Gdańsku okresu 20-lecia międzywojennego występuje sporadycznie i nie przedstawia specjalnej wartości estetycznej. Brakuje też publikacji na ten temat.
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Search for identity of Pomeranian house by means of educational activities
PublikacjaArchitecture is a universal phenomenon and is a culture-creating field closely related to other fields of art. Hence, experiencing and feeling identity are also conditioned by the proper formation of architectural objects, which are carriers specific values which co-decide about the possibility of this experience occurring in connection with a specific place and the fulfilment of a specific need in it. In the era of ubiquitous...
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Influence of the structure of vanadate-phosphate glasses containing alkali ions on their polaronic properties
PublikacjaBadano wpływ struktury szkieł wanadanowo-fosforanowych zawierających jony metali alkalicznych na ich właściwości polaronowe metodą NMR.
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Study of Phase Transitions Occurring in a Catalytic System of ncFe-NH3/H2 with Chemical Potential Programmed Reaction (CPPR) Method Coupled with In Situ XRD
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Usuwanie i podział fazowy metali ciężkich w ekosystemie oczyszczalni hydrofitowej zasilanej odciekami ze składowiska odpadów komunalnych
PublikacjaWyniki badań stężeń metali w odciekach i osadach dennych pochodzących z hydrofitowej oczyszczalni odcieków ze składowiska odpadów komunalnych w Örebro w Szwecji. Analizowany obiekt jest systemem o przepływie powierzchniowym, złożonym z 10 stawów zasiedlonych roślinnością hydrofitową. Zastosowany system zapewnia wysokie efektywności usuwania zanieczyszczeń z odcieków, co umożliwia ich odprowadzanie do odbiornika - cieku wodnego...
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VIBRATION SURVEILLANCE DURING MILLING OF FLEXIBLE DETAILS WITH A USE OF THE ACTIVE OPTIMAL CONTROL
PublikacjaThe main goal of modern machining operations is to achieve increasingly better performance. High Speed Machining and/or High Performance Cutting, despite a lot of advantages, have also some drawbacks, for example, a possibility of losing stability and development of self-excited chatter vibration. This paper presents an approach of vibration surveillance during high speed milling with a use of active optimal control. Non-stationary...
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A mechatronic approach towards vibration surveillance during slender milling of flexible details
PublikacjaPraca dotyczy zastosowania elementów projektowania mechatronicznego do nadzorowania drgań podczas frezowania przedmiotów podatnych z wykorzystaniem aktywnego sterowania optymalnego. Opisano dynamikę układu sterowanego i zdefiniowano optymalny sygnał sterujący we współrzędnych hybrydowych. Wyodrębniono trzy podukłady: strukturalny, modalny i łączący. Uruchomiono program symulacji komputerowej, który umożliwił uzyskanie wyników potwierdzających...
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Mortality in people with mental disorders in Poland: A nationwide, register-based cohort study
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Mental state and quality of life after 10 session whole-body cryotherapy
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Coping Styles, Mental Health, and the COVID-19 Quarantine: A Nationwide Survey in Poland
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The SARS-CoV-2 and mental health: From biological mechanisms to social consequences
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Vibration surveillance for efficient milling of flexible details fixed in adjustable stiffness holder
PublikacjaThe paper presents the results of research related to the possibility of using an intelligent workpiece holder with adjustable stiffness, during end milling process. Machining a one side supported flexible workpiece will be performed with constant spindle speed and feed speed. In order to avoid hazardous vibration, stiffness of the especially designed spring (mounted in a workpiece holder) will be modified off-line. In order to...