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Search results for: GAS - LIQUID REACTOR
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Modern techniques of sample preparation for determination of organic analytes by gas chromatography
PublicationW pracy dokonano przeglądu szerokiego spektrum technik przygotowania próbki, ze szczególnym uwzględnieniem technik o charakterze prośrodowiskowym. Opisu technik dokonano pod kątem wykorzystywanych mechanizmów izolacji analitów oraz stosowanych rozwiązań aparaturowych. Przegląd rozwiązań aparaturowych uzupełniono o podstawy teoretyczne izolacji bazującej na zjawisku podziału analitów.
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Dissociative electron attachment to gas phase thiothymine: experimental and theoretical approaches
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The Effect of CO2 Gas Emissions on the Market Value, Price and Shares Returns
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Standard gas mixtures – indispensable reference materials in the analysis of gaseous media
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Procedure of determination of volatile trihalomethanes in human urine with pervaporation and gas chromatography
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Non-matrix reference materials-the challenges in the preparation of standard gas mixtures
PublicationIn the last few years particularly great pressure is exerted on quality control and assurance of analytical measurement results. An invaluable role in this process is played by reference materials. The paper presents the characteristics of basic types of reference materials, with particular attention to gaseous reference materials.
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Electrochemical investigations of stainless steels used in flue‐gas desulphurization units
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Enantioselective comprehensive two-dimensional gas chromatography of lavender essential oil
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Ag/Pt-modified TiO2 nanoparticles for toluene photooxidation in the gas phase
PublicationAg/Pt-modified TiO2nanocomposites were synthesized using the sol–gel method. The effect of metal typeand amount as well as synthesis route on the photocatalytic activity in reaction of toluene removal, usedas a model volatile organic compound, was investigated. Toluene, at the concentration of about 200 ppm,was irradiated over modified TiO2using light-emitting diodes (LEDs, max= 415 nm). The results showedthat toluene could be...
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Non-matrix reference matrials- chalanges in the preparation of standard gas mixtures
PublicationIn the last few years particularly great pressure is exerted on quality control and assurance of analytical measurement results. An invaluable role in this process is played by reference materials. The paper presents the characteristics of basic types of reference materials, with particular attention to gaseous reference materials. In addition, a review of literature on techniques of preparation of gaseous standard materials, published...
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Investigation of solid polymer electrolyte gas sensor with different electrochemical techniques
PublicationIn this work solid polymer electrolyte (SPE) amperometric sulphur dioxide sensor is investigated. Nafion was used as a membrane electrode and 1M sulphuric acid as an internal electrolyte. Sensor response to sulphur dioxide was measured. Besides traditional constant voltage amperometry also different electrochemical techniques were used. Results obtained by these methods are compared.
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Some remarks on gas chromatographic challenges in the context of green analytical chemistry
PublicationOmówiono możliwości wprowadzenia zasad zielonej chemii analitycznej w odniesieniu do technik chromatograficznych.
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Properties of a lithium solid electrolyte gas sensor based on reaction kinetics
PublicationW artykule przedstawiono zasadę działania, budowę i właściwości czujnika gazu na bazie elektrolitu stałego z mobilnymi jonami litu. Czujnik został przygotowany w technologii grubowarstwowej. Przedstawiono wyniki badań czujnika w mieszaninach gazów toksycznych.
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Preparation of environmental samples for gas chromatographic determination of selected organic pollutants
PublicationOpisano różne metody izolacji i wzbogacania zanieczyszczeń organicznych z ciekłych, gazowych i stałych próbek środowiskowych. Opisano konstrukcję i testowanie nowych systemów do przygotowania próbek oraz ich zastosowanie w połączeniu z chromatografią gazową do oznaczania zanieczyszczeń organicznych w póbkach rzeczywistych.
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Derivatisation in gas chromatographic determination of acidic herbicides inaqueous environmental samples.
PublicationW pracy przedstawiono przegląd literaturowy dotyczący wykorzystania derywatyzacji w oznaczaniu herbicydów kwasowych w wodnych próbkach środowiskowych za pomocą chromatografii gazowej. Omówiono główne typy reakcji (transestryfikacja, estryfikacja, sililowanie, alkilacja, alkilacja ekstraktywna i pirolityczna), które powodują utworzenie pochodnych, łatwych do analizy techniką chromatografii gazowej. Scharakteryzowano także...
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Flue gas treatment for SO2 removal with air-sparged hydrocyclone technology
PublicationOpisano wstępne wyniki badań laboratoryjnych usuwania SO2 z mieszaniny gazów z zastosowaniem reaktora cyklonowego (ASH). Do absorpcji stosowano wodę wodociągową oraz roztwór alkaliów. Zbadano wpływ natężenia przepływu gazu, natężenia przepływu wody oraz długość elementów ASH. Stwierdzono, że efektywność absorpcji SO2 z powietrza stosując technologię ASH jest porównywalna z efektywnością metod konwencjonalnych.
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Flue gas treatment for SO2 removal with air-sparged hydrocyclone technology
PublicationWyniki badań dowodzą, że reaktor cyklonowy jest wysokosprawnym absorberem. Absorber cyklonowy pozwala na osiągnięcie stopnia redukcji 97% dla samej wody i zawartości dwutlenku siarki w fazie gazowej 5 mg/dm3. Dwutlenek siarki był usuwany również w wodnym rozworze alkaicznym (0.01 mol NaOH/dm3).
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A proposal of ship gas-turbine driven waterjet propulsion - preliminary considerations
PublicationPodstawową rolę w napędzie strugowodnym spełnia pompa. Jest ona napędzana, za pośrednictwem wału przez wysokoprężny silnik spalinowy lub turbinę gazową. Napęd strugowodny może być nawet sprawniejszy energetycznie, niż napęd konwencjonalny (śrubą okrętową), wszakże pod warunkiem właściwego doboru dyszy, pompy i silnika napędowego
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Rozpoznawanie uszkodzeń w części przepływowej okrętowego turbinowego silnika spalinowego na podstawie wyników badania endoskopowego = Failures' recognising within the passages of a marine gas turbine engine on the basis of results of endoscopic investigation
PublicationThe paper deals with diagnostic issues concerning endoscopic examinations of marine gas turbine engines. There will be presented selected information about failures within the passages and accessible endoscopic methods and means enabling their detection. The author focuses on the endoscopic techniques and widely presents the possibilities of this quickly developed diagnostic method. There will be also presented representative results...
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Adoption of the F-statistic of Fisher-Snedecor distribution to analyze importance of impact of modifications of injector opening pressure of a compression ignition engine on specific enthalpy value of exhaust gas flow
PublicationThis article analyzes the effect of modifications of injector opening pressure on the operating values of a compression ignition engine, including the temperature of the fumes. A program of experimental investigation is described, considering the available test stand and measurement capabilities. The structure of the test stand on which the experimental measurements were conducted is presented. The method of introducing real modifications...
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Process Control and Investigation of Oxidation Kinetics of Postoxidative Effluents Using Gas Chromatography with Pulsed Flame Photometric Detection (GC-PFPD)
PublicationThis article presents the results of investigations on the use of headspace analysis and gas chromatography with pulsed flame photometric detection (HSA-GC-PFPD) to evaluate the effectiveness of oxidation of postoxidative effluents from the production of bitumens. Samples of effluents from the bitumen oxidation unit were used in the experiments. In addition, the kinetics of effluent oxidation was also investigated. The content...
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Simultaneous analysis of non-steroidal anti-inflammatory drugs and estrogenic hormones in water and wastewater samples using gas chromatography–mass spectrometry and gas chromatography with electron capture detection
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Techno-economic evaluation of combined cycle gas turbine and a diabatic compressed air energy storage integration concept
PublicationMore and more operational flexibility is required from conventional power plants due to the increasing share of weather-dependent renewable energy sources (RES) generation in the power system. One way to increase power plant’s flexibility is integrating it with energy storage. The energy storage facility can be used to minimize ramping or shutdowns and therefore should lower overall generating costs and CO2 emissions. In this article,...
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Determination of eight artificial sweeteners and common Stevia rebaudiana glycosides in non-alcoholic and alcoholic beverages by reversed-phase liquid chromatography coupled with tandem mass spectrometry.
PublicationThe method for the determination of acesulfame-K, saccharine, cyclamate, aspartame, sucralose, alitame, neohesperidin dihydrochalcone, neotame and five common steviol glycosides (rebaudioside A, rebaudioside C, steviol, steviolbioside and stevioside) in soft and alcoholic beverages was developed using high-performance liquid chromatography and tandem mass spectrometry with electrospray ionisation (HPLC-ESI-MS/MS). To the best of...
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Various types of semiconductor photocatalysts modified by CdTe QDs and Pt NPs for toluene photooxidation in the gas phase under visible light
PublicationA novel synthesis process was used to prepare TiO2 microspheres, TiO2 P-25, SrTiO3 and KTaO3 decorated by CdTe QDs and/or Pt NPs. The effect of semiconductor matrix, presence of CdTe QDs and/or Pt NPs on the semiconductor surface as well as deposition technique of Pt NPs (photodeposition or radiolysis) on the photocatalytic activity were investigated. The as-prepared samples were characterized by X-ray powder diffractometry (XRD),...
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Capillary gas chromatography using a -cyclodextrin forenantiomeric separation of methylamphetamine, its precursors andchloro intermediates after optimization of the derivatization reaction
PublicationtThe enantiomeric ratio of methylamphetamine (MAMP) is closely related to the optical activity of precur-sors and reagents used for the synthesis and this knowledge can provide useful information concerningthe origins and synthetic methods used for illicit manufacture. The information can be utilized for reg-ulation of the precursors and investigation of the manufacturing sources but this requires analyticalprocedures to determine...
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Liquid crystal thermography and true-colour digital image processing in engineering and biomedical research
PublicationWykład dotyczy zastosowań termografii ciekłokrystalicznej i analizy kolorowych obrazów w nieniszczących badaniach inżynierksich oraz w medycynie.
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(Vapour + liquid) equilibrium in (n,n-dimethylacetamide + ethanol + water) at the temperature 313.15 K
PublicationW pracy prezentowane są pomiary całkowitej prężności pary dla tytułowego układu trójskładnikowego oraz dla składowych układów binarnych. Uzyskane w pracy wyniki porównane zostały z wcześniejszymi danymi dla podobnych układów. Znaleziono w przybliżeniu liniową zależność pomiędzy wartościami nadmiarowej entalpii swobodnej Gibbsa a objętością molową amidu, spełnianą w układach dwuskładnikowych: amid + alkohol alifatyczny.
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Surface phenomena in discotic liquid crystals investigated using polarized FTIR transmission spectroscopy
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Anomalous temperature dependence of layer spacing of de Vries liquid crystals: Compensation model
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PhageScore-based analysis of Acinetobacter baumannii infecting phages antibiotic interaction in liquid medium
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Lyotropic liquid crystal based on zinc oxide nanoparticles obtained by microwave solvothermal synthesis
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Potential of Liquid Biopsy in Papillary Thyroid Carcinoma in Context of miRNA, BRAF and p53 Mutation
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Evaluation of methods for determining the combustion ignition delay in a diesel engine powered by liquid biofuel
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Energy resolution and non-proportionality of the light yield of pure CsI at liquid nitrogen temperatures
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Polyfunctional chemically bonded stationary phase for reversed phase high-performance liquid chromatography
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Quantitative structure–retention relationships of ionic liquid cations in characterization of stationary phases for HPLC
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Liquid chromatography tandem mass spectrometry study of urinary nucleosides as potential cancer markers
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Suppression of deleterious effects of free silanols in liquid chromatography by imidazolium tetrafluoroborate ionic liquids
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Comparative study of surface topography of high performance liquid chromatography columns in terms of hydrophobicity
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Development of multilayer coatings for forming dies and tools of aluminium alloy from liquid state
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Characterization of In Vitro and In Vivo Metabolism of Antazoline Using Liquid Chromatography-Tandem Mass Spectrometry
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The use of liquid crystal thermography and particle image velocimetry in the exploration of heat transfer measurements
PublicationArtykuł dotyczy badań eksperymentalnych wymiany ciepła w modelowym wymienniku ciepła z turbulizatorami przepływu przy użyciu termografii ciekłokrystalicznej i cyfrowej anemometrii obrazowej.
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Troubleshooting of the determination of bisphenol A at ultra-trace levels by liquid chromatography and tandem mass spectrometry
PublicationDetermination of trace amounts of bisphenol A (BPA) may cause problems mainly related to the presence of BPA in solvents (even in LC-MS grade), laboratory vessels, and plastic equipment used for sample preparation. Variable and sometimes significant amounts of BPA present in the background cause problems in obtaining good repeatability of measurements at the ultra-trace levels. Such observations (i.e., poor repeatability of results)...
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An inclination in Thermal Energy Using Nanoparticles with Casson Liquid Past an Expanding Porous Surface
PublicationPhysical aspects of inclined MHD nanofluid towards a stretching sheet embedded in a porous medium are visualized. Two types of nanoparticles are used named as copper and alumna dioxide with water as base fluid. Similarity transformations are used to convert the partial differential equations into the set of ordinary differential equation. Closed solutions are found to examine the velocity and the temperature profiles. It is examined...
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(Vapour and liquid) equilibrium in (N,N-dimethylacetamide+methanol+water) at the temperature 313.15 K.
PublicationPraca zawiera wyniki pomiarów całkowitej prężności pary dla tytułowego układu trójskładnikowego oraz dla ''składowych'' układów binarnych. Wyniki obliczeń nadmiarowej energii swobodnej mieszania dla układów (N,N-dimetyloaceta-mid+woda) i (N,N-dimetyloacetamid+metanol) porównane zostały z rezultatami uzyskanymi wcześniej dla innych układów (amid+metanol) oraz (amid+woda). Znaleziono interesującą zależność wartości nadmiaru...
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On the mechanism of oscillations in three-phase system containing coationc surfactant and nitrobenzene liquid membrane
PublicationObserwuje się oscylacje różnicy potencjału elektochemicznego między fazami wodnymi oscylatora zawierającego bromek heksadecylotrimetyloamoniowy. Ta różnica potencjału składa sie z potencjałów na granicach faz między membraną a fazą wodną donorową oraz membraną a fazą wodną akceptorową. Wykazano, że oscylacje zachodzą na granicy fazy akceptorowej i membrany. Są one spowodowane procesami adsorpcji/desorpcji pary jonowej surfaktantu...
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A nontargeted approach to determine the authenticity of Ginkgo biloba L. plant materials and dried leaf extracts by liquid chromatography-high-resolution mass spectrometry (LC-HRMS) and chemometrics
PublicationThe lack of stringent regulations regarding raw materials for herbal supplements used for medicinal purposes has been a constant challenge in the industry. Ginkgo biloba L. leaf extracts attract consumers because of the supposed positive effect on mental performance and memory. Supplements are produced using dried leaf materials and standardized leaf extracts such as EGb 761. Adulteration of Ginkgo biloba L. plants and extracts...
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Removal of ketoprofen from surface water in a submerged photocatalytic membrane reactor utilizing membrane distillation: effect of process parameters and evaluation of long‐term performance
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The Verification of the Usefulness of Electronic Nose Based on Ultra-Fast Gas Chromatography and Four Different Chemometric Methods for Rapid Analysis of Spirit Beverages
PublicationSpirit beverages are a diverse group of foodstuffs. They are very often counterfeited which cause the appearance of low quality products or wrongly labelled products on the market. It is important to find a proper quality control and botanical origin method enabling the same time preliminary check of the composition of investigated samples, which was the main goal of this work. For this purpose, the usefulness of electronic nose...