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Search results for: characterization
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Characterization of novel trehalose synthase from Deinococcus geothermalis.
PublicationThe method of trehalose extraction from yeast or othernatural sources is unsuitable for industrial production becauseof its low yield and high cost. Thus, the trehalose synthesizingenzyme systems that originated from a few microorganisms have been investigated.
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Wide range of properties of polyurethanes for medicine - characterization of biomaterials
PublicationW artykule opisano różnorodność poliuretanów stosowanych na polu biomedycznym. Wyrózniono mtody otrzymywania materiałów o róznych własciwościach, a tym samym zastosowaniach. Opisano 10 serii potrzymanych PU oraz wyniki charakterystyki fizycznej, powierzchniowej i biologicznej tych poliuretanów.
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Characterization of recombinant homocitrate synthase from Candida albicans
PublicationLYS21 and LYS22 genes from Candida albicans encoding isoforms of homocitrate synthase (HCS), an enzyme catalyzing the first committed step in the L-lysine biosynthetic pathway, were cloned and expressed as NoligoHistagged fusion proteins in Escherichia coli. The purified gene products revealed HCS activity, i.e. catalyzed the condensation of α-ketoglutarate with acetyl-coenzyme A to yield homocitrate. The recombinant enzymes were purified...
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Preparation and characterization of TiO2 nanostructures for catalytic CO2 photoconversion
PublicationThe titanium dioxide target (99.7%) of 1 cm in dia was ablated in vacuum by laser pulses(6 ns) at 266 nm and at repetition rate of 10 Hz. During deposition the laser fluence between 1 and 3.5 J/cm2 and the O2 pressure from the range of 10-2 - 1 Pa were applied. The thin TiO2 films were deposited on glass substrate (1 × 1 cm2) heated up to 500 °C. The chemical composition of the film and samples produced by annealing were investigated...
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Densimetric and ultrasonic characterization of urea and its derivatives in water
PublicationW oparciu o pomiary gęstości dla serii roztworów jak i rozpuszczalnika wykonanych w temperaturach 15, 20, 25, 30 i 35oC wyznaczono pozorne molowe objętości mocznika, N-metylomocznika, N,N'-dimetylomocznika, N,N,N',N'-tetrametylomocznika, N-etylomocznika, N,N'-dietylomocznika jak i N-butylomocznika w wodzie. Dodatkowe pomiary szybkości dźwięku przeprowadzone w temperaturze 25oC pozwoliły obliczyć ściśliwości adiabatyczne, pozorne...
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Analysis and characterization of coordination compounds by resonance Raman spectroscopy
PublicationResonance Raman spectroscopy has become a powerful tool to study excited-state geometries, excited-state charge distributions and photoinduced reaction dynamics in coordination compounds. Due to their rich photophysical properties coordination compounds are utilized for a variety of applications ranging from DNA sensing to photocatalysis. This review features recent applications of various resonance Raman scattering techniques...
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Novel Biomass-Based Polymers: Synthesis, Characterization, and Application
PublicationA wide range of polymers were prepared from biomass-derivatives, using different polymerization mechanisms. Well-defined, fully hydroxy-functional polyesters based on aliphatic diols were synthesized, using either conventional metal-based catalysts or the organic superbase 1,5,7-triazabicyclododecene (TBD). Unsaturated polyesters were also made, offering additional functionality to these biobased resins. Metal-catalyzed or enzymatic...
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Identification and characterization of the grinding burns by eddy current method
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Preparation and characterization of 3D collagen materials with magnetic properties
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The Characterization of Scaffolds Based on Dialdehyde Chitosan/Hyaluronic Acid
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Cyclosporine CsA—The Physicochemical Characterization of Liposomal and Colloidal Systems
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Preparation, characterization and photocatalytic activity of metal-loaded NaNbO3
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Synthesis and characterization of iron-filled multi-walled nanotubes
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Characterization of the Functionally Graded Shear Modulus of a Half-Space
PublicationIn this article, a method is proposed for determining parameters of the exponentialy varying shear modulus of a functionally graded half-space. The method is based on the analytical solution of the problem of pure shear of an elastic functionally graded half-space by a strip punch. The half-space has the depth-wise exponential variation of its shear modulus, whose parameters are to be determined. The problem is reduced to an integral...
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CHARACTERIZATION STUDY ON MECHANICAL PROPERTIES OF POLYESTER COATED FABRIC
PublicationThe scope of the paper is to determine the mechanical properties of the Precontraint 1302 polyester coated fabric under uniaxial and biaxial tensile tests. The results are compared for Precontraint 1302 fabric and other types of coated fabrics. The author applied an orthotropic model and a dense net model to reflect the polyester coated fabric performance under uniaxial and biaxial tensile tests. Material parameters are specified...
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Application of Impedance Spectroscopy for Bi1−xNdxFeO3 Ceramics Characterization
PublicationIn the present paper the synthesis conditions for fabrication of Bi1−xNdxFeO3 ceramics are reported. The single phase polycrystalline samples of Bi1−xNdxFeO3 were prepared by standard solid state reaction method from the mixture of oxides viz.: Bi2O3, Fe2O3 and Nd2O3. The samples were characterized by impedance spectroscopy in the frequency range 10Hz – 1MHz at room temperature.
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SYNTHESIS AND STRUCTURAL CHARACTERIZATION OF NIOBIUM-DOPED HYDROXYAPATITE CERAMICS
PublicationHydroxyapatite (HAp) ceramic materials are considered as one of the most promising implant materials in bone surgery and in dentistry. They exhibit unique biocompatibility, bioactivity, and osteoconductivity, which are the most desirable biomaterial features. However, HAp itself is brittle, has low strength, high degree of crystallinity and low solubility at physiological pH. Doping synthetic HAp with metal ions plays an important...
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Mid-infrared spectroscopy for characterization of Baltic amber (succinite)
PublicationNatural Baltic amber (succinite) is the most appreciated fossil resin of the rich cultural traditions dating back to prehistoric times. Its unequivocal identification is extremely important in many branches of science and trades including archeology, paleontology, chemistry and finally mineralogical and gemological societies. Current methods of modification of natural succinite are more and more sophisticated making the identification...
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Synthesis and Characterization of Poly(zwitterionic) Structures for Energy Conversion and Storage
PublicationZwitterions are unique class of molecules that possess two functional groups bearing electric charges, one positive and second negative. This setup results in peculiar properties such as high water retention and anti-fouling capability. Therefore, zwitterionic coatings and gels are commonly applied in e.g. biosensing and bioelectronic devices. Despite those applications, there are other perspectives for zwitterionic materials....
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New Complementary Resonator for Permittivity- and Thickness-Based Dielectric Characterization
PublicationThe design of high-performance complementary meta-resonators for microwave sensors featur-ing high sensitivity and consistent evaluation of dielectric materials is challenging. This paper presents the design and implementation of a novel complementary resonator with high sensi-tivity for dielectric substrate characterization based on permittivity and thickness. A comple-mentary crossed arrow resonator (CCAR) is proposed and integrated...
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Growth, Crystal Structure and Magnetic Characterization of Zn-Stabilized CePtIn4
PublicationThe growth and characterization of CePtIn4, stabilized by 10% Zn substitution for In, is reported. The new material is orthorhombic, space group Cmcm (No. 63), with lattice parameters a = 4.51751(4) Å, b = 16.7570(2) Å, and c = 7.36682(8) Å, and the refined crystal composition has 10% of Zn substituted for In, i.e., the crystals are CePt(In0.9Zn0.1)4. Crystals were grown using a self-flux method: only growths containing Zn yielded...
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Characterization of d-xylose reductase, XyrB, from Aspergillus niger
PublicationD-xylose reductase is a member of the aldo-keto reductase family, and is involved in D-xylose and L-arabinose conversion through the Pentose Catabolic Pathway (PCP) in fungi. In this study, we biochemically characterized a newly identified second D-xylose reductase (XyrB) from Aspergillus niger. This NADPH-dependent reductase is able to efficiently convert D-xylose and L-arabinose, and it has the highest affinity for these sugars...
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Characterization of the natural chemical and osmotic environment of early wheat embryogenesis
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Microwave solvothermal synthesis and characterization of manganese-doped ZnO nanoparticles
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Identification and characterization of Staphylococcus spp. and their susceptibility to insect apolipophorin III
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The progress in characterization of polyurethanes morphology with different microscopic methods----WYJAŚNIĆ-----
PublicationW pracy opisano wyniki badań dotyczące analizy morfologii poliuretyanów określanej różnymi metodami. Omówiono mikroskopię optyczną, elektronową, mikroskopię termiczną, mikroskopię fluoroscencyjną, mikro-Ramana i mikroskopię sił atomowych.
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Electromagnetic characterization of a silver nanowire grating embedded into a dielectric slab
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Applying of the optical time-of-flight spectroscopy for the paper and pulp characterization
PublicationW pracy przedstawiono korzyści wykorzystania optycznej spektroskopii czasu przelotu w badaniach papieru i miazgi drzewnej. Przedmiotem badań były różne gatunki papieru oraz miazgi drzewnej (bez obróbki cieplnej, po obróbce cieplnej lub po obróbce chemicznej). W pomiarach wykorzystano półprzewodnikowe lasery impulsowe oraz w charakterze fotoodbiorników kamerę smugową lub licznik fotonów.
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Growth and characterization of chalcopyrite nanocrystals: beyond conventional thin films
PublicationPrzedstawiona została sucha metoda wytwarzania na podłożach stałych kryształów chalkopirytu zawierających miedź z wykorzystaniem prekursorów metalicznych. Dzięki odpowiedniemu doborowi parametrów nakładania otrzymano zarówno nanokryształy oraz polikrystaliczne struktury submikronowe jak i makroskopowe klastry. Zamieszczona została charakterystyka wytworzonych materiałów otrzymana techniką mikroskopii skaningowej.
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Characterization of a cryptic plasmid pSFKW33 from Shewanella sp. 33b
PublicationA cryptic plasmid pSFKW33 from psychrotrophic bacterium Shewanella sp. 33B, an isolate from the Gulf of Gdansk (the Baltic Sea), was sequenced and characterized. It is an 8021 bpcircular molecule with 38% GC content, which shows a distinctive nucleotide sequence without homology to other known plasmids. The nucleotide sequence analysis predicts eight open reading frames. The deduced amino acid sequence of ORF-1 shared significant...
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Pitting corrosion characterization by electrochemical noise measurements on asymmetric electrodes
PublicationKorozja wżerowa stali nierdzewnych może być wykryta za pomocą obserwacji charakterystycznych sygnałów prądowych, jakie płyną między dwiema elektrodami metalowymi. W artykule proponuje się wyznaczanie funkcji bispektrum dla układu dwóch elektrod o istotnie różnej powierzchni narażonej na występowanie korozji. Proponowana metoda została zastosowana do analizy korozji wżerowej stali 0H18N9 powstającej pod wpływem 1M roztworu FeCl3...
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Characterization of low-dose doxorubicin-loaded silica-based nanocomposites
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Preparation and characterization of TiO2/carbon nanowall composite on a transparent substrate
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Copolyester-coated mineral fertilizers – preparation, characterization, and nutrient release
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Synthesis and Characterization of Magnetic Nanomaterials with Adsorptive Properties of Arsenic Ions
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Ziziphora taurica subsp. taurica: Analytical Characterization and Biological Activities
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Slow growth conservation and molecular characterization of Deutzia scabra Thunb
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Characterization of NiTi SMA in its unusual behaviour in wear tests
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Photoelectrochemical and thermal characterization of aromatic hydrocarbons substituted with a dicyanovinyl unit
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Characterization of the Co-base layers obtained by laser cladding technique.
PublicationBadano zawory wydechowe napawane dwoma stopami kobaltu, w tym mikrostrukturę strefy wierzchniej i strefy w pobliżu podłoża. Badano także rozkład pierwiastków w warstwie napawanej. Stwierdzono podobny skład chemiczny warstw i proszków.
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Characterization of wave structures containing sets of bow-tie resonators
PublicationArtykuł opisuje metodę analizy rozpraszania fali elektromagnetycznej układzie rezonatorów motylkowych w strukturach otwartych i zamkniętych. W artykule zaprezentowano przykłady aplikacji układów mikrofalowych zawierające opisywane elementy.
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Characterization of the c-BN/TiC, Ti3SiC2 systems by element selectivespectroscopy.
PublicationPomimo dużego technologicznego zainteresowania tytanowymi kompozytami bazującymi na c-BN daje się zauważyć wyraźny brak danych dotyczących lokalnego otoczenia atomów Ti w tego typu materiałach. Główna przyczyna tego stanu rzeczy tkwi w trudności związanej z analizą układu wielofazowego o dużej twardości za pomocą konwencjonalnych metod. Praca poświęcona jest analizie składu i struktury tytanowych kompozytów za pomocą atomowo-selektywnych...
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Characterization of the Co-base layers obtained by laser cladding technique.
PublicationBadano zawory wylotowe pokrywane stopami kobaltu: mikrostrukturę warstw w strefie wierzchniej i przy granicy napoina - metal. Badano rozkład pierwiastków w warstwach. Zarówno mikrostruktura, jak i skład chemiczny warstw były podobne w przypadku dwóch stosowanych stopów kobaltu.
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Development and Characterization of Bioactive Polypropylene Films for Food Packaging Applications
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Biochemical and Structural Characterization of SplD Protease from Staphylococcus aureus
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Graphene-based Silicone rubber Nanocomposites: Preparation, Characterization, and Properties
PublicationThis study aims to understand better the mechanical, thermal, and tribological behavior of silicone rubber nanocomposites. Graphite, exfoliated graphite, reduced graphene oxide, ionic liquid modified graphene oxide, silane-modified graphene oxide, fumed silica, and other fillers were used in this study. Adding graphene-based fillers to the silicone rubber matrix substantially improves the nanocomposite's mechanical, thermal, and...
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Fabrication and characterization of anode supported solid oxide fuel cells
PublicationW tej pracy, napylanie aerozolowe zawiesiny proszków jest oceniane jako metoda osadzania cienkich elektrolitów tlenkowych ogniw paliwowych. Metoda ta jest tania, prosta i mam zalety w stosunku do szeroko stosowanej metody sitodruku. Wpływ parametrów osadzania: stężenie zawiesiny, ciśnienie robocze są w artykule omawiane.
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Preparation and physicochemical characterization of ceramic supports for supported liquid membranes
PublicationImmobilizowane membrany ciekłe stały się przedmiotem intensywnych badań w ostanich latach, głównie w procesach oczyszczania strumieni gazowych. Kluczowym czynnikiem mającym wpływ na efektywność tych procesów ma czas życia układu membranowego, a zatem odpowiedni dobór nośnika i fazy membranowej. W porównaniu do nośników polimerowych, ceramiczne charakteryzują się większą grubością, jednak są bardziej stabilne termicznie. Praca...
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Preparation and Surface Characterization of Chitosan-Based Coatings for PET Materials
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Reduced graphene oxide and inorganic nanoparticles composites – synthesis and characterization
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