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Wyniki wyszukiwania dla: DI-SPME
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Evolution of the nanostructure of Pt and Pt–Co polymer electrolyte membrane fuel cell electrocatalysts at successive degradation stages probed by X-ray photoemission
PublikacjaWe present a set of XPS (X-ray photoemission spectroscopy) measurements and detailed data-analysis of electrodes for polymer electrolyte membrane fuel cell (PEMFC) based on carbon supported catalysts (Pt and Pt–Co) subjected to a step-like potential cycling (accelerated degradation test). The results of the measurements complete and corroborate parallel TEM (transmission electron microscopy), XRD (X-ray diffraction) and XAS (X-ray...
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Structural change of carbon supported Pt nanocatalyst subjected to a step-like potential cycling in PEM FC
PublikacjaIn this paper we present detailed X-ray absorption fine structure (XAFS), X-ray diffraction (XRD) and transmission electron microscopy (TEM) investigations of the changes in the local geometric and electronic structure of Pt nanoparticles used as a cathode catalyst in proton exchange membrane fuel cell (PEMFC), working under controlled potential cycling conditions.
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Local structural and chemical ordering of nanosized Pt(3±δ)Co probed by multiple-scattering x-ray absorption spectroscopy
PublikacjaThis work reports a detailed investigation of the local structure and chemical disorder of a Pt(3±δ)Co thin film and Pt(3±δ)Co nanoparticles. We have used a combination of techniques including x-ray absorption spectroscopy (XAS), x-ray diffraction (XRD), and high-resolution transmission electron microscopy (TEM). The important effect of chemical ordering on pair and three-atom configurations has been studied using computer simulations...
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Kinetic characterization of hydrogen sulfide inhibition of suspended anammox biomass from a membrane bioreactor
PublikacjaThe inhibition effects of hydrogen sulfide (H2S) on anammox-enriched biomass from a laboratory membrane reactor were analyzed in a series of batch respirometric experiments. The determined half maximal inhibitory concentration (IC50) was 4.67 mg H2S-S L−1 at the constant pH = 7.0 and the total sulfide concentration varying between 1 and 15 mg TS-S L−1. In another test, the IC50 was found to be 4.25 mg H2S-S L−1 under a constant...
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An adaptive-noise Augmented Kalman Filter approach for input-state estimation in structural dynamics
PublikacjaThe establishment of a Digital Twin of an operating engineered system can increase the potency of Structural Health Monitoring (SHM) tools, which are then bestowed with enhanced predictive capabilities. This is particularly relevant for wind energy infrastructures, where the definition of remaining useful life is a main driver for assessing the efficacy of these systems. In order to ensure a proper representation of the physical...
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Zielona Chemia.
PublikacjaPrzedstawiono podstawy Zielonej Chemii -nowego podejścia do zagadnień syntezy, przeróbki i wykorzystania związków chemicznych, związanego ze zmniejszeniem zagrożenia dla zdrowia i środowiska. Zielona Chemia dotyczy nie tylko syntezy, przeróbki i wykorzystania związków chemicznych ale również metod analitycznych które pomagają w prowadzeniu procesów chemicznych i ocenie ich wpływu na środowisko. Zastosowanie odpowiednich technik...
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A review of theoretical and practical aspects of solid-phase microextraction in food analysis.
PublikacjaSPME (mikroekstrakcja do fazy stacjonarnej) to szybka, nowoczesna technika przygotowania próbki do analizy. W niniejszej pracy dokonano przeglądu zastosowania techniki SPME do badania zanieczyszczeń żywności i analizy jej naturalnych składników. Praca zawiera również krótki teoretyczny opis zasad działania techniki SPME.
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Interactions of positrons with atoms and molecules
PublikacjaThe positron is the antiparticle of the electron. It has the same mass as the electron, but opposite charge. The understanding of the interactions of positrons with normal matter, like atoms and molecules, is of interest in various scientific fields, like nuclear medicine, plasma physics and astronomy. In this talk we will give a short introduction to some theoretical methods to describe the interactions of positrons with atoms...
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Numerical Study of the Impinging Jets Formed by an Injector with Different Nozzle Diameters
PublikacjaThe collision of two or more liquid jets may provide considerable atomisation and efficient mixing of injected substances at the same time. This phenomenon is used, among others, in rocket engines, where the fuel and oxidiser are introduced separately and almost immediately mixed through self-impingement. Depending on the injection and operating conditions, diverse configurations of impinging jets are used, such as doublets,...
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The logistics streamlining of the material flow at the production company
PublikacjaThe main practical problem in the Logistics Department at the company is overstaffing in the unit responsible for the flow of materials. Carried out by the authors of the article, some detailed research on the process analysis in the discussed company indicates that the main cause of such a situation is related to an increase in the amount of transported material and a lack of redesigning the material flow in...
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Porous material-based sorbent coatings in Solid-phase microextraction technique: Recent trends and future perspectives
PublikacjaThe use of porous materials as sorbents in sample preparation techniques has gained recent scientific attention in the context of developing novel fibers for the Solid-phase microextraction (SPME) technique. SPME requires the appropriate selection of a robust sorbent for successful utilization under variable conditions. A deeper understanding of the nature of newly developed porous SPME coatings and the impact of their structures...
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Nanosorbents as Materials for Extraction Processes of Environmental Contaminants and Others
PublikacjaThe aim of this work focuses on the application of nanomaterials (NMs) in different sorp- tive extraction techniques for the analysis of organic contaminants from environmental samples of distinct matrix compositions. Without any doubt, the integration of specific NMs such as carbona- ceous nanomaterials, magnetic nanoparticles (MNPs), metal–organic frameworks (MOFs), silica na- noparticles, and ion-imprinted NPs with so lid-phase...
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Genetic and Epigenetic Aspects of Atopic Dermatitis
PublikacjaAtopic dermatitis is a heterogeneous disease, in which the pathogenesis is associated with mutations in genes encoding epidermal structural proteins, barrier enzymes, and their inhibitors; the role of genes regulating innate and adaptive immune responses and environmental factors inducing the disease is also noted. Recent studies point to the key role of epigenetic changes in the development of the disease. Epigenetic modifications...
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Recycling of Polyurethanes Containing Flame-Retardants and Polymer Waste Transformed into Flame-Retarded Polyurethanes
PublikacjaThe growing number of polyurethanes (PUs) produced every year has developed methods for their mechanical and chemical recycling which yield valuable products like substitutes for commercial polyols or flame-retardants. PUs can be produced in different shapes and forms (i.e., elastomers, flexible or rigid foams, coatings, etc.) using several different components (i.e., di- or polyisocyanates, ester- or ether-based polyols, low-molecular...
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A headspace solid-phase microextraction method development and itsapplication in the determination of volatiles in honeys by gas chromatography
PublikacjaThe first part of the paper presents the detailed optimisation of all steps of the determination procedureof volatiles from Polish honeys by headspace solid-phase microextraction (HS-SPME) as the sample preparationmethod and gas chromatography/mass spectrometry (GC-MS) as the method of final determination.The methodology of semi-quantative analysis allowed the isolation and identification of volatile fractioncompounds from popular...
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Ionic liquids in the microextraction techniques: the influence of ILs structure and properties
PublikacjaIonic liquids (ILs) are composed entirely of ions thus they possess unique properties, including negligible volatility, a liquid state in a broad range of temperatures and ability to change them depending on the chosen type of anion and cation, which make ILs unique and useful for many applications in sample preparation techniques. A deeper understanding of the nature of ILs and the impact of their structure on their parameters...
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Nowe rozwiązania metodyczne i techniczne w zakresie techniki mikroekstrakcji do fazy stracjonarnej
PublikacjaSample preparation has been recognized as a critical step of the analytical process, being even considered as the bottleneck of the overall process. Enrichment of target compounds, transfer of the analytes into a solvent compatible with the analytical instrumentation, minimization of potential interferences, and efficient sample clean-up, are among the main aims of sample preparation techniques. In this regard, liquid-liquid extraction...
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Optical readout of superheated emulsions
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Histological Features of Neovaginal Epithelium after Vaginoplasty in Mayer-Rokitansky-Küster-Hauser Syndrome
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Stereochemical analysis of β-keto sulfoxides by circular dichroism
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Chiral [Mn II Mn III 3 M′] (M′=Na I , Ca II , Mn II ) and [Mn II Mn III 6 Na I 2 ] Clusters Built from an Enantiomerically Pure Schiff Base: Synthetic, Chiroptical, and Magnetic Properties
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Rare extragenital endometriosis: pathogenesis and therapy
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Menopause: a trigger for simultaneous development of ulcerative colitis in sigmoid neovagina and residual colorectum?
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Syntheses, structures, and chiroptical and magnetic properties of chiral clusters built from Schiff bases: a novel [MnIIMnIII6NaI2] core
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IMPACT OF DIRECT CURRENT ON NITRIFYING BIOMASS
PublikacjaEffects of short term exposure of nitrifying biomass to direct current were studied. DC was applied to mixed liquor from municipal BNR plant using graphite electrodes in no substrate limiting conditions. Both, ammonia oxidizing bacteria (AOB) and nitrite oxidizing bacteria (NOB) populations were affected by the current, however in opposite ways. The AOB population activity was inhibited by applied voltage. Activity decrease was...
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An annotated timeline of sensitivity analysis
PublikacjaThe last half a century has seen spectacular progresses in computing and modelling in a variety of fields, applications, and methodologies. Over the same period, a cross-disciplinary field known as sensitivity analysis has been making its first steps, evolving from the design of experiments for laboratory or field studies, also called ‘in-vivo’, to the so-called experiments ‘in-silico’. Some disciplines were quick to realize the...
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Effective configuration of a double triad planar parallel manipulator for precise positioning of heavy details during their assembling process
PublikacjaIn the paper, dynamics analysis of a parallel manipulator is presented. It is an atypical manipulator, devoted to help in assembling of heavy industrial constructions. Few atypical properties are required: small workspace; slow velocities; high loads. Initially, a short discussion about definition of the parallel manipulators is presented, as well as the sketch of the proposed structure. In parallel, some definitions, assumptions...
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Research project I (February 2024)
Kursy OnlineThis is the course for English-speaking students of Research project I. Access code: KSiSR2024 If you have some problem with access to the course please sent me e-mail to: slagaj@eti.pg.edu.pl (give me the name and your id number).
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Application of IR UWB Spectrum Shaping to IEEE 802.15.4a Standard
PublikacjaCoexistence of existing narrowband systems and new ultra wideband devices in the same frequency range requires using some interference mitigation techniques, for example based on spectrum shaping. This paper presents efficiency of impulse radio spectrum shaping methods, applied to IEEE 802.15.4a UWB alternate physical layer signals. Basic parameters of 802.15.4a signal structure and outline of proposed spectrum shaping methods...
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Impact of Spatial Noise Correlation on Bearing Accuracy in DIFAR Systems
PublikacjaDIFAR type underwater passive systems are one of the more commonly used tools for detecting submarines. At the design stage, which usually uses computer simulations, it is necessary to generate acoustic noise of the sea. It has been shown that correlating noise significantly reduces these errors compared to the assumption that noise is uncorrelated. In addition, bearing errors have been shown to be the same in systems with a commonly...
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Rengel Cane Sia Doctoral Candidate
OsobyI'm Rengel, born and raised in the Philippines. As an undergraduate I did kinetic modeling on Copper-catalyzed atom transfer radical addition (ATRA). Then I was inspired to do both theoretical and experimental studies, which led me to propose my master's thesis on Synthesis, Computational, Electrochemical, and Photoconductivity Studies on Naphthalene and its derivatives. This led to a master's degree in Chemistry in the Mindanao...
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Wpływ równości nawierzchni i dynamicznego oddziaływania pojazdów ciężkich na trwałość zmęczeniową nawierzchni podatnych
PublikacjaPodczas ruchu pojazdu obserwuje się odchylenia nacisków osi pojazdów od nacisku statycznego, co jest spowodowane nierównościami nawierzchni. Dynamiczne obciążenia pojazdów w większym stopniu wytężają konstrukcję nawierzchni drogowej. Rozkład obciążeń dynamicznych ma kształt rozkładu normalnego i jest opisywany poprzez obciążenie statyczne oraz wskaźniki dynamiczne DI lub DLC. Wraz z pogorszeniem równości i zwiększeniem prędkości...
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The demand for skills and the labor cost in partner countries: evidence from the enlarged EU
PublikacjaWe analyse the consequences of trade integration in Europe (1995-2005) detecting how thelabor costs in partner countries affects the demand for domestic high- and low-skilled labor inthe EU-15 (Old) and five New member states. In general, independently on the skill level, the resultshint at complementarity between domestic and foreign labor. However, the demand for thehigh skilled in New EU members' low skill intensive sectors...
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Application of Ionic Liquids in Amperometric Gas Sensors
PublikacjaThis article presents an analysis of available literature data on metrological parameters of the amperometric gas sensors containing ionic liquids as an electrolyte. Four mechanism types of signal generation in amperometric sensors with ionic liquid are described. Moreover, this article describes the influence of selected physico-chemical properties of the ionic liquids on the metrological parameters of these sensors. Some metrological...
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Quaestio. Annuario di storia della metafisica / Cahiers d'histoire de la métaphysique / Jahrbuch für die Geschichte der Metaphysik / Journal of the History of Metaphysics.
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A white phosphor based on oxyfluoride nano-glass-ceramics co-doped with Eu3+ and Tb3+: Energy transfer study
PublikacjaStrontium fluoride nanocrystals doped separately with Ln3+ = Eu3+ or Tb3+ ions (95SrF2·5LnF2), as well as co-doped with both the ions (95SrF2·Eu4Tb) were synthesized for comparison. Then, glass-ceramics consisting of the mono-doped or di-doped SrF2 nanocrystals incorporated into amorphous silica (90SiO2·9.5SrF2·0.5Ln or 90SiO2·9.5SrF2·0.1EuF3·0.4Tb) were prepared by sol-gel procedure. The studied materials were characterized by...
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Reactive Sintering of Ground Tire Rubber (GTR) Modified by a Trans-Polyoctenamer Rubber and Curing Additives
PublikacjaThe proposed method of ground tire rubber (GTR) utilization involves the application of trans-polyoctenamer rubber (TOR), a commercially available waste rubber modifier. The idea was to investigate the influence of various curing additives (sulfur, N-cyclohexyl-2-benzothiazole sulfenamide (CBS), dibenzothiazole disulfide (MBTS) and di-(2-ethyl)hexylphosphorylpolysulfide (SDT)) on curing characteristics, physico-mechanical, thermal,...
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Entrepreneurship Today: Selected Aspects
PublikacjaAt its very beginning, entrepreneurship was a purely economic notion. However, this growing interest in entrepreneurship-related problems prompted other sciences to participate in explaining the entrepreneurship phenomenon. Nowadays, entrepreneurship is analyzed through multiple theoretical lenses of economics, management, psychology, sociology – just to name a few. Therefore, it would be difficult to find a notion that could be...
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Piotr Lorens prof. dr hab. inż. arch.
OsobyPiotr Lorens – prof. dr hab. inż. arch., prof. nzw. Politechniki Gdańskiej. Po ukończeniu studiów w 1994 roku podjął pracę w Zakładzie Rozwoju Miasta na Wydziale Architektury Politechniki Gdańskiej. Uzyskawszy Stypendium Fulbrighta wyjechał na staż do USA, gdzie w latach 1996-1997 ukończył Special Program for Urban and Regional Studies na Massachusetts Institute of Technology oraz International Training Program na Harvard University...
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Distance learning trends: introducing new solutions to data analysis courses
PublikacjaNowadays data analysis of any kind becomes a piece of art. The same happens with the teaching processes of statistics, econometrics and other related courses. This is not only because we are facing (and are forced to) teach online or in a hybrid mode. Students expect to see not only the theoretical part of the study and solve some practical examples together with the instructor. They are waiting to see a variety of tools, tutorials,...
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Farzin Kazemi Ph.D. Student at Gdansk University of Technology
OsobyHis main research areas are seismic performance assessment of structures and seismic hazard analysis in earthquake engineering. He performed a comprehensive study on the effect of pounding phenomenon and proposed modification factors to modify the seismic collapse capacity of structures or predict the seismic collapse capacity of structures which were retrofitted with linear and nonlinear Fluid Viscous Dampers (FVDs). His current...
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UAV Design and Construction for Real Time Photogrammetry and Visual Navigation
PublikacjaA unmanned aerial vehicles applications in photogrammetry have increased rapidly last years. A fast data gathering and processing in real time in some cases become crucial and desired in some application. In the paper, a real time solution is proposed. A real time photogrammetry from UAV is proposed, where image data are gathered and processed on board UAV and finally reconstructed 3D model and measurements are delivered. The paper...
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Implementation of control system and tracking objects in a Quadcopter
PublikacjaIn this paper, we implement a quadcopter assembly with control and navigation module. The project also includes the design of the control panel for the operator which consists of a set of the micro-controller and the glove equipped with sensors and buttons. The panel has a touch screen which displays current parameters such as vehicle status, including information about orientation and geographical coordinates. The concept of quadcopter...
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Ekstrakcja do fazy stałej niejedno ma imię
PublikacjaW czasach, gdy we wszystkich przejawach aktywności człowieka trzeba się odnieść do przesłanek leżących u podstaw zrównoważonego rozwoju trudno jest uzasadnić stosowanie w praktyce analitycznej takich procedur i operacji, które pociągają za sobą konieczność:użycia dużych ilości rozpuszczalników i odczynników chemicznychdużych nakładów energii czy też przyczyniają się do wzrostu ekspozycji pracowników laboratoriów na niekorzystne...
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Superconducting transition in granular Bi-Sr-Ca-Cu-O superconductors
PublikacjaW układzie(Bi,Pb)-Sr-Ca-Cu-O poprzez krystalizację w fazie stałej można wytworzyć materiały o bardzo różnych właściwościach elektrycznych i nadprzewodzących. W zależności od warunków krystalizacji, można wytworzyć nadprzewodnik o temperaturze krytycznej między 8 a 105 st. K lub materiał nie przechodzący do stanu nadprzewodzącego. Przejście do stanu nadprzewodzacego w materiałach granulastych ma charakter dwustopniowy. Zbadano wpływ...
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Triplet energy exchange between fluorescent and phosphorescent organic molecules in a solid state matrix.
PublikacjaW pracy przedstawiono model wymiany energii trypletów na podstawie mechanizmu Dextera i zweryfikowano go w układzie dwuamina TPD : organiczny komleks Ir(ppy)3: matryca poliwęglanowa, mierząc czasy życia emisji Ir(ppy)3 przy różnych koncentracjach molekuł TPD.
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Testing interaction models by using x-ray absorption spectroscopy: solid Pb
PublikacjaPraca prezentuje zastosowanie metody EXAFS jako narzędzia do testowania potencjałów oddziaływań międzyatomowych używanych w symulacjach dynamiczno-molekularnych na przykładzie czystego ołowiu w fazie stałej (od temperatury pokojowej do temperatury topnienia). Testowaniu poddano następujące potencjały: dwuciałowy empiryczny potencjał Dzugutova, Larssona i Ebbsjo (DLE), potencjał ciasnego wiązania (TB) i potencjał w modelu osadzonego...
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Mind the framing: Match purpose and context
PublikacjaIn several ways, the following chapters will allude to the concept of frames. The assumptions of a mathematical model tell us what it can explain and what it cannot (see chapter 5). The trade-off between the usefulness of a mathemati- cal model and the scale of complexity it seeks to capture further conditions the narrative, highlighting or downsizing cognitive elements relevant to responsible modelling (see ‘Mathematics and tales’...
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Helicene Monomers and Dimers: Chiral Chromophores Featuring Strong Circularly Polarized Luminescence
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Impact of the trap–assisted recombination in the perovskite solar cells
PublikacjaTo achieve the highest performance using perovskite solar cells it is necessary to understand all the dominant mechanisms which affect the operation of solar cell. Here, we have investigated the bulk and interface trap–assisted recombination processes in the solar cells with p–i–n architecture. These studies are based on the numerical and experimental methods to get better understanding of these physical processes. The following results...